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ASTM D 8028 : 2017

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Measurement of Dissolved Gases Methane, Ethane, Ethylene, and Propane by Static Headspace Sampling and Flame Ionization Detection (GC/FID)

Available format(s)

Hardcopy , PDF

Superseded date

20-05-2024

Language(s)

English

Published date

12-12-2017

€74.48
Excluding VAT

Defines the determination of the dissolved gases methane, ethane, ethylene, and propane in drinking, waste, and ground waters, including domestic wells whether naturally occurring or resulting from commercial activities, or both.

Committee
D 19
DocumentType
Test Method
Pages
16
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

1.1This test method covers the determination of the dissolved gases methane, ethane, ethylene, and propane in drinking, waste, and ground waters, including domestic wells whether naturally occurring or resulting from commercial activities, or both. This test method has an analytical range from 10 µg/L to 11 000 µg/L for methane, and 10 µg/L to 5000 µg/L for ethane, ethylene, and propane. If a sample has a dissolved gas concentration above the calibration range, the sample would require dilution. Other analytical ranges may be used as long as the instrument calibration encompasses the desired range and demonstrates adequate linearity.

1.2This test method is applicable to samples collected at a nominal ambient pressure. Samples collected under high pressures, that is, above ambient pressure, may not be accurately analyzed using this method.

1.3This test method is applicable to a variety of dissolved gases; however, for the present standard, only methane, ethane, ethylene, and propane were validated. In order to validate for a gas not listed in this method, the analyst would need to establish the saturation concentration of the new gas, and establish a valid curve, method detection limits, and demonstration of capability following the procedures outlined in this method.

1.4It is the analyst’s responsibility to ensure the validity of this test method for dissolved gases other than methane, ethane, ethylene, and propane and other sample matrices.

1.5Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.

1.6A single laboratory study was done in order to establish precision and bias for the surrogate (see Section 16).

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.8This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 8006 : 2024 Standard Guide for Sampling and Analysis of Residential and Commercial Water Supply Wells in Areas of Exploration and Production (E&P) Operations

ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM D 1129 : 2013 : REDLINE Standard Terminology Relating to Water
ASTM D 1129 : 2003 Standard Terminology Relating to Water
ASTM E 177 : 2014 : REDLINE Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM D 8006 : 2016 Standard Guide for Sampling and Analysis of Residential and Commercial Water Supply Wells in Areas of Exploration and Production (E&P) Operations
ASTM D 1129 : 2013 Standard Terminology Relating to Water
ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
ASTM D 1129 : 2013 : R2020 : EDT 2 Standard Terminology Relating to Water
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 1129 : 2006 Standard Terminology Relating to Water
ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1129 : 2013 : R2020 : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
ASTM D 1129 : 2002 Standard Terminology Relating to Water
ASTM E 355 : 1996 : R2021 : EDT 1 Standard Practice for Gas Chromatography Terms and Relationships
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 1129 : 2004 Standard Terminology Relating to Water
ASTM D 8006 : 2024 Standard Guide for Sampling and Analysis of Residential and Commercial Water Supply Wells in Areas of Exploration and Production (E&P) Operations
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
CFR 40(PTS136-149) : JUL 2017 PROTECTION OF ENVIRONMENT - ENVIRONMENTAL PROTECTION AGENCY
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1129 : 2010 Standard Terminology Relating to Water
ASTM E 355 : 1996 : R2014 Standard Practice for Gas Chromatography Terms and Relationships
ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 2001 Standard Terminology Relating to Water
ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water

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