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PREN 16277 : DRAFT 2011

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

ANIMAL FEEDING STUFFS - DETERMINATION OF MERCURY BY COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CVAAS) AFTER MICROWAVE PRESSURE DIGESTION (EXTRACTION WITH 65% NITRIC ACID AND 30% HYDROGEN PEROXIDE)

Superseded date

01-07-2012

Published date

12-01-2013

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Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus and equipment
6 Procedure
7 Calculation
8 Precision
9 Test report
Annex A (informative) - Results of the interlaboratory
        tests
Annex B (informative) - Flowchart
Annex C (informative) - Adjustment of a microwave oven
Annex D (informative) - Alternative digestion procedure
        with the same extraction efficiency: Acid
        digestion with a mixture of 65% nitric acid and
        70% perchloric acid (7:3 v/v) at atmospheric
        pressure
Annex E (informative) - Alternative digestion procedure
        with the same extraction efficiency: Acid
        digestion with a mixture of 65% nitric acid,
        37% hydrochloric acid and 30% hydrogen peroxide
        under reflux
Bibliography

Describes a method for the determination of mercury in animal feeding stuffs by cold-vapour atomic absorption spectrometry (CVAAS) after microwave pressure digestion.

Committee
TC 327
DocumentType
Draft
PublisherName
Comite Europeen de Normalisation
Status
Superseded

Standards Relationship
DIN EN 16277:2012-09 Identical
11/30199734 DC : 0 Identical

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