• ASTM D 3326 : 2007 : R2017

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Practice for Preparation of Samples for Identification of Waterborne Oils

    Available format(s):  Hardcopy, PDF

    Superseded date:  26-04-2024

    Language(s):  English

    Published date:  20-12-2017

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    CONTAINED IN VOL. 11.02, 2017 Outlines the preparation for analysis of waterborne oils recovered from water.

    Scope - (Show below) - (Hide below)

    1.1This practice covers the preparation for analysis of waterborne oils recovered from water. The identification is based upon the comparison of physical and chemical characteristics of the waterborne oils with oils from suspect sources. These oils may be of petroleum or vegetable/animal origin, or both. Seven procedures are given as follows:

    Sections

    Procedure A (for samples of more than 50-mL volume containing significant quantities of hydrocarbons with boiling points above 280°C)

    8 to 12

    Procedure B (for samples containing significant quantities of hydrocarbons with boiling points above 280°C)

    13 to 17

    Procedure C (for waterborne oils containing significant amounts of components boiling below 280°C and to mixtures of these and higher boiling components)

    18 to 22

    Procedure D (for samples containing both petroleum and vegetable/animal derived oils)

    23 to 27

    Procedure E (for samples of light crudes and medium distillate fuels)

    28 to 34

    Procedure F (for thin films of oil-on-water)

    35 to 39

    Procedure G (for oil-soaked samples)

    40 to 44

    1.2Procedures for the analytical examination of the waterborne oil samples are described in Practice D3415 and Test Methods D3328, D3414, and D3650. Refer to the individual oil identification test methods for the sample preparation method of choice. The deasphalting effects of the sample preparation method should be considered in selecting the best methods.

    1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific caution statements are given in Sections 6 and 32.

    1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee D 19
    Document Type Standard Practice
    Product Note Reconfirmed 2017
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 3325 : 1990 : R2013 Standard Practice for Preservation of Waterborne Oil Samples
    ASTM D 6469 : 2017 Standard Guide for Microbial Contamination in Fuels and Fuel Systems
    ASTM D 5739 : 2006 : R2013 Standard Practice for Oil Spill Source Identification by Gas Chromatography and Positive Ion Electron Impact Low Resolution Mass Spectrometry
    ASTM D 3328 : 2006 : R2013 Standard Test Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography
    ASTM D 3415 : 1998 : R2017 Standard Practice for Identification of Waterborne Oils
    ASTM D 5412 : 1993 : R2017 : EDT 1 Standard Test Method for Quantification of Complex Polycyclic Aromatic Hydrocarbon Mixtures or Petroleum Oils in Water
    ASTM D 8112 : 2017 Standard Guide for Obtaining In-Service Samples of Turbine Operation Related Lubricating Fluid
    ASTM D 6469 : 2020 Standard Guide for Microbial Contamination in Fuels and Fuel Systems
    ASTM D 8112 : 2024 Standard Guide for Obtaining In-Service Samples of Turbine Operation Related Lubricating Fluid
    ASTM D 8506 : 2023 Standard Guide for Microbial Contamination and Biodeterioration in Turbine Oils and Turbine Oil Systems
    ASTM D 5739 : 2006 : R2020 Standard Practice for Oil Spill Source Identification by Gas Chromatography and Positive Ion Electron Impact Low Resolution Mass Spectrometry

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 3325 : 1990 : R2002 : EDT 1 Standard Practice for Preservation of Waterborne Oil Samples
    ASTM D 3325 : 1990 : R1996 : EDT 1 Standard Practice for Preservation of Waterborne Oil Samples
    ASTM E 1 : 2014 : REDLINE Standard Specification for ASTM Liquid-in-Glass Thermometers
    ASTM D 1129 : 2013 : REDLINE Standard Terminology Relating to Water
    ASTM D 1129 : 2003 Standard Terminology Relating to Water
    ASTM E 133 : 1992 : R2016 Standard Specification for Distillation Equipment
    ASTM D 4489 : 1995 : R2017 Standard Practices for Sampling of Waterborne Oils
    ASTM D 1129 : 2013 Standard Terminology Relating to Water
    ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
    ASTM D 3328 : 2000 Standard Test Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography
    ASTM D 3415 : 1998 : R2004 Standard Practice for Identificaiton of Waterborne Oils
    ASTM D 1129 : 2013 : R2020 : EDT 2 Standard Terminology Relating to Water
    ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
    ASTM D 3325 : 1990 : R2020 Standard Practice for Preservation of Waterborne Oil Samples
    ASTM D 4489 : 1995 : R2011 Standard Practices for Sampling of Waterborne Oils
    ASTM D 3414 : 1998 : R2004 Standard Test Method for Comparison of Waterborne Petroleum Oils by Infrared Spectroscopy
    ASTM D 1129 : 2006 Standard Terminology Relating to Water
    ASTM D 4489 : 1995 : R2006 Standard Practices for Sampling of Waterborne Oils
    ASTM D 3650 : 1993 : R2006 Standard Test Method for Comparison of Waterborne Petroleum Oils By Fluorescence Analysis
    ASTM D 3325 : 1990 : R2006 Standard Practice for Preservation of Waterborne Oil Samples
    ASTM D 4489 : 1995 : R2001 Standard Practices for Sampling of Waterborne Oils
    ASTM D 3415 : 1998 Standard Practice for Identificaiton of Waterborne Oils
    ASTM D 1129 : 2013 : R2020 : EDT 1 Standard Terminology Relating to Water
    ASTM D 4489 : 1995 Standard Practices for Sampling of Waterborne Oils
    ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
    ASTM D 95 : 2013 : R2018 Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
    ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
    ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
    ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
    ASTM D 1129 : 2002 Standard Terminology Relating to Water
    ASTM D 3325 : 1990 : R2013 Standard Practice for Preservation of Waterborne Oil Samples
    ASTM E 133 : 1992 : R2022 Standard Specification for Distillation Equipment
    ASTM D 3414 : 1998 Standard Test Method for Comparison of Waterborne Petroleum Oils by Infrared Spectroscopy
    ASTM D 1193 : 1991 Standard Specification for Reagent Water
    ASTM D 3328 : 2006 Standard Test Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography
    ASTM D 1129 : 2004 Standard Terminology Relating to Water
    ASTM D 3414 : 1998 : R2011 : EDT 1 Standard Test Method for Comparison of Waterborne Petroleum Oils by Infrared Spectroscopy (Withdrawn 2018)
    ASTM D 3328 : 2006 : R2013 Standard Test Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography
    ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
    ASTM E 1 : 2014 : R2020 Standard Specification for ASTM Liquid-in-Glass Thermometers
    ASTM D 3650 : 1993 : R1999 Standard Test Method for Comparison of Waterborne Petroleum Oils By Fluorescence Analysis
    ASTM D 3415 : 1998 : R2017 Standard Practice for Identification of Waterborne Oils
    ASTM D 1193 : 1970 Standard Specification For Reagent Water
    ASTM D 1193 : 2006 Standard Specification for Reagent Water
    ASTM D 1193 : 1999 Standard Specification for Reagent Water
    ASTM D 1129 : 2010 Standard Terminology Relating to Water
    ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
    ASTM D 1129 : 2001 Standard Terminology Relating to Water
    ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water
    ASTM D 3650 : 1993 : R2011 Standard Test Method for Comparison of Waterborne Petroleum Oils By Fluorescence Analysis (Withdrawn 2018)
    ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
    ASTM D 95 : 2023 Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
    ASTM D 3415 : 1998 : R2011 Standard Practice for Identificaiton of Waterborne Oils
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