PD CEN/TS 15968:2010
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
Determination of extractable perfluorooctanesulphonate (PFOS) in coated and impregnated solid articles, liquids and fire fighting foams. Method for sampling, extraction and analysis by LCqMS or LC-tandem/MS
Hardcopy , PDF
27-11-2023
English
31-01-2014
Important note : Users cannot be edited or removed once added to your Multi user PDF.
Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
5 Principle
6 Apparatus and Reagents
7 Sampling
8 Sample pre-treatment
9 Extraction
10 Interference with LC-tandemMS
11 Analysis
12 System suitability test
13 Calculation
14 Expression of results
15 Test report
Annex A (informative) - LC-QMS and LC-TOFMS
Annex B (informative)
Annex C (informative) - Confirmation of compound
identity by MS methods
Bibliography
Establishes the determination of perfluorooctanesulfonate (PFOS) in concentrated extracts from coated and impregnated solid articles, liquids and fire extinguishing foams using high performance liquid chromatography-tandem mass spectrometry (LC-tandemMS) or quadrupole mass spectrometry (LC-qMS).
| Committee |
TCI/100
|
| DevelopmentNote |
Issue Date: 31/01/2014. (02/2014)
|
| DocumentType |
Standard
|
| Pages |
36
|
| PublisherName |
British Standards Institution
|
| Status |
Withdrawn
|
This Technical Specification describes the determination of perfluorooctanesulfonate (PFOS) in concentrated extracts from coated and impregnated solid articles, liquids and fire extinguishing foams using high performance liquid chromatography-tandem mass spectrometry (LC-tandemMS) or quadrupole mass spectrometry (LC-qMS).
The method is applicable for a concentration range for PFOS in the extract solution of 0,5 μg/l to 50 μg/l.
WARNING ― Persons using this Technical Specification should be familiar with normal laboratory practice. This Technical Specification does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions.
IMPORTANT ― It is absolutely essential that tests conducted in accordance with this Technical Specification be carried out by suitably qualified staff.
| Standards | Relationship |
| CEN/TS 15968:2010 | Identical |
| ISO 15194:2009 | In vitro diagnostic medical devices Measurement of quantities in samples of biological origin Requirements for certified reference materials and the content of supporting documentation |
| ISO 6427:2013 | Plastics — Determination of matter extractable by organic solvents (conventional methods) |
| EN ISO 6427:2014 | Plastics - Determination of matter extractable by organic solvents (conventional methods) (ISO 6427:2013) |
| EN ISO 8130-9:1999 | Coating powders - Part 9: Sampling (ISO 8130-9:1992) |
| ISO 187:1990 | Paper, board and pulps — Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples |
| ISO 25101:2009 | Water quality — Determination of perfluorooctanesulfonate (PFOS) and perfluorooctanoate (PFOA) — Method for unfiltered samples using solid phase extraction and liquid chromatography/mass spectrometry |
| ISO 9113:1986 | Plastics Polypropylene (PP) and propylene-copolymer thermoplastics Determination of isotactic index |
| EN 20187:1993 | Paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples (ISO 187:1990) |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| ISO 8466-1:1990 | Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function |
| EN ISO 2419:2012 | Leather - Physical and mechanical tests - Sample preparation and conditioning (ISO 2419:2012) |
| EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
| ISO 8130-9:1992 | Coating powders Part 9: Sampling |
| ISO 2419:2012 | Leather — Physical and mechanical tests — Sample preparation and conditioning |
| EN 12127:1997 | Textiles - Fabrics - Determination of mass per unit area using small samples |
| EN ISO 15194:2009 | In vitro diagnostic medical devices - Measurement of quantities in samples of biological origin - Requirements for certified reference materials and the content of supporting documentation (ISO 15194:2009) |
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