ASTM C 1128 : 2018 : REDLINE
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
17-02-2023
English
30-01-2018
CONTAINED IN VOL. 12.01, 2018 Defines the preparation and characterization of working reference materials (WRM) that are produced by a laboratory for its own use in the analysis of nuclear materials.
Committee |
C 26
|
DocumentType |
Redline
|
Pages |
26
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy |
1.1This guide covers the preparation and characterization of working reference materials (WRM) that are produced by a laboratory for its own use in the analysis of nuclear fuel cycle materials. Guidance is provided for proper preparation, packaging, and storage; requirements for characterization; homogeneity and stability considerations; and establishing traceability of WRMs to certified reference materials by a defined, statistically sound characterization process. While the guidance provided is generic for nuclear fuel cycle materials, detailed examples for some materials are provided in the appendixes.
1.2This guide does not apply to the preparation and characterization of certified reference materials (CRM). Refer to ISO 17034 and Guide 35 for those requirements.
1.3The information provided by this guide is found in the following sections:
Section | |
Perform WRM Planning | 6 |
Select, Collect, Prepare, and Process Materials | 7 |
Packaging and Store Materials | 8 |
Perform Homogeneity Study | 9 |
Perform Stability Studies | 10 |
Characterize Materials | 11 |
Perform Uncertainty Analysis | 12 |
Produce Documentation | 13 |
Carry Out WRM Utilization and Monitoring | 14 |
1.4The values stated in SI units are to be regarded as standard. Any non-SI units of measurement shown in parentheses are for information only.
1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ISO/IEC 17025:2005 | General requirements for the competence of testing and calibration laboratories |
ISO 17034:2016 | General requirements for the competence of reference material producers |
ISO Guide 33:2015 | Reference materials — Good practice in using reference materials |
ASTM C 1625 : 2012 : REDLINE | Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry |
ASTM C 1637 : 2013 : REDLINE | Standard Test Method for the Determination of Impurities in Plutonium Metal: Acid Digestion and Inductively Coupled Plasma-Mass Spectroscopy (ICP-MS) Analysis |
ISO 10576-1:2003 | Statistical methods — Guidelines for the evaluation of conformity with specified requirements — Part 1: General principles |
ISO Guide 35:2017 | Reference materials — Guidance for characterization and assessment of homogeneity and stability |
ISO Guide 80:2014 | Guidance for the in-house preparation of quality control materials (QCMs) |
ISO/IEC Guide 99:2007 | International vocabulary of metrology Basic and general concepts and associated terms (VIM) |
ISO Guide 30:2015 | Reference materials — Selected terms and definitions |
ASTM C 1672 : 2017 : REDLINE | Standard Test Method for Determination of Uranium or Plutonium Isotopic Composition or Concentration by the Total Evaporation Method Using a Thermal Ionization Mass Spectrometer |
ASTM C 1068 : 2015 : REDLINE | Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry |
ASTM C 1168 : 2015 : REDLINE | Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis |
ISO Guide 31:2015 | Reference materials — Contents of certificates, labels and accompanying documentation |
ISO/IEC Guide 98-3:2008 | Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995) |
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