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  • EN ISO 22892:2011

    Current The latest, up-to-date edition.

    Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)

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    Language(s): 

    Published date:  29-06-2011

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Principle
    3 Terms and definitions
    4 Apparatus
    5 Procedure
    6 Qualification
    7 Test report
    Annex A (informative) - Diagnostic ions to be used for
            identification using GC-MS
    Annex B (informative) - Examples
    Annex C (informative) - Examples of Spectra
    Bibliography

    Abstract - (Show below) - (Hide below)

    ISO 22892:2006 gives criteria for gas chromatography and mass spectrometry (GC-MS) identification of target compounds in soil samples. ISO 22892:2006 is intended for use with standards developed for the determination of specific compounds. The identification criteria are based on the comparison of retention times followed by interpretation of the electron ionization mass spectra, or if necessary, additional mass spectrometric techniques and other relevant factors.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 444
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    DIN EN 16694 E : 2015 WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
    DIN EN 16694:2015-12 WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
    BS EN 15308:2016 Characterization of waste. Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
    DIN EN 16693:2015-12 WATER QUALITY - DETERMINATION OF ORGANOCHLORINE PESTICIDES (OCP) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
    S.R. CEN/TS 16189:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF LINEAR ALKYLBENZENE SULFONATES (LAS) BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) WITH FLUORESCENCE DETECTION (FLD) OR MASS SELECTIVE DETECTION (MS)
    DIN EN 16691 E : 2015 WATER QUALITY - DETERMINATION OF SELECTED POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
    DIN EN 16693 E : 2015 WATER QUALITY - DETERMINATION OF ORGANOCHLORINE PESTICIDES (OCP) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
    DIN EN 16167:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    UNE-EN 16694:2016 Water quality - Determination of selected polybrominated diphenly ether (PBDE) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography - mass spectrometry (GC-MS)
    17/30364005 DC : 0 BS EN 16181 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
    CEN/TS 16189:2012 Sludge, treated biowaste and soil - Determination of linear alkylbenzene sulfonates (LAS) by high-performance liquid chromatography (HPLC) with fluorescence detection (FLD) or mass selective detection (MS)
    CEN/TS 16692:2015 Water quality - Determination of tributyltin (TBT) in whole water samples - Method using solid phase extraction (SPE) with SPE disks and gas chromatography with triple quadrupole mass spectrometry
    13/30291096 DC : 0 BS EN 16694 - WATER QUALITY - DETERMINATION OF PENTABROMODIPHENYL ETHER (PBDE) IN WHOLE WATER SAMPLES USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS)
    DIN EN 16691:2015-12 WATER QUALITY - DETERMINATION OF SELECTED POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
    UNE-EN 16693:2016 Water quality - Determination of organochlorine pesticides (OCP) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC-MS)
    UNE-EN 16377:2014 Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste
    S.R. CEN/TS 16182:2012 SLUDGE TREATED BIOWASTE AND SOIL - DETERMINATION OF NONYLPHENOLS (NP) AND NONYLPHENOL-MONO- AND DIETHOXYLATES USING GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GCMS)
    EN 15308:2016 Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
    S.R. CEN/TS 16181:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
    UNE-EN 15308:2017 Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
    DIN EN 16377 E : 2013 CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE
    BS EN 16167:2012 Sludge, treated biowaste and soil. Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
    XP CEN/TS 16189 : 2012 XP SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF LINEAR ALKYLBENZENE SULFONATES (LAS) BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) WITH FLUORESCENCE DETECTION (FLD) OR MASS SELECTIVE DETECTION (MS)
    13/30290864 DC : 0 BS EN 16691 - WATER QUALITY - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WHOLE WATER SAMPLES USING LIQUID SOLID EXTRACTION COMBINED WITH GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS)
    BS EN 16377:2013 Characterization of waste. Determination of brominated flame retardants (BFR) in solid waste
    13/30291093 DC : 0 BS EN 16693 - WATER QUALITY - DETERMINATION OF ORGANOCHLORINE PESTICIDES (OCP) IN WHOLE WATER SAMPLES USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS)
