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ASTM D 7528 : 2017 : REV A

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Bench Oxidation of Engine Oils by ROBO Apparatus

Available format(s)

Hardcopy , PDF

Superseded date

11-01-2021

Superseded by

ASTM D 7528 : 2021

Language(s)

English

Published date

17-10-2017

€96.91
Excluding VAT

Committee
D 02
DocumentType
Test Method
Pages
23
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method describes a bench procedure to simulate the oil aging encountered in Test Method D7320, the Sequence IIIG engine test method. These aged oils are then tested for kinematic viscosity and for low-temperature pumpability properties as described in the Sequence IIIGA engine test, Appendix X1 of Test Method D7320.

1.2Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.2.1Exceptions—There are no SI equivalents for some apparatus in Section 6, and there are some figures where inch units are to be regarded as standard.

1.3This test method is arranged as follows:

Section

Scope

1

Reference Documents

2

Terminology

3

Summary of Test Method

4

Significance and Use

5

Apparatus

6

Reagents and Materials

7

Hazards

8

New and Existing Test Stand Calibration

9

Procedure

10

Cleaning

11

Calculations and Determination of Test Results

12

Report

13

Precision and Bias

14

Keywords

15

Annexes

ASTM Test Monitoring Center: Organization

Annex A1

ASTM Test Monitoring Center: Calibration Procedures

Annex A2

ASTM Test Monitoring Center: Maintenance Activities

Annex A3

ASTM Test Monitoring Center: Related Information

Annex A4

Reaction Vessel

Annex A5

Reaction Vessel Head

Annex A6

Reaction Vessel-to-Head Seal

Annex A7

Agitator Turbine Blade

Annex A8

Agitator Packing Gland

Annex A9

Nitrogen Dioxide Graduated Tube

Annex A10

Vacuum System Plumbing

Annex A11

Vacuum Trap Condensers

Annex A12

Setting the Vacuum Control Valve

Annex A13

Appendixes

Sample Preparation and Addition

Appendix X1

Charging the Liquid Nitrogen Dioxide

Appendix X2

Nitrogen Dioxide Precision Needle Valve

Appendix X3

Example of an Assembled ROBO Apparatus

Appendix X4

Information Package to Aid Setting Up a New Robo Apparatus

Appendix X5

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Sections 7 and 8.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 4175 : 2020 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 7320 : 2011 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4175 : 2014 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2003 : REV A Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2009 : REV A : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4684 : 2002 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 4175 : 2008 : REV B : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2006 Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2005 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2011 : REV C Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 4175 : 2005 : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2001 Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2015 : REV C Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2017 : REV A : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4485 : 2003 Standard Specification for Performance of Engine Oils
ASTM D 4485 : 2008 Standard Specification for Performance of Engine Oils
ASTM D 4485 : 2015 Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 4485 : 2005 : REV A Standard Specification for Performance of Engine Oils
ASTM D 4684 : 2008 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 4175 : 2008 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2020 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4684 : 2020 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 4175 : 2017 : REV B Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2009 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2011 : REV A Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 5293 : 2010 : EDT 1 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between <span class='unicode'>–</span>5 and <span class='unicode'>–</span>35<span class='unicode'>°</span>C Using Cold-Cranking Simulator
ASTM D 7320 : 2014 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4485 : 2018 Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 5293 : 2020 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
ASTM D 4175 : 2009 : REV A : EDT 4 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2009 : REV A : EDT 3 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2011 : REV B Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 4684 : 2007 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 4485 : 2016 Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 4175 : 2018 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4485 : 2007 Standard Specification for Performance of Engine Oils
ASTM D 4485 : 2010 Standard Specification for Performance of Engine Oils
ASTM D 4485 : 2001 : REV A Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2001 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4684 : 2017 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 4175 : 2001 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2005 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2002 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 7320 : 2015 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4485 : 2004 Standard Specification for Performance of Engine Oils
ASTM D 5293 : 2014 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –5°C and –35°C Using Cold-Cranking Simulator
ASTM D 7320 : 2016 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4684 : 2012 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 7320 : 2015 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4175 : 2015 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2000 Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2002 : REV A : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 5293 : 2008 : EDT 1 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
ASTM D 4485 : 2015 : REV A Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 7320 : 2007 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 5293 : 2017 : REV A Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
ASTM D 4684 : 2014 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 4175 : 2009 : REV A : EDT 5 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2016 : REV C Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2015 : REV B Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 7320 : 2011 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 7320 : 2006 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 7320 : 2017 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4175 : 2015 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2006 : REV A Standard Specification for Performance of Engine Oils
ASTM D 4684 : 2002 : REV A Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 4175 : 2009 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2016 : REV B Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2002 : REV A : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2008 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 5293 : 2009 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
ASTM D 4175 : 2002 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2000 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2016 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4684 : 2007 : EDT 1 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 4684 : 1999 : EDT 1 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 4175 : 2019 : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 7320 : 2009 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4485 : 2018 : REV A Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 7320 : 2013 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 5293 : 1999 : REV A : EDT 1 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35<sup>o</sup>C Using the Cold-Cranking Simulator
ASTM D 4485 : 2005 Standard Specification for Performance of Engine Oils
ASTM D 4684 : 2017 : REV A Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 7320 : 2008 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 5293 : 2017 : EDT 1 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
ASTM D 4485 : 2014 Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 4485 : 2002 Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2017 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 7320 : 2018 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4485 : 2005 : EDT 1 Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2009 : REV A : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 7320 : 2017 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4175 : 2018 : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4175 : 2016 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 5293 : 2004 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
ASTM D 5293 : 2015 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
ASTM D 4684 : 2018 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature
ASTM D 5293 : 2008 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
ASTM D 7320 : 2012 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4175 : 2017 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 7320 : 2010 : REV B Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 5293 : 2010 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
ASTM D 7320 : 2016 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 7320 : 2010 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 4175 : 2019 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4485 : 2009 Standard Specification for Performance of Engine Oils
ASTM D 4485 : 2019 Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 4175 : 2015 : REV B : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2010 : REV A Standard Specification for Performance of Engine Oils
ASTM D 5293 : 2017 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
ASTM D 5293 : 2002 Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator
ASTM D 4485 : 2011 Standard Specification for Performance of Engine Oils
ASTM D 4175 : 2008 : REV B Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4485 : 2007 : REV A Standard Specification for Performance of Engine Oils

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