UNE-EN ISO 17943:2016
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Water quality - Determination of volatile organic compounds in water - Method using headspace solid-phase micro-extraction (HS-SPME) followed by gas chromatography-mass spectrometry (GC-MS) (ISO 17943:2016)
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Spanish, Castilian, English
14-09-2016
This International Standard specifies a method for the determination of volatile organic compounds. This comprises e.g. halogenated hydrocarbons, trihalogen methanes, gasoline components (like BTEX, MTBE and ETBE), naphthalene, 2-ethyl-4-methyl-1,3-dioxolane and highly odorous substances like geosmin and 2-methylisoborneol in drinking water, ground water, surface water and treated waste water by means of headspace solid-phase microextraction (HS-SPME) followed by gas chromatography-mass spectrometry (GC-MS). The limit of determination depends on the matrix, on the specific compound to be analysed and on the sensitivity of the mass spectrometer. For most compounds to which this International Standard applies, it is at least 0,01 µg/l. Validation data related to a concentration range between 0,02 µg/l and 2,6 µg/l have been demonstrated in an interlaboratory trial. Additional validation data derived from standardization work show applicability of the method within a concentration range from 0,01 µg/l to 100 µg/l of individual substances. All determinations are performed on small sample amounts (e.g. sample volumes of 10 ml).This method is applicable to other compounds not explicitly covered by this International Standard or to other types of water. However, it is necessary to verify the applicability for each case.
| Committee |
CTN 77/SC 1
|
| DocumentType |
Standard
|
| Pages |
50
|
| PublisherName |
Asociación Española de Normalización
|
| Status |
Current
|
| Standards | Relationship |
| EN ISO 17943:2016 | Identical |
| ISO 17943:2016 | Identical |
| ISO 4796-2:2000 | Laboratory glassware — Bottles — Part 2: Conical neck bottles |
| ISO 1042:1998 | Laboratory glassware — One-mark volumetric flasks |
| ISO 648:2008 | Laboratory glassware — Single-volume pipettes |
| ISO 11423-2:1997 | Water quality — Determination of benzene and some derivatives — Part 2: Method using extraction and gas chromatography |
| ISO 11423-1:1997 | Water quality — Determination of benzene and some derivatives — Part 1: Head-space gas chromatographic method |
| ISO 5667-3:2012 | Water quality — Sampling — Part 3: Preservation and handling of water samples |
| ISO 10301:1997 | Water quality — Determination of highly volatile halogenated hydrocarbons — Gas-chromatographic methods |
| ISO 5667-1:2006 | Water quality — Sampling — Part 1: Guidance on the design of sampling programmes and sampling techniques |
| DIN 38407-41:2011-06 | GERMAN STANDARD METHODS FOR THE EXAMINATION OF WATER, WASTE WATER AND SLUDGE - JOINTLY DETERMINABLE SUBSTANCES (GROUP F) - PART 41: DETERMINATION OF SELECTED EASILY VOLATILE ORGANIC COMPOUNDS IN WATER - METHOD USING GAS CHROMATOGRAPHY (GC-MS) AFTER HEADSPACE SOLID-PHASE MICRO EXTRACTION (HS-SPME) (F 41) |
| ISO 15680:2003 | Water quality — Gas-chromatographic determination of a number of monocyclic aromatic hydrocarbons, naphthalene and several chlorinated compounds using purge-and-trap and thermal desorption |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| ISO 5667-5:2006 | Water quality — Sampling — Part 5: Guidance on sampling of drinking water from treatment works and piped distribution systems |
| ISO 8466-1:1990 | Water quality — Calibration and evaluation of analytical methods and estimation of performance characteristics — Part 1: Statistical evaluation of the linear calibration function |
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