• Shopping Cart
    There are no items in your cart

ASTM C 1128 : 2023

Current

Current

The latest, up-to-date edition.

Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

13-02-2023

€80.76
Excluding VAT

Committee
C 26
DocumentType
Guide
Pages
29
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1This guide covers the preparation and characterization of working reference materials (WRM) that are produced by a laboratory for its own use in the analysis of nuclear fuel cycle materials. Guidance is provided for proper planning, preparation, packaging, and storage; requirements for characterization; homogeneity and stability considerations; and value assignment. When traceability to SI is desired for a WRM, it will be achieved by a defined, statistically sound characterization process that is traceable to a certified value on a certified reference materials. While the guidance provided is generic for nuclear fuel cycle materials, detailed examples for some materials are provided in the appendixes.

1.2This guide does not apply to the production and characterization of certified reference materials (CRM). Refer to ISO 17034 and ISO Guide 35 for guidance on reference material production, characterization, certification, sale, and distribution requirements.

1.3The information provided by this guide is found in the following sections:

Section

Perform WRM Planning

6

Prepare and Process Materials

7

Packaging and Storage of Materials

8

Perform Homogeneity Study

9

Perform Stability Studies

10

Characterize Materials

11

Perform Uncertainty Analysis

12

Produce Documentation

13

Carry Out WRM Utilization and Monitoring

14

1.4The values stated in SI units are to be regarded as standard. The non-SI units of molar, M, and normal, N, are also regarded as standard. Any non-SI units of measurement shown in parentheses are for information only.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM C 1316 : 2008 : R2017 Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using <sup>252</sup>Cf Shuffler
ASTM C 1297 : 2018 Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
ASTM C 1855 : 2018 Standard Test Method for Determination of Uranium and Plutonium Concentration in Aqueous Solutions Using Hybrid K-Edge Densitometry and X-Ray Fluorescence
ASTM C 1832 : 2023 Standard Test Method for Determination of Uranium Isotopic Composition by Modified Total Evaporation (MTE) Method Using Thermal Ionization Mass Spectrometer
ASTM C 1267 : 2017 : R2022 Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium
ASTM C 1204 : 2014 : R2023 Standard Test Method for Uranium in Presence of Plutonium by Iron(II) Reduction in Phosphoric Acid Followed by Chromium(VI) Titration
ASTM C 1207 : 2010 : R2018 Standard Test Method for Nondestructive Assay of Plutonium in Scrap and Waste by Passive Neutron Coincidence Counting
ASTM C 1718 : 2010 : R2019 Standard Test Method for Nondestructive Assay of Radioactive Material by Tomographic Gamma Scanning
ASTM C 761 : 2018 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Uranium Hexafluoride
ASTM C 1625 : 2019 Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry
ASTM E 3264 : 2021 Standard Guide for Homogeneity of Samples and Reference Materials Used for Inter- and Intra-Laboratory Studies
ASTM C 1865 : 2018 Standard Test Method for The Determination of Carbon and Sulfur Content in Plutonium Oxide Powder by the Direct Combustion-Infrared Spectrophotometer
ASTM C 791 : 2019 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Boron Carbide
ASTM C 1592/C1592M : 2021 Standard Guide for Making Quality Nondestructive Assay Measurements
ASTM C 1009 : 2021 Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry
ASTM C 759 : 2018 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Nitrate Solutions
ASTM C 1210 : 2021 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry
ASTM C 809 : 2019 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Aluminum Oxide and Aluminum<brk/>Oxide-Boron Carbide Composite Pellets
ASTM C 1133/C1133M : 2010 : R2018 Standard Test Method for Nondestructive Assay of Special Nuclear Material in Low-Density Scrap and Waste by Segmented Passive Gamma-Ray Scanning
ASTM C 758 : 2018 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal
ASTM C 1156 : 2018 Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
ASTM C 1871 : 2022 Standard Test Method for Determination of Uranium Isotopic Composition by the Double Spike Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1068 : 2021 Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry

ASTM C 1168 : 2023 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 1165 : 2023 Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<inf>2</inf>SO<inf>4</inf> at a Platinum Working Electrode
ASTM C 1108 : 2023 Standard Test Method for Plutonium by Controlled-Potential Coulometry
ASTM C 859 : 2023 Standard Terminology Relating to Nuclear Materials
ASTM C 859 : 2024 Standard Terminology Relating to Nuclear Materials
ASTM C 1672 : 2017 Standard Test Method for Determination of Uranium or Plutonium Isotopic Composition or Concentration by the Total Evaporation Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1165 : 2022 Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<inf>2</inf>SO<inf>4</inf> at a Platinum Working Electrode
ASTM C 1672 : 2023 Standard Test Method for Determination of the Uranium, Plutonium or Americium Isotopic Composition or Concentration by the Total Evaporation Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1168 : 2015 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 1689 : 2021 Standard Practice for Subsampling of Uranium Hexafluoride
ASTM C 859 : 2022 : REV A Standard Terminology Relating to Nuclear Materials
ASTM D 8293 : 2022 Standard Guide for Evaluating and Expressing the Uncertainty of Radiochemical Measurements
ASTM C 1108 : 2022 Standard Test Method for Plutonium by Controlled-Potential Coulometry

Access your standards online with a subscription

Features

  • Simple online access to standards, technical information and regulations.

  • Critical updates of standards and customisable alerts and notifications.

  • Multi-user online standards collection: secure, flexible and cost effective.