ASTM E 291 : 2018
Current
The latest, up-to-date edition.
Standard Test Methods for Chemical Analysis of Caustic Soda and Caustic Potash (Sodium Hydroxide and Potassium Hydroxide)
Hardcopy , PDF
English
22-02-2019
These test methods cover only the analyses usually required on the following commercial products Caustic soda (sodium hydroxide), 50 and 73 % liquors; anhydrous (solid, flake, ground, or powdered), and Caustic potash (potassium hydroxide), 45 % liquor; anhydrous (solid, flake, ground, or powdered).
Committee |
D 16
|
DocumentType |
Test Method
|
Pages |
16
|
PublisherName |
American Society for Testing and Materials
|
Status |
Current
|
Supersedes |
1.1These test methods cover only the analyses usually required on the following commercial products:
1.1.1Caustic soda (sodium hydroxide), 50 and 73 % liquors; anhydrous (solid, flake, ground, or powdered), and
1.1.2Caustic potash (potassium hydroxide), 45 % liquor; anhydrous (solid, flake, ground, or powdered).
1.2The analytical procedures appear in the following order:
Alkalinity (Total), Titrimetric (for 50 to 100 % | 3 to 4 |
Carbonate, Gas-Volumetric (0.001 g CO2, min) | 4 to 7 |
Carbonate, Gravimetric (0.001 g CO2, min) | 7 to 10 |
Chloride, Titrimetric, (0.001 g Cl−, min) | 10 to 11 |
Chloride, Potentiometric Titration (0.3 to 1.2 %) | 11 to 12 |
Chloride, Ion Selective Electrode (0.6 to 120 μg/g) | 12 to 13 |
Iron, Photometric (0.005 mg Fe, min) | 13 to 15 |
Sulfate, Gravimetric, (0.002 g SO3, min) | 15 to 16 |
Keywords | 16 |
1.3Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard with the exception of inch-pound units for apparatus descriptions.
1.4In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.
1.5Review the current Safety Data Sheet (SDS) for detailed information concerning toxicity, first-aid procedures, handling, and safety precautions.
1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 6.
1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D 6809 : 2002 : R2016 | Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials |
ASTM D 6809 : 2020 | Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials |
ASTM E 29 : 2013 : R2019 | Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications |
ASTM E 29 : 2002 | Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications |
ASTM D 1193 : 1977 : R1983 : EDT 1 | Standard Specification for Reagent Water |
ASTM E 691 : 2020 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 691 : 2019 : EDT 1 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 60 : 2011 : R2016 | Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry |
ASTM E 691 : 2023 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM D 1193 : 2006 : R2011 | Standard Specification for Reagent Water |
ASTM D 6809 : 2020 : REV A | Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials |
ASTM D 6809 : 2002 : R2012 | Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials |
ASTM E 200 : 2016 | Standard Practice for Preparation, Standardization, and Storage of Standard and Reagent Solutions for Chemical Analysis |
ASTM E 691 : 2022 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 691 : 2009 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM D 1193 : 1991 | Standard Specification for Reagent Water |
ASTM E 200 : 2023 | Standard Practice for Preparation, Standardization, and Storage of Standard and Reagent Solutions for Chemical Analysis |
ASTM E 691 : 2021 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM D 6809 : 2002 | Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials |
ASTM E 60 : 2011 : R2022 : EDT 1 | Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry |
ASTM D 1193 : 1970 | Standard Specification For Reagent Water |
ASTM D 1193 : 2006 | Standard Specification for Reagent Water |
ASTM D 6809 : 2024 | Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials |
ASTM D 1193 : 1999 | Standard Specification for Reagent Water |
ASTM D 6809 : 2002 : R2007 | Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials |
ASTM D 1193 : 2006 : R2018 | Standard Specification for Reagent Water |
ASTM E 29 : 2022 | Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications |
Access your standards online with a subscription
Features
-
Simple online access to standards, technical information and regulations.
-
Critical updates of standards and customisable alerts and notifications.
-
Multi-user online standards collection: secure, flexible and cost effective.