ASTM D 1646 : 2000
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
Standard Test Methods for Rubber-Viscosity, Stress Relaxation, and Pre-Vulcanization Characteristics (Mooney Viscometer)
Hardcopy , PDF
11-11-2014
English
10-11-2000
Committee |
D 11
|
DocumentType |
Test Method
|
Pages |
12
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy | |
Supersedes |
1.1 These test methods describe procedures for measuring a property called Mooney viscosity. Mooney viscosity is defined as the shearing torque resisting rotation of a cylindrical metal disk (or rotor) embedded in rubber within a cylindrical cavity. The dimensions of the shearing disk viscometer, test temperatures, and procedures for determining Mooney viscosity are defined in these test methods.
1.2 When disk rotation is abruptly stopped, the torque or stress on the rotor decreases at some rate depending on the rubber being tested and the temperature of the test. This is called 'stress relaxation' and these test methods describe a test method for measuring this relaxation.
Note 1--Viscosity as used in these test methods is not a true viscosity and should be interpreted to mean Mooney viscosity, a measure of shearing torque averaged over a range of shearing rates. Stress relaxation is also a function of the test configuration and for these test methods the results are unique to the Mooney viscometer.
1.3 When compounded rubber is placed in the Mooney viscometer at a temperature at which vulcanization may occur, the vulcanization reaction produces an increase in torque. These test methods include procedures for measuring the initial rate of rubber vulcanization.
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.5 ISO Standard 289 Parts 1 and 2 also describes the determination of Mooney viscosity and pre-vulcanization characteristics. In addition to a few insignificant differences there are major technical differences between ISO 289 and this test method in the way samples are prepared on the mill prior to running a Mooney viscosity test. This can result in different viscosity values for some rubbers.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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ASTM D 1417 : 2016 | Standard Test Methods for Rubber Latices—Synthetic |
ASTM D 3191 : 2010 : R2014 | Standard Test Methods for Carbon Black in SBR (Styrene-Butadiene Rubber)—Recipe and Evaluation Procedures |
ASTM D 6204 : 2019 | Standard Test Method for Rubber—Measurement of Unvulcanized Rheological Properties Using Rotorless Shear Rheometers |
ASTM D 1566 : 2019 | Standard Terminology Relating to Rubber |
ASTM D 3958 : 2006 : R2016 | Standard Test Methods for Rubber—Evaluation of BIIR and CIIR (Halogenated Isobutene—Isoprene Rubber) |
ASTM D 3185 : 2006 : R2016 | Standard Test Methods for Rubber—Evaluation of SBR (Styrene-Butadiene Rubber) Including Mixtures With Oil |
ASTM D 3189 : 2006 : R2016 | Standard Test Methods for Rubber—Evaluation of Solution BR (Polybutadiene Rubber) |
ASTM D 3182 : 2016 | Standard Practice for Rubber—Materials, Equipment, and Procedures for Mixing Standard Compounds and Preparing Standard Vulcanized Sheets |
ASTM D 297 : 2015 | Standard Test Methods for Rubber Products—Chemical Analysis |
ASTM D 3346 : 2017 | Standard Test Methods for Rubber Property—Processability of Emulsion SBR (Styrene-Butadiene Rubber) With the Mooney Viscometer (Delta Mooney) |
ASTM D 2227 : 1996 : R2015 | Standard Specification for Natural Rubber (NR) Technical Grades |
ASTM D 6048 : 2007 : R2018 | Standard Practice for Stress Relaxation Testing of Raw Rubber, Unvulcanized Rubber Compounds, and Thermoplastic Elastomers |
ASTM D 3187 : 2006 : R2016 | Standard Test Methods for Rubber—Evaluation of NBR (Acrylonitrile-Butadiene Rubber) |
ASTM D 3484 : 2006 : R2016 | Standard Test Methods for Rubber—Evaluation of Oil-Extended Solution BR (Polybutadiene Rubber) |
ASTM D 5605 : 1994 : R2016 | Standard Practice for Styrene-Butadiene Rubber (SBR)—Establishing Raw Mooney Viscosity Target Values |
ASTM D 3568 : 2003 : R2018 | Standard Test Methods for Rubber—Evaluation of EPDM (Ethylene Propylene Diene Terpolymers) Including Mixtures With Oil |
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