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ASTM D 4483 : 2005 : REV A
Superseded
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Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
Hardcopy , PDF
11-11-2014
English
01-12-2005
Committee |
D 11
|
DocumentType |
Standard Practice
|
Pages |
60
|
ProductNote |
Reconfirmed EV A
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy | |
Supersedes |
1.1 This practice covers guidelines for evaluating precision and serves as the governing practice for interlaboratory test programs (ITP) used to evaluate precision for test methods as used in the rubber manufacturing and the carbon black industries. This practice uses the basic one way analysis of variance calculation algorithms of Practice E 691. Although bias is not evaluated in this practice, it is an essential concept in understanding precision evaluation.
1.2 This practice applies to test methods that have test results expressed in terms of a quantitative continuous variable. Although exceptions may occur, it is in general limited to test methods that are fully developed and in routine use in a number of laboratories.
1.3 Two precision evaluation methods are given that are described as robust statistical procedures that attempt to eliminate or substantially decrease the influence of outliers. The first is a General Precision procedure intended for all test methods in the rubber manufacturing industry, and the second is a specific variation of the general precision procedure designated as Special Precision, that applies to carbon black testing. Both of these procedures use the same uniform level experimental design and the Mandel h and k statistics to review the precision database for potential outliers. However, they use slight modifications in the procedure for rejecting incompatible data values as outliers. The Special Precision procedure is specific as to the number of replicates per database cell or material-laboratory combination.
1.4 This practice is divided into the following sections:
1.5 Six annexes are presented; these serve as supplements to the main body of this practice. are given mainly as background information that is important for a full understanding of precision evaluation. contain detailed instructions and procedures needed to perform the operations as called for in various parts of the practice. The use of these annexes in this capacity avoids long sections of involved instruction in the main body of this practice. This allows for a better presentation and understanding of the central concepts involved in the evaluation of precision. is also important; it gives a complete example of precision evaluation that illustrates all of the procedures and options likely to be encountered in any precision evaluation, from the simple to the most complex.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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ASTM D 3568 : 2003 : R2018 | Standard Test Methods for Rubber—Evaluation of EPDM (Ethylene Propylene Diene Terpolymers) Including Mixtures With Oil |
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ASTM F 1957 : 1999 : R2017 | Standard Test Method for Composite Foam Hardness-Durometer Hardness |
ASTM D 1414 : 2015 | Standard Test Methods for Rubber O-Rings |
ASTM D 7771 : 2017 : REV A | Standard Test Method for Determination of Benzo-α-Pyrene (BaP) Content in Carbon Black |
ASTM D 1229 : 2003 : R2015 | Standard Test Method for Rubber Property—Compression Set at Low Temperatures |
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ASTM D 395 : 2018 | Standard Test Methods for Rubber Property—Compression Set |
ASTM D 4569 : 2006 : R2017 | Standard Test Method for Rubber Compounding Materials—Determination of Acidity in Sulfur |
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ASTM D 454 : 2004 : R2015 | Standard Test Method for Rubber Deterioration by Heat and Air Pressure |
ASTM D 6556 : 2019 | Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption |
ASTM D 3492 : 2016 | Standard Specification for Rubber Contraceptives (Male Condoms) |
ASTM D 3186 : 2007 : R2016 | Standard Test Methods for Rubber—Evaluation of SBR (Styrene-Butadiene Rubber) Mixed With Carbon Black or Carbon Black and Oil |
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ASTM D 813 : 2007 : R2014 | Standard Test Method for Rubber Deterioration—Crack Growth |
ASTM D 6047 : 2017 | Standard Test Methods for Rubber, Raw—Determination of 5-Ethylidenenorbornene (ENB) or Dicyclopentadiene (DCPD) in Ethylene-Propylene-Diene (EPDM) Terpolymers |
ASTM D 4527 : 2018 | Standard Test Method for Carbon Black—Solvent Extractables |
ASTM D 751 : 2019 | Standard Test Methods for Coated Fabrics |
ASTM D 5099 : 2008 : R2017 | Standard Test Methods for Rubber—Measurement of Processing Properties Using Capillary Rheometry |
ASTM D 5712 : 2015 | Standard Test Method for Analysis of Aqueous Extractable Protein in Latex, Natural Rubber, and Elastomeric Products Using the Modified Lowry Method |
ASTM D 6147 : 1997 : R2014 | Standard Test Method for Vulcanized Rubber and Thermoplastic Elastomer—Determination of Force Decay (Stress Relaxation) in Compression |
ASTM D 1511 : 2012 : R2017 | Standard Test Method for Carbon Black—Pellet Size Distribution |
ASTM D 4573 : 2003 : R2018 | Standard Test Method for Rubber Chemicals—Determination of Oil Content in Oil-Treated Sulfur |
ASTM D 5289 : 2019 | Standard Test Method for Rubber Property—Vulcanization Using Rotorless Cure Meters |
ASTM D 3185 : 2006 : R2016 | Standard Test Methods for Rubber—Evaluation of SBR (Styrene-Butadiene Rubber) Including Mixtures With Oil |
ASTM D 3189 : 2006 : R2016 | Standard Test Methods for Rubber—Evaluation of Solution BR (Polybutadiene Rubber) |
ASTM D 1329 : 2016 | Standard Test Method for Evaluating Rubber Property—Retraction at Lower Temperatures (TR Test) |
ASTM D 1509 : 2018 | Standard Test Methods for Carbon Black—Heating Loss |
ASTM D 4004 : 2006 : R2017 | Standard Test Methods for Rubber—Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis |
ASTM D 991 : 1989 : R2014 | Standard Test Method for Rubber Property—Volume Resistivity Of Electrically Conductive and Antistatic Products |
ASTM D 5670 : 1995 : R2019 | Standard Test Method for Rubber—Determination of Residual Unsaturation in Hydrogenated Nitrile Rubber (HNBR) by Infrared Spectrophotometry |
ASTM D 3190 : 2006 : R2016 | Standard Test Method for Rubber—Evaluation of Chloroprene Rubber (CR) |
ASTM D 3403 : 2007 : R2016 | Standard Test Methods for Rubber—Evaluation of IR (Isoprene Rubber) |
ASTM D 5775 : 1995 : R2019 | Standard Test Method for Rubber—Determination of Bound Styrene in Styrene Butadiene Rubber by Refractive Index |
ASTM D 6746 : 2015 | Standard Test Method for Determination of Green Strength and Stress Relaxation of Raw Rubber or Unvulcanized Compounds |
ASTM D 4075 : 2006 : R2017 | Standard Test Methods for Rubber Compounding Materials—Flame Atomic Absorption Analysis—Determination of Metals |
ASTM D 1512 : 2015 : REV B | Standard Test Methods for Carbon Black—pH Value |
ASTM D 380 : 1994 : R2012 | Standard Test Methods for Rubber Hose |
ASTM D 6049 : 2003 : R2017 | Standard Test Method for Rubber Property—Measurement of the Viscous and Elastic Behavior of Unvulcanized Raw Rubbers and Rubber Compounds by Compression Between Parallel Plates |
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