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ASTM C 758 : 2018

Current

Current

The latest, up-to-date edition.

Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-09-2018

€56.53
Excluding VAT

1.1These test methods cover procedures for the chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of nuclear-grade plutonium metal to determine compliance with specifications.

Committee
C 26
DocumentType
Test Method
Pages
9
ProductNote
THIS STANDARD ALSO REFERS TO ASTM C1108, ASTM C 1297, ASTM C 1165 ,ASTM C 1156
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1These test methods cover procedures for the chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of nuclear-grade plutonium metal to determine compliance with specifications.

1.2The analytical procedures appear in the following order:

Sections

Dissolution Procedure

2

Plutonium by Controlled-Potential Coulometry

3

Plutonium by Amperometric Titration with Iron (II)

2

Plutonium by Ceric Sulfate Titration Test Method

3

Plutonium by Diode Array Spectrophotometry

3

Uranium by Arsenazo I Spectrophotometric Test Method

8 – 10

Thorium by Thorin Spectrophotometric Test Method

11 – 13

Iron by 1,10-Phenanthroline Spectrophotometric Test Method

14 – 16

Iron by 2,2ʹ-Bipyridyl Spectrophotometric Test Method

17 – 23

Impurities by ICP-AES

Chloride by the Thiocyanate Spectrophotometric Test Method

24 – 26

Fluoride by Distillation-Spectrophotometric Test Method

2728

Nitrogen by Distillation-Nessler Reagent Spectrophotometric Test
 Method

2930

Carbon by the Direct Combustion-Thermal Conductivity Test
 Method

31 – 33

Sulfur by Distillation-Spectrophotometric Test Method

34 – 36

Isotopic Composition by Mass Spectrometry

37 and 38

Plutonium-238 Isotopic Abundance by Alpha Spectrometry

Americium-241 by Extraction and Gamma Counting

39 – 41

Americium-241 by Gamma Counting

3

Gamma-Emitting Fission Products, Uranium, and Thorium by
 Gamma-Ray Spectroscopy

42 – 49

Rare Earths by Copper Spark Spectrochemical Test Method

50 – 52

Tungsten, Niobium (Columbium), and Tantalum by Spectro-
 chemical Test Method

53 – 55

Sample Preparation for Spectrographic Analysis for Trace Impuri-
 ties

56 – 60

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific safeguard and safety hazards statements, see Section 6.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM C 1206 : 2002 : R2010 Standard Test Method for Plutonium by Iron (II)/Chromium (VI) Amperometric Titration (Withdrawn 2015)
ASTM C 1168 : 2023 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 1165 : 2023 Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<inf>2</inf>SO<inf>4</inf> at a Platinum Working Electrode
ASTM C 1009 : 2013 : REV A Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry
ASTM C 1307 : 2015 Standard Test Method for Plutonium Assay by Plutonium (III) Diode Array Spectrophotometry
ASTM C 1415 : 2001 Standard Test Method for <sup>238</sup>Pu Isotopic Abundance by Alpha Spectrometry
ASTM C 1108 : 2023 Standard Test Method for Plutonium by Controlled-Potential Coulometry
ASTM C 859 : 2023 Standard Terminology Relating to Nuclear Materials
ASTM C 1210 : 2018 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM C 1415 : 1999 Standard Test Method for <sup>238</sup>Pu Isotopic Abundance by Alpha Spectrometry
ASTM C 859 : 2014 : REV B Standard Terminology Relating to Nuclear Materials
ASTM C 859 : 2024 Standard Terminology Relating to Nuclear Materials
ASTM C 1128 : 2018 Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM C 1206 : 1991 : R1996 Standard Test Method for Plutonium by Iron (II)/Chromium (VI) Amperometric Titration
ASTM C 1268 : 1994 : R2008 Standard Test Method for Quantitative Determination of Americium 241 in Plutonium by Gamma-Ray Spectrometry
ASTM C 1268 : 2015 Standard Test Method for Quantitative Determination of <sup>241</sup>Am in Plutonium by Gamma-Ray Spectrometry
ASTM C 1009 : 1996 : EDT 1 Standard Guide for Establishing a Quality Assurance Program for Analytical Chemistry Laboratories Within the Nuclear Industry (Withdrawn 2005)
ASTM C 1235 : 1999 Standard Test Method for Plutonium by Titanium(III)/Cerium(IV) Titration (Withdrawn 2005)
ASTM C 1210 : 1996 : EDT 1 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry (Withdrawn 2005)
ASTM C 1210 : 2021 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry
ASTM C 1165 : 1990 : R2005 Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<sub>2</sub>SO<sub>4</sub> at a Platinum Working Electrode
ASTM C 1128 : 1995 : EDT 1 Standard Guide for Preparation of Working Reference Materials for Use in the Analysis of Nuclear Fuel Cycle Materials
ASTM C 1068 : 1996 : EDT 1 Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
ASTM C 1165 : 2022 Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<inf>2</inf>SO<inf>4</inf> at a Platinum Working Electrode
ASTM C 1108 : 2017 Standard Test Method for Plutonium by Controlled-Potential Coulometry
ASTM C 1156 : 2003 : R2011 Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
ASTM C 1307 : 2002 : R2008 Standard Test Method for Plutonium Assay by Plutonium (III) Diode Array Spectrophotometry