    UNI CEN/TS 16189 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF LINEAR ALKYLBENZENE SULFONATES (LAS) BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) WITH FLUORESCENCE DETECTION (FLD) OR MASS SELECTIVE DETECTION (MS)
    PREN 15308 : DRAFT 2015 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    I.S. EN 16691:2015 WATER QUALITY - DETERMINATION OF SELECTED POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS)
    17/30364002 DC : 0 BS EN 16167 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    EN 16693:2015 Water quality - Determination of organochlorine pesticides (OCP) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC-MS)
    UNI CEN/TS 16181 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
    EN 16691:2015 WATER QUALITY - DETERMINATION OF SELECTED POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS)
    UNI EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    DIN EN 16377:2013-12 Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste
    BS EN 16691:2015 Water quality. Determination of selected polycyclic aromatic hydrocarbons (PAH) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC-MS)
    PD CEN/TS 16692:2015 Water quality. Determination of tributyltin (TBT) in whole water samples. Method using solid phase extraction (SPE) with SPE disks and gas chromatography with triple quadrupole mass spectrometry
    UNI EN 16377 : 2014 CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE
    UNE-EN 16691:2016 Water quality - Determination of selected polycyclic aromatic hydrocarbons (PAH) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC-MS)
    S.R. CEN/TS 16692:2015 WATER QUALITY - DETERMINATION OF TRIBUTYLTIN (TBT) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE DISKS AND GAS CHROMATOGRAPHY WITH TRIPLE QUADRUPOLE MASS SPECTROMETRY
    UNI CEN/TS 16182 : 2012 SLUDGE TREATED BIOWASTE AND SOIL - DETERMINATION OF NONYLPHENOLS (NP) AND NONYLPHENOL-MONO- AND DIETHOXYLATES USING GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GCMS)
    I.S. EN 16693:2015 WATER QUALITY - DETERMINATION OF ORGANOCHLORINE PESTICIDES (OCP) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS)
    S.R. CEN/TS 16183:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF SELECTED PHTHALATES USING CAPILLARY GAS CHROMATOGRAPHY WITH MASS SPECTROMETRIC DETECTION (GC-MS)
    PREN 16167 : DRAFT 2017 SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    EN 16694 : 2015 WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS)
    EN 16377:2013 Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste
    BS EN 16694:2015 Water quality. Determination of selected polybrominated diphenly ether (PBDE) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography-mass spectrometry (GC-MS)
    I.S. EN 16694:2015 WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENYL ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS)
    UNI CEN/TS 16183 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF SELECTED PHTHALATES USING CAPILLARY GAS CHROMATOGRAPHY WITH MASS SPECTROMETRIC DETECTION (GC-MS)
    15/30330799 DC : 0 BS EN 15308 - CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    12/30255723 DC : 0 BS EN 16377 - CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE
    BS EN 16693:2015 Water quality. Determination of organochlorine pesticides (OCP) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC-MS)
    XP CEN/TS 16182 : 2012 XP SLUDGE TREATED BIOWASTE AND SOIL - DETERMINATION OF NONYLPHENOLS (NP) AND NONYLPHENOL-MONO- AND DIETHOXYLATES USING GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS)
    I.S. EN 15308:2016 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    I.S. EN 16167:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRONCAPTURE DETECTION (GC-ECD)
    EN 16167:2012 Sludge, treated biowaste and soil - Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
    I.S. EN 16377:2013 CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE
    CEN/TS 16181:2013 Sludge, treated biowaste and soil - Determination of polycyclic aromatic hydrocarbons (PAH) by gas chromatography (GC) and high performance liquid chromatography (HPLC)
    CEN/TS 16183:2012 Sludge, treated biowaste and soil - Determination of selected phthalates using capillary gas chromatography with mass spectrometric detection (GC-MS)
    CEN/TS 16182:2012 Sludge treated biowaste and soil - Determination of nonylphenols (NP) and nonylphenol-mono- and diethoxylates using gas chromatography with mass selective detection (GC-MS)

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
    ISO 15009:2016 Soil quality Gas chromatographic determination of the content of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons Purge-and-trap method with thermal desorption
    ISO 11264:2005 Soil quality Determination of herbicides Method using HPLC with UV-detection
    ISO 10382:2002 Soil quality — Determination of organochlorine pesticides and polychlorinated biphenyls — Gas-chromatographic method with electron capture detection
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