ASTM D 7417 : 2017 : REDLINE
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Analysis of In-Service Lubricants Using Particular Four-Part Integrated Tester (Atomic Emission Spectroscopy, Infrared Spectroscopy, Viscosity, and Laser Particle Counter)
19-07-2024
English
01-10-2017
Important note : Users cannot be edited or removed once added to your Multi user PDF.CONTAINED IN VOL. 05.05, 2017 Describes the quantitative analysis of in-service lubricants using an automatic testing device that integrates these varied technologies: atomic emission spectroscopy, infrared spectroscopy, viscosity, and particle counting.
| Committee |
D 02
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| DocumentType |
Redline
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| Pages |
9
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| PublisherName |
American Society for Testing and Materials
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| Status |
Superseded
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| SupersededBy |
1.1This test method covers the quantitative analysis of in-service lubricants using an automatic testing device that integrates these varied technologies: atomic emission spectroscopy, infrared spectroscopy, viscosity, and particle counting.
1.2This is suited for in-service lubricating oils having viscosities in the range between ISO 10 and ISO 320 and properties in the ranges given in Tables 1 and 2.
TABLE 1 Element Test Parameters Measured, Calculated, and Reported
| Element | Low Range, mg/kg | High Range, mg/kg | Element | Low Range, mg/kg | High Range, mg/kg |
| Aluminum | 5 to 100 | NA | Molybdenum | 10 to 1000 | NA |
| Barium | 25 to 150 | 150 to 2000 | Nickel | 5 to 100 | NA |
| Boron | 5 to 100 | 100 to 1000 | Phosphorous | 100 to 600 | 600 to 4000 |
| Calcium | 25 to 500 | 500 to 9000 | Potassium | 10 to 1000 | 1000 to 4000 |
| Chromium | 8 to 100 | NA | Silicon | 5 to 150 | 150 to 3000 |
| Copper | 5 to 500 | 500 to 1000 | Sodium | 10 to 1000 | NA |
| Iron | 6 to 1000 | 1000 to 3000 | Tin | 6 to 100 | NA |
| Lead | 6 to 150 | NA | Titanium | 8 to 100 | NA |
| Magnesium | 5 to 100 | 100 to 3000 | Vanadium | 7 to 100 | NA |
| Manganese | 5 to 100 | NA | Zinc | 8 to 100 | 100 to 4000 |
TABLE 2 Physical Properties Parameters Measured, Calculated, and Reported
Note 1:Review Test Method D4739 and D2896 for particular lubricating oil applications.
| Physical Property | Range |
| Water, % by mass | 0.1 to 3 |
| Glycol, % by mass | 0.1 to 2 |
| Soot, % by mass | 0.1 to 4 |
| Fuel Dilution, % by mass | 0.1 to 15 |
| Oxidation, abs. | 0.1 to 50 |
| Nitration, abs. | 0.1 to 35 |
| Calculated Viscosity - IR | 4 to 35 (100° cSt) |
| Viscosity 40 °C, cSt (optional) | 30 to 320 |
| Viscosity 100 °C, cSt (optional) | 5 to 25 |
| Viscosity Index | 5 to 150 |
| Base Number, mg/g KOH | 1.0 to 17 |
1.3This test method may be used to establish trends in wear and contamination of in-service lubricants and may not give equivalent numerical results to current ASTM test methods.
1.4This test method is not intended for use with crude oil.
1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Specific hazard statements are given in Section 9 and 11.3.)
1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
| ASTM D 6595 : 2017 : REDLINE | Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry |
| ASTM D 2896 : 2015 : REDLINE | Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration |
| ISO 11171:2016 | Hydraulic fluid power Calibration of automatic particle counters for liquids |
| ASTM E 2412 : 2010 | Standard Practice for Condition Monitoring of Used Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry |
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