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UNI EN 15527 : 2008

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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CHARACTERIZATION OF WASTE - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WASTE USING GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC/MS)

Superseded date

01-09-2022

Superseded by

UNI EN 17503:2022

Published date

26-11-2008

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Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
   5.1 General
   5.2 Reagents for extraction procedures
   5.3 Reagents for clean-up procedures
   5.4 Reagents for gas chromatographic analysis
   5.5 Standards
6 Apparatus
   6.1 Extraction and clean-up procedures
   6.2 Gas chromatograph
   6.3 Capillary columns
   6.4 Preparation of standard solutions
7 Hazards
8 Interference
   8.1 Interference during sampling, storage
        and extraction
   8.2 Interference due to co-elution
9 Sample conservation
10 Pretreatment
   10.1 General
   10.2 Drying
   10.3 Particle size reduction
11 Procedure
   11.1 Blank
   11.2 Extraction
   11.3 Addition of the internal standard solution
   11.4 Concentration or dilution
   11.5 Clean up of the extract
   11.6 Addition of the injection standard
   11.7 Gas chromatographic analysis with mass
        spectrometric detection
12 Performance characteristics
13 Test report
Annex A (informative) - Representative chromatograms
Annex B (informative) - Additional validation data
Annex C (informative) - Summary of general requirements
        and recommendations
Bibliography

Describes the quantitative determination of 16 polynuclear aromatic hydrocarbons (PAH) according to the priority list of the Environmental Protection Agency (EPA, 1982).

Committee
CT 4
DevelopmentNote
Supersedes UNI/TS 11223. (11/2008)
DocumentType
Standard
PublisherName
Ente Nazionale Italiano di Unificazione (UNI)
Status
Superseded
SupersededBy
Supersedes

Standards Relationship
EN 15527:2008 Identical

UNI 10802 : 2013 WASTES - MANUAL SAMPLING AND PREPARATION OF SAMPLE AND ANALYSIS OF ELUATES

ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 18287:2006 Soil quality Determination of polycyclic aromatic hydrocarbons (PAH) Gas chromatographic method with mass spectrometric detection (GC-MS)
EN 14346:2006 Characterization of waste - Calculation of dry matter by determination of dry residue or water content
ISO 16720:2005 Soil quality Pretreatment of samples by freeze-drying for subsequent analysis
EN ISO 16720:2007 Soil quality - Pretreatment of samples by freeze-drying for subsequent analysis (ISO 16720:2005)
ISO 14507:2003 Soil quality Pretreatment of samples for determination of organic contaminants
EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample

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