PD CEN/TS 17083:2017
Current
The latest, up-to-date edition.
Foodstuffs. Determination of acrylamide in food and coffee by gas chromatography-mass spectrometry (GC-MS)
Hardcopy , PDF
English
25-08-2017
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European foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Standard solution preparation
6 Apparatus
7 Procedure
8 GC-MS analysis
9 Calculating and reporting
10 Test report
11 Precision data
Annex A (informative) - Typical chromatograms
Annex B (informative) - GC-MS troubleshooting
Annex C (informative) - Single laboratory validation
Annex D (informative) - Interlaboratory trial precision data
Bibliography
Defines a method for the determination of acrylamide in cereal-based products, potato-based products and coffee by gas-chromatography mass spectrometry (GC-MS).
| Committee |
AW/275
|
| DocumentType |
Standard
|
| Pages |
26
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
This Technical Specification specifies a method for the determination of acrylamide in cereal-based products, potato-based products and coffee by gas-chromatography mass spectrometry (GC-MS). The method has been single-laboratory validated via the analysis of spiked samples (French fries (uncooked), bread, water biscuit, infant cereal, biscuit, green coffee, roast coffee and instant coffee), ranging from 30 ?g/kg to 1 500 ?g/kg acrylamide. The results from the single laboratory validation were obtained by a laboratory with significant experience in acrylamide analysis. In addition, this method has also been studied by inter laboratory trial via the analysis of samples containing incurred acrylamide, ranging from approximately 200 ?g/kg to 2 000 ?g/kg. Critical points of the method are identified in 7.5 and Clause 8.
| Standards | Relationship |
| CEN/TS 17083:2017 | Identical |
| ISO 1042:1998 | Laboratory glassware — One-mark volumetric flasks |
| EN ISO 1042:1999 | Laboratory glassware - One-mark volumetric flasks (ISO 1042:1998) |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
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