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ASTM D 4590 : 2018

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Colorimetric Determination of p-tert-Butylcatechol In Styrene Monomer or AMS (α–Methylstyrene) by Spectrophotometry

Available format(s)

Hardcopy , PDF

Superseded date

21-11-2022

Superseded by

ASTM D 4590 : 2022

Language(s)

English

Published date

02-07-2018

€59.22
Excluding VAT

Committee
D 16
DocumentType
Test Method
Pages
4
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method is applicable to the determination of residual 4-tertiary-butylcatechol (TBC) in styrene monomer or AMS in the 1 to 100 mg/kg range. Any other compound producing color at 490 nm when contacted with aqueous sodium hydroxide solution will interfere. It may be compensated for by including it in the preparation of the standard solutions, if its identity and concentration in the sample are known.

1.2In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29. The limit of detection is 0.2 mg/kg while the limit of quantitation is 0.8 mg/kg based on the ILS data in Table 1.

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific statements on hazards, see Section 8.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 6367 : 2021 Standard Specification for AMS (α-Methylstyrene)
ASTM D 2827 : 2019 Standard Specification for Styrene Monomer
ASTM D 6367 : 2017 Standard Specification for AMS (α-Methylstyrene)

ASTM E 29 : 2013 : R2019 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM D 3437 : 1999 Standard Practice for Sampling and Handling Liquid Cyclic Products
ASTM E 29 : 2002 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 3437 : 2015 : R2022 Standard Practice for Sampling and Handling Liquid Cyclic Products
ASTM D 4790 : 1999 Standard Terminology of Aromatic Hydrocarbons and Related Chemicals
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 3437 : 2015 Standard Practice for Sampling and Handling Liquid Cyclic Products
ASTM D 6809 : 2002 Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

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