ASTM D 4874 : 1995 : R2014
Current
The latest, up-to-date edition.
Standard Test Method for Leaching Solid Material in a Column Apparatus (Withdrawn 2021)
Hardcopy , PDF
English
27-05-2014
CONTAINED IN VOL. 11.04, 2015 Defines a procedure for generating aqueous leachate from materials using a column apparatus.
Committee |
D 34
|
DocumentType |
Test Method
|
Pages |
8
|
ProductNote |
Reconfirmed 2014
|
PublisherName |
American Society for Testing and Materials
|
Status |
Current
|
Supersedes |
1.1This test method is a standard laboratory procedure for generating aqueous leachate from materials using a column apparatus. It provides a leachate suitable for organic analysis of semivolatile and nonvolatile compounds as well as inorganic analyses.
1.2The column apparatus is designed and constructed of materials chosen to enhance the leaching of low concentrations of semivolatile and nonvolatile organic constituents as well as to maximize the leaching of metallic species from the solid. Analysis of column effluent provides information on the leaching characteristics of material under the conditions used in the test.
1.3This test method provides for the passage of an aqueous fluid through materials of known mass in a saturated up-flow mode.
1.4It is intended that the sample used in the procedure be physically, chemically, and biologically representative of the material.
1.5This test method does not produce results that can be used as the sole basis for (1) engineering design of a disposal site, or (2) the characterization of wastes based on their leaching characteristics.
1.6This test method has the following limitations:
1.6.1Maximum particle size is 10 mm (0.4 in.). Particle size reduction is not recommended. Large-diameter material (cinders, rocks, and so forth) should be removed prior to packing the column to ensure adequate compaction.
1.6.2Test materials containing densely immiscible organic material may result in phase separation and lead to column plugging.
1.6.3This test method does not differentiate between dissolved constituents and sub-70-μm particulates that pass through the pores of the end plates.
1.6.4This test method is not applicable to the leachability characterization of materials with regard to volatile compounds.
1.6.5This test method is not applicable to the characterization of materials that dissolve in water to a degree that significantly impacts the void volume in the column or the determination of the specific gravity of the material.
1.7Application of this test method to materials with initial low permeability, or to those that lose permeability over the course of the test, may result in long testing periods.
1.8The values stated in SI units are to be regarded as the standard. The values given in parentheses are in approximate inch-pound equivalents.
1.9This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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