1.1This test method covers a method for the measurement of particulate matter (dust) concentration in emission gases in the concentrations below 20 mg/m3 standard conditions, with special emphasis around 5 mg/m3.
1.2To meet the requirements of this test method, the particulate sample is weighed to a specified level of accuracy. At low dust concentrations, this is achieved by:
1.2.1Precise and repeatable weighing procedures,
1.2.2Using low tare weight weighing dishes,
1.2.3Extending the sampling time at conventional sampling rates, or
1.2.4Sampling at higher rates at conventional sampling times (high-volume sampling).
1.3This test method differs from Test Method D3685/D3685M by requiring the mass measurement of filter blanks, specifying weighing procedures, and requiring monitoring of the flue gas flow variability over the testing period. It requires that the particulate matter collected on the sample filter have a mass at least five times a positive mass difference on the filter blank. High volume sampling techniques or an extension of the sampling time may be employed to satisfy this requirement. This test method has tightened requirements on sampling temperature fluctuations and isokinetic sampling deviation. This test method has eliminated the in-stack filtration technique.
1.4This test method may be used for calibration of automated monitoring systems (AMS). If the emission gas contains unstable, reactive, or semi-volatile substances, the measurement will depend on the filtration temperature.
1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.