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ASTM D 4773 : 2002 : R2012

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Standard Test Method for Purity of Propylene Glycol Monomethyl Ether, Dipropylene Glycol Monomethyl Ether, and Propylene Glycol Monomethyl Ether Acetate (Withdrawn 2021)

Available format(s)

Hardcopy , PDF

Withdrawn date

26-01-2021

Language(s)

English

Published date

18-09-2012

€67.30
Excluding VAT

CONTAINED IN VOL. 06.04, 2018 Defines the determination by gas chromatography of propylene glycol monomethyl ether (PM), dipropylene glycol monomethyl ether (DPM), and propylene glycol monomethyl ether acetate (PMA).

Committee
D 01
DocumentType
Test Method
Pages
5
ProductNote
Reconfirmed 2012
PublisherName
American Society for Testing and Materials
Status
Withdrawn
Supersedes

1.1This test method covers the determination by gas chromatography of propylene glycol monomethyl ether (PM), dipropylene glycol monomethyl ether (DPM), and propylene glycol monomethyl ether acetate (PMA).

Note 1Propylene glycol monomethyl ether (PM) is a mixture of two isomers: 1-methoxy-2-propanol and 2-methoxy-1-propanol.
 Dipropylene glycol monomethyl ether (DPM) is a mixture of four isomers: 1-(2-methoxy-1-methylethoxy)-2-propanol is one of the major isomers.
 Propylene glycol monomethyl ether acetate (PMA) is a mixture of two isomers: 1-methoxy-2-acetoxypropane and 2-methoxy-1-acetoxypropane.

1.1.1This test method covers the determination of PM in the range from 98 to 100 %, and DPM in the range from 0.08 to 0.6 %.

1.1.2This test method covers the determination of DPM in the range from 98 to 100 %, PM in the range from 0.05 to 0.3 %, and tripropylene glycol monomethyl ether (TPM) in the range from 0.06 to 0.3 %.

1.1.3This test method covers the determination of PMA in the range from 99 to 100 %, and PM in the range from 0.03 to 1.0 %.

1.2Water and acid cannot be determined by this test method and must be measured in accordance with Test Methods D1364 and D1613, and the results used to normalize the chromatographic data.

1.3The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5For hazard information and guidance, see the supplier's Material Safety Data Sheet.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D 4836 : 2009 : R2017 Standard Specification for Dipropylene Glycol Monomethyl Ether
ASTM D 4835 : 2008 : R2012 Standard Specification for Propylene Glycol Monomethyl Ether Acetate (Withdrawn 2021)
ASTM D 4837 : 2007 : R2012 Standard Specification for Propylene Glycol Monomethyl Ether (Withdrawn 2021)

ASTM D 1613 : 2017 : REDLINE Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
ASTM D 1613 : 1996 : R1999 Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
ASTM D 1613 : 2003 Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
ASTM D 1364 : 2002 Standard Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method)
ASTM D 1613 : 2002 Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
ASTM D 1613 : 2006 Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
ASTM D 1613 : 2006 : R2012 Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
ASTM D 1364 : 2002 : R2012 Standard Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method) (Withdrawn 2021)
ASTM D 1364 : 1995 : R1999 Standard Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method)
ASTM D 1364 : 2002 : R2007 Standard Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method)
ASTM D 1613 : 2017 Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products

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