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  • UNI CEN/TS 16181 : 2013

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    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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    SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)

    Available format(s): 

    Superseded date:  26-07-2022

    Language(s): 

    Published date:  15-05-2013

    Publisher:  Ente Nazionale Italiano di Unificazione (UNI)

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Interferences
    6 Safety remarks
    7 Reagents
    8 Apparatus
    9 Sample storage and preservation
    10 Procedure
    11 Performance characteristics
    12 Precision
    13 Test report
    Annex A (informative) - Repeatability and
            reproducibility data
    Annex B (informative) - Examples of instrumental
            conditions and chromatograms
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines the quantitative determination of 16 polycyclic aromatic hydrocarbons (PAH) (see Table 2) in sludge, soil and treated biowaste using GC/MS and HPLC-UV-DAD/FLD covering a wide range of PAH contamination levels.

    General Product Information - (Show below) - (Hide below)

    Document Type Technical Specification
    Publisher Ente Nazionale Italiano di Unificazione (UNI)
    Status Superseded
    Superseded By

    Standards Referencing This Book - (Show below) - (Hide below)

    EN ISO 17993 : 2003 WATER QUALITY - DETERMINATION OF 15 POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WATER BY HPLC WITH FLUORESCENCE DETECTION AFTER LIQUID-LIQUID EXTRACTION
    DIN 38414-23:2002-02 GERMAN STANDARD METHODS FOR THE EXAMINATION OF WATER, WASTE WATER AND SLUDGE - SLUDGE AND SEDIMENTS (GROUP S) - PART 23: DETERMINATION OF 15 POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) AND FLUORESCENCE DETECTION (S 23)
    ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
    ISO 18287:2006 Soil quality Determination of polycyclic aromatic hydrocarbons (PAH) Gas chromatographic method with mass spectrometric detection (GC-MS)
    EN 15308:2016 Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
    ISO 5667-15:2009 Water quality — Sampling — Part 15: Guidance on the preservation and handling of sludge and sediment samples
    ISO 17993:2002 Water quality — Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction
    ISO 16720:2005 Soil quality Pretreatment of samples by freeze-drying for subsequent analysis
    ISO 28540:2011 Water quality — Determination of 16 polycyclic aromatic hydrocarbons (PAH) in water — Method using gas chromatography with mass spectrometric detection (GC-MS)
    EN ISO 16720:2007 Soil quality - Pretreatment of samples by freeze-drying for subsequent analysis (ISO 16720:2005)
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
    EN ISO 22892:2011 Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
    EN 15527:2008 Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS)
    EN ISO 5667-15:2009 Water quality - Sampling - Part 15: Guidance on the preservation and handling of sludge and sediment samples (ISO 5667-15:2009)
    EN 15934:2012 Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content
    EN 16179:2012 Sludge, treated biowaste and soil - Guidance for sample pretreatment
    ISO 18512:2007 Soil quality Guidance on long and short term storage of soil samples
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