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ASTM D 7994 : 2017

Current

Current

The latest, up-to-date edition.

Standard Test Method for Total Fluorine, Chlorine, and Sulfur in Liquid Petroleum Gas (LPG) by Oxidative Pyrohydrolytic Combustion Followed by Ion Chromatography Detection (Combustion Ion Chromatography-CIC)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2017

€56.53
Excluding VAT

Defines the individual determination of total fluorine, chlorine, and sulfur in liquid petroleum gas (LPG), low molecular weight hydrocarbons, their mixtures, and dimethyl ether (DME) in the range of 1 mg Dkg to 300 mg Dkg fluorine and sulfur and 5 mg Dkg to 300 mg Dkg for chlorine.

Committee
D 02
DocumentType
Test Method
Pages
10
PublisherName
American Society for Testing and Materials
Status
Current

1.1This test method covers the individual determination of total fluorine, chlorine, and sulfur in liquid petroleum gas (LPG), low molecular weight hydrocarbons, their mixtures, and dimethyl ether (DME) in the range of 1 mg/kg to 300 mg/kg fluorine and sulfur and 5 mg/kg to 300 mg/kg for chlorine. This test method is applicable to products described in Specifications D1835 and D7901 and it can be applicable to process streams with similar properties to LPG and other materials such as butylene, propylene, and olefins.

1.2This test method can also be applied to the measurement of the bromine and iodine in samples covered by the scope of this test method, but the precision and bias statement of this test method is not applicable to these halides.

1.3This test method can be applied to sample concentrations outside the scope of this test method through adjustments of sample injection volume or number of injections combusted (or both), adjustment of injection volume to the ion chromatograph, and adjustment of the final dilution volume of the absorbing solution prior to injection to the ion chromatograph. The precision and scope of this test method is not applicable to samples that are outside the scope of the method.

1.4The values stated in SI units are to be regarded as standard.

1.4.1Exception—Values given in parentheses are for information only.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 9.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 1835 : 2018 : REV A Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 5273 : 2018 Standard Guide for Analysis of Propylene Concentrates
ASTM D 8149 : 2017 Standard Practice for Optimization, Calibration, and Validation of Ion Chromatographic Determination of Heteroatoms and Anions in Petroleum Products and Lubricants

ASTM D 6849 : 2022 Standard Practice for Storage and Use of Liquefied Petroleum Gases (LPG) in Sample Cylinders for LPG Test Methods
ASTM D 1193 : 2024 Standard Specification for Reagent Water
ASTM E 969 : 2002 : R2024 Standard Specification for Glass Volumetric (Transfer) Pipets
ASTM E 29 : 2013 : R2019 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM D 3700 : 2016 : REDLINE Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM E 29 : 2002 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM D 1265 : 2023 : REV A Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 3700 : 1994 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 6849 : 2013 : R2021 Standard Practice for Storage and Use of Liquefied Petroleum Gases (LPG) in Sample Cylinders for LPG Test Methods
ASTM D 3700 : 2021 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM E 288 : 1994 : R1998 Standard Specification for Laboratory Glass Volumetric Flasks
ASTM D 7901 : 2020 Standard Specification for Dimethyl Ether for Fuel Purposes
ASTM E 969 : 2002 : R2019 Standard Specification for Glass Volumetric (Transfer) Pipets
CFR 29(PT1910.1000 TO END) : 0 LABOR - OCCUPATIONAL SAFETY AND HEALTH ADMINISTRATION, DEPARTMENT OF LABOR
ASTM D 6849 : 2013 Standard Practice for Storage and Use of Liquefied Petroleum Gases (LPG) in Sample Cylinders for LPG Test Methods
ASTM D 1835 : 2022 Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 1265 : 2011 : R2017 : EDT 1 Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 6849 : 2013 : REDLINE Standard Practice for Storage and Use of Liquefied Petroleum Gases (LPG) in Sample Cylinders for LPG Test Methods
ASTM D 3700 : 2016 Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 1265 : 2023 Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 7901 : 2023 Standard Specification for Dimethyl Ether for Fuel Purposes
ASTM D 1265 : 2022 Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

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