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ASTM C 1432 : 2015

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Determination of Impurities in Plutonium: Acid Dissolution, Ion Exchange Matrix Separation, and Inductively Coupled Plasma-Atomic Emission Spectroscopic (ICP/AES) Analysis

Available format(s)

Hardcopy , PDF

Superseded date

23-01-2024

Superseded by

ASTM C 1432 : 2023

Language(s)

English

Published date

13-07-2015

€67.30
Excluding VAT

Committee
C 26
DocumentType
Test Method
Pages
5
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers the determination of 25 elements in plutonium (Pu) materials. The Pu is dissolved in acid, the Pu matrix is separated from the target impurities by an ion exchange separation, and the concentrations of the impurities are determined by inductively coupled plasma-atomic emission spectroscopy (ICP-AES).

1.2This test method is specific for the determination of impurities in 8 M HNO3 solutions. Impurities in other plutonium materials, including plutonium oxide samples, may be determined if they are appropriately dissolved (see Practice C1168) and converted to 8 M HNO3 solutions.

1.3The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions that are provided for information only and are not considered standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM C 698 : 2016 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Mixed Oxides ((U, Pu)O<inf>2</inf>)
ASTM C 697 : 2016 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Plutonium Dioxide Powders and Pellets
ASTM C 1637 : 2013 Standard Test Method for the Determination of Impurities in Plutonium Metal: Acid Digestion and Inductively Coupled Plasma-Mass Spectroscopy (ICP-MS) Analysis
ASTM C 759 : 2018 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Nitrate Solutions
ASTM C 758 : 2018 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal
ASTM C 1647 : 2013 Standard Practice for Removal of Uranium or Plutonium, or both, for Impurity Assay in Uranium or Plutonium Materials
ASTM C 1637 : 2021 Standard Test Method for Determination of Impurities in Plutonium Materials—Acid Digestion and Inductively Coupled Plasma-Mass Spectroscopy (ICP-MS) Analysis
ASTM C 1647 : 2020 Standard Practice for Removal of Uranium or Plutonium, or both, for Impurity Assay in Uranium or Plutonium Materials

ASTM C 1168 : 2023 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 859 : 2023 Standard Terminology Relating to Nuclear Materials
ASTM C 859 : 2014 : REV B Standard Terminology Relating to Nuclear Materials
ASTM C 757 : 1990 : R1996 : EDT 1 Standard Specification for Nuclear-Grade Plutonium Dioxide Powder, Sinterable
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM C 757 : 2016 : EDT 1 Standard Specification for Nuclear-Grade Plutonium Dioxide Powder for Light Water Reactors
ASTM C 1168 : 2015 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM C 757 : 2016 : R2021 Standard Specification for Nuclear-Grade Plutonium Dioxide Powder for Light Water Reactors
ASTM C 859 : 2022 Standard Terminology Relating to Nuclear Materials
ASTM C 859 : 2022 : REV A Standard Terminology Relating to Nuclear Materials
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM C 1168 : 2001 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 1168 : 1990 : R1995 : EDT 1 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM C 1168 : 2008 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis

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