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ASTM D 6438 : 2005 : R2015

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Acetone, Methyl Acetate, and Parachlorobenzotrifluoride Content of Paints, and Coatings by Solid Phase Microextraction-Gas Chromatography

Available format(s)

Hardcopy , PDF

Superseded date

07-07-2022

Language(s)

English

Published date

12-06-2015

€59.22
Excluding VAT

CONTAINED IN VOL. 06.01, 2017 Defines the determination of acetone, methyl acetate, or parachlorobenzotrifluoride (PCBTF), or combination of any of the three, in paints and coatings, by solid phase microextraction (SPME) headspace sampling, and subsequent injection into a gas chromatograph.

Committee
D 01
DocumentType
Test Method
Pages
4
ProductNote
Reconfirmed 2015
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method is for the determination of acetone, methyl acetate, or parachlorobenzotrifluoride (PCBTF), or combination of any of the three, in paints and coatings, by solid phase microextraction (SPME) headspace sampling, and subsequent injection into a gas chromatograph. It has been evaluated for cellulose nitrate, acrylic, and urethane solvent-borne systems. The established working range of this test method is: acetone, 28 to 90 %; methyl acetate, 12 to 22 %; parachlorobenzotrifluoride, 10 to 17 %. There is no reason to believe that it will not work outside these ranges. A minor modification of this test method would make it suitable for the analysis of the same analytes in water-borne coatings (see Note 1).

Note 1:Water-borne paints are internally standardized and diluted with water followed by addition of solid sodium chloride.

1.2The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D 6133 : 2002 : R2014 Standard Test Method for Acetone, <i>p</i>-Chlorobenzotrifluoride, Methyl Acetate or <i>t</i>-Butyl Acetate Content of Solventborne and Waterborne Paints, Coatings, Resins, and Raw Materials by Direct Injection Into a Gas Chromatograph
ASTM D 7270 : 2007 : R2021 Standard Guide for Environmental and Performance Verification of Factory-Applied Liquid Coatings
ASTM D 6133 : 2002 : R2021 Standard Test Method for Acetone, <emph type="ital">p</emph>-Chlorobenzotrifluoride, Methyl Acetate or <emph type="ital">t</emph>-Butyl Acetate Content of Solventborne and Waterborne Paints, Coatings, Resins, and Raw Materials by Direct Injection Into a Gas Chromatograph
ASTM D 3960 : 2005 : R2018 Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings
ASTM D 7270 : 2007 : R2013 Standard Guide for Environmental and Performance Verification of Factory-Applied Liquid Coatings

ASTM D 3925 : 1981 : R1985 Standard Practice for Sampling Liquid and Related Pigmented Coatings
ASTM D 3925 : 1991 : R1996 Standard Practice for Sampling Liquid Paints and Related Pigmented Coatings
ASTM D 6133 : 2002 : R2014 Standard Test Method for Acetone, <i>p</i>-Chlorobenzotrifluoride, Methyl Acetate or <i>t</i>-Butyl Acetate Content of Solventborne and Waterborne Paints, Coatings, Resins, and Raw Materials by Direct Injection Into a Gas Chromatograph
ASTM D 6133:2002 Standard Test Method for Acetone, <i>p</i>-Chlorobenzotrifluoride, Methyl Acetate or <i>t</i>-Butyl Acetate Content of Solventborne and Waterborne Paints, Coatings, Resins, and Raw Materials by Direct Injection Into a Gas Chromatograph
ASTM E 180 : 2003 Standard Practice for Determining the Precision of ASTM Methods for Analysis and Testing of Industrial and Specialty Chemicals (Withdrawn 2009)
ASTM D 6133 : 2002 : R2021 Standard Test Method for Acetone, <emph type="ital">p</emph>-Chlorobenzotrifluoride, Methyl Acetate or <emph type="ital">t</emph>-Butyl Acetate Content of Solventborne and Waterborne Paints, Coatings, Resins, and Raw Materials by Direct Injection Into a Gas Chromatograph
ASTM D 6133 : 2002 : R2008 Standard Test Method for Acetone, <i>p</i>-Chlorobenzotrifluoride, Methyl Acetate or <i>t</i>-Butyl Acetate Content of Solventborne and Waterborne Paints, Coatings, Resins, and Raw Materials by Direct Injection Into a Gas Chromatograph
ASTM D 6133 : 2000 Test Method for Acetone, <i>p</i>-Chlorobenzotrifluoride, Methyl Acetate or <i>t</i>-Butyl Acetate Content of Solvent-Reducible and Water-Reducible Paints, Coatings, Resins, and Raw Materials by Direct Injection Into a Gas Chromatograph
ASTM D 3925 : 2002 Standard Practice for Sampling Liquid Paints and Related Pigmented Coatings
ASTM D 3925 : 2002 : R2015 Standard Practice for Sampling Liquid Paints and Related Pigmented Coatings
ASTM D 3925 : 2002 : R2010 Standard Practice for Sampling Liquid Paints and Related Pigmented Coatings

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