ASTM C 1210 : 2012 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM C 1168 : 2015 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 1432 : 2023 Standard Test Method for Determination of Impurities in Plutonium: Acid Dissolution, Ion Exchange Matrix Separation, and Inductively Coupled Plasma-Atomic Emission Spectroscopic (ICP/AES) Analysis
ASTM C 1206 : 2002 Standard Test Method for Plutonium by Iron (II)/Chromium (VI) Amperometric Titration
ASTM C 1165 : 1990 : R2000 : EDT 1 Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<sub>2</sub>SO<sub>4</sub> at a Platinum Working Electrode
ASTM C 1128 : 2015 Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
ASTM C 1068 : 2003 : R2011 Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
ASTM C 1210 : 2006 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM C 1432 : 2003 Standard Test Method for Determination of Impurities in Plutonium: Acid Dissolution, Ion Exchange Matrix Separation, and Inductively Coupled Plasma-Atomic Emission Spectroscopic (ICP/AES) Analysis
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM C 1108 : 1999 Standard Test Method for Plutonium by Controlled-Potential Coulometry
ASTM C 1415 : 2014 Standard Test Method for <sup>238</sup>Pu Isotopic Abundance By Alpha Spectrometry
ASTM C 1432 : 2003 : R2008 Standard Test Method for Determination of Impurities in Plutonium: Acid Dissolution, Ion Exchange Matrix Separation, and Inductively Coupled Plasma-Atomic Emission Spectroscopic (ICP/AES) Analysis
ASTM C 1068 : 2015 Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
ASTM C 1415 : 2001 : REV A : R2007 Standard Test Method for <sup>238</sup>Pu Isotopic Abundance by Alpha Spectrometry
ASTM C 1307 : 1995 Standard Test Method for Plutonium Assay by Plutonium (III) Diode Array Spectrophotometry
ASTM C 1068 : 2021 Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
ASTM C 1165 : 2012 Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<inf>2</inf>SO<inf>4</inf> at a Platinum Working Electrode
ASTM C 1432 : 2015 Standard Test Method for Determination of Impurities in Plutonium: Acid Dissolution, Ion Exchange Matrix Separation, and Inductively Coupled Plasma-Atomic Emission Spectroscopic (ICP/AES) Analysis
ASTM C 1297 : 2003 : R2011 Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
ASTM C 1297 : 2003 Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
ASTM C 1268 : 1994 : R2000 Standard Test Method for Quantitative Determination of Americium 241 in Plutonium by Gamma-Ray Spectrometry
ASTM C 859 : 2022 Standard Terminology Relating to Nuclear Materials
ASTM C 859 : 2022 : REV A Standard Terminology Relating to Nuclear Materials
ASTM C 1297 : 1995 : EDT 1 Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM C 1156 : 2018 Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
ASTM C 1128 : 2023 Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
ASTM C 1128 : 2001 Standard Guide for Preparation of Working Reference Materials for Use in the Analysis of Nuclear Fuel Cycle Materials
ASTM C 1068 : 2003 Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
ASTM C 1307 : 2014 Standard Test Method for Plutonium Assay by Plutonium (III) Diode Array Spectrophotometry
ASTM C 1268 : 2023 Standard Test Method for Quantitative Determination of <sup>241</sup>Am in Plutonium by Gamma-Ray Spectrometry
ASTM C 1307 : 2021 Standard Test Method for Plutonium Assay by Plutonium (III) Diode Array Spectrophotometry
ASTM C 1156 : 1995 : EDT 1 Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
ASTM C 1108 : 2022 Standard Test Method for Plutonium by Controlled-Potential Coulometry
ASTM C 1108 : 2012 Standard Test Method for Plutonium by Controlled-Potential Coulometry
ASTM C 1168 : 2001 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 1165 : 2017 Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<inf>2</inf>SO<inf>4</inf> at a Platinum Working Electrode
ASTM C 1168 : 1990 : R1995 : EDT 1 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 852/C852M : 2017 : R2022 Standard Guide for Design Criteria for Plutonium Gloveboxes
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM C 1307 : 2002 Standard Test Method for Plutonium Assay by Plutonium (III) Diode Array Spectrophotometry
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM C 1432 : 1999 Standard Test Method for Determination of Impurities in Plutonium: Acid Dissolution, Ion Exchange Matrix Separation, and Inductively Coupled Plasma-Atomic Emission Spectroscopic (ICP/AES) Analysis
ASTM C 1009 : 2021 Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry
ASTM C 852/C852M : 2017 Standard Guide for Design Criteria for Plutonium Gloveboxes
ASTM C 1128 : 2001 : R2008 Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
ASTM C 1415 : 2018 Standard Test Method for <sup>238</sup>Pu Isotopic Abundance By Alpha Spectrometry
ASTM C 1009 : 2013 Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM C 1156 : 2003 Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
ASTM C 1009 : 2006 Standard Guide for Establishing a Quality Assurance Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM C 1297 : 2018 Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
ASTM C 1168 : 2008 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis

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