• ASTM C 613 : 2019

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Test Method for Constituent Content of Composite Prepreg by Soxhlet Extraction

    Available format(s):  Hardcopy, PDF

    Superseded date:  05-12-2023

    Language(s):  English

    Published date:  20-05-2019

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    This test method covers a Soxhlet extraction procedure to determine the matrix content, reinforcement content, and filler content of composite material prepreg.

    Scope - (Show below) - (Hide below)

    1.1This test method covers a Soxhlet extraction procedure to determine the matrix content, reinforcement content, and filler content of composite material prepreg. Volatiles content, if appropriate, and required, is determined by means of Test Method D3530.

    1.1.1The reinforcement and filler must be substantially insoluble in the selected extraction reagent and any filler must be capable of being separated from the reinforcement by filtering the extraction residue.

    1.1.2Reinforcement and filler content test results are total reinforcement content and total filler content; hybrid material systems with more than one type of either reinforcement or filler cannot be distinguished.

    1.2This test method focuses on thermosetting matrix material systems for which the matrix may be extracted by an organic solvent. However, other, unspecified, reagents may be used with this test method to extract other matrix material types for the same purposes.

    1.3Alternate techniques for determining matrix and reinforcement content include Test Methods D3171 (matrix digestion), D2584 (matrix burn-off/ignition), and D3529 (matrix dissolution and ignition loss). Test Method D2584 is preferred for reinforcement materials, such as glass, quartz, or silica, that are unaffected by high-temperature environments.

    1.4The technical content of this standard has been stable since 1997 without significant objection from its stakeholders. As there is limited technical support for the maintenance of this standard, changes since that date have been limited to items required to retain consistency with other ASTM D30 Committee standards. The standard therefore should not be considered to include any significant changes in approach and practice since 1997. Future maintenance of the standard will only be in response to specific requests and performed only as technical support allows.

    1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9 and 7.2.3 and 8.2.1.

    1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee D 30
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 4762 : 2023 Standard Guide for Testing Polymer Matrix Composite Materials

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 3171 : 1999 Standard Test Methods for Constituent Content of Composite Materials
    ASTM D 883 : 2023 Standard Terminology Relating to Plastics
    ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
    ASTM D 2584 : 2002 Standard Test Method for Ignition Loss of Cured Reinforced Resins
    ASTM E 456 : 2002 Standard Terminology for Relating to Quality and Statistics
    ASTM D 3878 : 2002 : REV A Standard Terminology for Composite Materials
    ASTM D 3878 : 2023 Standard Terminology for Composite Materials
    ASTM E 456 : 2013 : REV A : R2022 Standard Terminology Relating to Quality and Statistics
    ASTM D 3878 : 2015 Standard Terminology for Composite Materials
    ASTM D 3529 : 2016 : R2021 Standard Test Methods for Constituent Content of Composite Prepreg
    ASTM D 2584 : 2008 Standard Test Method for Ignition Loss of Cured Reinforced Resins
    ASTM D 3878 : 2019 Standard Terminology for Composite Materials
    ASTM D 3878 : 2000 Standard Terminology Composite Materials
    ASTM D 2584 : 1994 Standard Test Method for Ignition Loss of Cured Reinforced Resins
    ASTM D 883 : 2022 Standard Terminology Relating to Plastics
    ASTM D 883 : 2020 : REV B Standard Terminology Relating to Plastics
    ASTM D 3171 : 2011 Standard Test Methods for Constituent Content of Composite Materials
    ASTM D 3529 : 2016 Standard Test Methods for Constituent Content of Composite Prepreg
    ASTM E 456 : 2013 : REV A : R2017 : EDT 5 Standard Terminology Relating to Quality and Statistics
    ASTM E 122 : 2017 : R2022 Standard Practice for Calculating Sample Size to Estimate, With Specified Precision, the Average for a Characteristic of a Lot or Process
    ASTM E 122 : 2017 Standard Practice for Calculating Sample Size to Estimate, With Specified Precision, the Average for a Characteristic of a Lot or Process
    ASTM D 3878 : 2003 : REV A Standard Terminology for Composite Materials
    ASTM D 2584 : 2011 Standard Test Method for Ignition Loss of Cured Reinforced Resins
    ASTM D 3878 : 2016 Standard Terminology for Composite Materials
    ASTM D 3530 : 1997 : R2015 Standard Test Method for Volatiles Content of Composite Material Prepreg
    ASTM D 3878 : 2019 : REV A Standard Terminology for Composite Materials
    ASTM D 3878 : 2020 : REV A Standard Terminology for Composite Materials
    ASTM D 3878 : 1998 Standard Terminology Composite Materials
    ASTM D 3171 : 2022 Standard Test Methods for Constituent Content of Composite Materials
    ASTM D 3878 : 2018 Standard Terminology for Composite Materials
    ASTM D 3171 : 2009 Standard Test Methods for Constituent Content of Composite Materials
    ASTM D 3878 : 2002 Standard Terminology for Composite Materials
    ASTM D 3878 : 2020 : REV B Standard Terminology for Composite Materials
    ASTM D 2584 : 1968 Standard Method Of Test For Ignition Loss Of Cured Reinforced Resins
    ASTM D 3878 : 2004 Standard Terminology for Composite Materials
    ASTM D 3878 : 2007 : R2013 Standard Terminology for Composite Materials
    ASTM D 3878 : 2020 : REDLINE Standard Terminology for Composite Materials
    ASTM D 3878 : 2020 Standard Terminology for Composite Materials
    ASTM D 2584 : 2018 Standard Test Method for Ignition Loss of Cured Reinforced Resins
    ASTM D 3878 : 2003 Standard Terminology for Composite Materials
    ASTM D 3878 : 2007 Standard Terminology for Composite Materials
    ASTM D 3171 : 1999 : R2004 Standard Test Methods for Constituent Content of Composite Materials
    ASTM D 3171 : 2015 Standard Test Methods for Constituent Content of Composite Materials
    ASTM E 456 : 2013 : REV A : R2017 : EDT 4 Standard Terminology Relating to Quality and Statistics
    ASTM E 456 : 2013 : REV A : R2017 : EDT 6 Standard Terminology Relating to Quality and Statistics
    ASTM D 3878 : 2004 : REV A Standard Terminology for Composite Materials
    ASTM D 3171 : 2006 Standard Test Methods for Constituent Content of Composite Materials
    ASTM D 3878 : 2001 Standard Terminology Composite Materials
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