ASTM E 2994 : 2016
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Analysis of Titanium and Titanium Alloys by Spark Atomic Emission Spectrometry and Glow Discharge Atomic Emission Spectrometry (Performance-Based Method)
Hardcopy , PDF
21-01-2022
English
12-05-2016
Important note : Users cannot be edited or removed once added to your Multi user PDF.CONTAINED IN VOL. 03.05, 2016 Specifies the analysis of titanium and its alloys by spark atomic emission spectrometry (Spark-AES) and glow discharge atomic emission spectrometry (GD-AES).
| Committee |
E 01
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| DocumentType |
Test Method
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| Pages |
15
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| PublisherName |
American Society for Testing and Materials
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| Status |
Superseded
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| SupersededBy |
1.1This test method describes the analysis of titanium and its alloys by spark atomic emission spectrometry (Spark-AES) and glow discharge atomic emission spectrometry (GD-AES). The titanium specimen to be analyzed may be in the form of a disk, casting, foil, sheet, plate, extrusion or some other wrought form or shape. The elements and ranges covered in the scope by spark-AES of this method are listed below.
| Element | Tested Mass Fraction Range (%) |
| Aluminum | 0.008 to 7.0 |
| Chromium | 0.006 to 0.1 |
| Copper | 0.014 to 0.1 |
| Iron | 0.043 to 0.3 |
| Manganese | 0.005 to 0.1 |
| Molybdenum | 0.014 to 0.1 |
| Nickel | 0.006 to 0.1 |
| Silicon | 0.018 to 0.1 |
| Tin | 0.02 to 0.1 |
| Vanadium | 0.015 to 5.0 |
| Zirconium | 0.013 to 0.1 |
1.1.1The elements oxygen, nitrogen, carbon, niobium, boron, yttrium, palladium, and ruthenium, were included in the ILS but the data did not contain the required six laboratories. Precision tables were provided for informational use only.
1.2The elements and ranges covered in the scope by GD-AES of this method are listed below.
| Element | Tested Mass Fraction Range (%) |
| Aluminum | 0.02 to 7.0 |
| Chromium | 0.006 to 0.1 |
| Copper | 0.028 to 0.1 |
| Iron | 0.09 to 0.3 |
| Molybdenum | 0.016 to 0.1 |
| Nickel | 0.006 to 0.1 |
| Silicon | 0.018 to 0.1 |
| Tin | 0.022 to 0.1 |
| Vanadium | 0.054 to 5.0 |
| Zirconium | 0.026 to 0.1 |
1.3The mass fractions given in the above scope tables are the ranges validated through the interlaboratory study. However, it is known that the techniques used in this standard allow the useable range to be extended higher or lower based on individual instrument and laboratory capabilities, and the spectral characteristics of the specific element wavelength being used. Laboratories must provide sufficient evidence of method validation when extending the analytical range as described in Guide E2857 Validating Analytical Methods.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.
| SAE AMS 4966 : 2017 | TITANIUM ALLOY, FORGINGS, 5AL - 2.5SN, ANNEALED, 110 KSI (758 MPA) YIELD STRENGTH |
| SAE AMS4916L | Titanium Alloy Sheet, Strip, and Plate 8Al - 1Mo - 1V Duplex Annealed |
| SAE AMS4992B | Casting, Structural Investment, Titanium Alloy 6Al - 4V Hot Isostatically Pressed |
| SAE AMS4928W | Titanium Alloy Bars, Wire, Forgings, Rings, and Drawn Shapes 6Al - 4V Annealed |
| SAE AMS4905F | Titanium Alloy, Damage-Tolerant Grade Plate 6Al - 4V Beta Annealed |
| SAE AMS4910R | Titanium Alloy, Sheet, Strip, and Plate 5Al - 2.5Sn Annealed |
| SAE AMS4975N | Titanium Alloy, Bars, Wire, and Rings 6.0Al - 2.0Sn - 4.0Zr - 2.0Mo - 0.08Si Solution and Precipitation Heat Treated |
| SAE AMS6946C | Titanium Alloy, Sheet, Strip, and Plate 4Al - 2.5V - 1.5Fe Annealed |
| SAE AMS4959G | Titanium Alloy Wire 13.5V - 11Cr - 3Al Spring Temper |
| ASTM B 1009 : 2018 | Standard Specification for Titanium Alloy Bars for Near Surface Mounts in Civil Structures |
| SAE AMS4909K | Titanium Alloy, Sheet, Strip, and Plate 5Al - 2.5Sn, Extra Low Interstitial Annealed |
| SAE AMS4951J | Titanium Welding Wire Commercially Pure Environment Controlled Packaging |
| SAE AMS 6953 : 2018 | TITANIUM ALLOY SHEET, 6AL - 4SN - 3NB - 0.5MO - 0.3SI, DUPLEX ANNEALED |
| SAE AMS4963D | Titanium Alloy, Bars, Wire, Forgings, and Rings 6.0Al - 4.0V Annealed, Heat Treatable, Modified Strength |
| SAE AMS 6952 : 2018 | TITANIUM ALLOY, FORGINGS, 5.8AL - 4.0SN - 3.5ZR - 2.8MO - 0.7NB - 0.35SI - 0.06C, SOLUTION AND PRECIPITATION HEAT TREATED |
| SAE AMS2380G | Approval and Control of Premium-Quality Titanium Alloys |
| SAE AMS4981H | Titanium Alloy Bars, Wire, and Forgings 6.0Al - 2.0Sn - 4.0Zr - 6.0Mo Solution and Precipitation Heat Treated |
| SAE AMS4935L | Titanium Alloy Extrusions and Flash Welded Rings 6Al - 4V Annealed Beta Processed |
| SAE AMS4911P | Titanium Alloy, Sheet, Strip, and Plate 6Al - 4V Annealed |
| SAE AMS4940C | Titanium Sheet, Strip, and Plate Commercially Pure Annealed, 25.0 ksi (172 MPa) Yield Strength |
| SAE AMS4939C | Titanium Alloy Sheet, Strip, and Plate 3Al - 8V - 6Cr - 4Mo - 4Zr Solution Heat Treated |
| SAE AMS4978H | Titanium Alloy Bars, Wire, Forgings, and Rings 6Al - 6V - 2Sn Annealed |
| SAE AMS4976K | Titanium Alloy, Forgings 6.0Al - 2.0Sn - 4.0Zr - 2.0Mo - 08Si Solution and Precipitation Heat Treated |
| SAE AMS4958E | Titanium Alloy Bars and Rods 3Al - 8V - 6Cr - 4Mo - 4Zr Consumable Electrode Melted Solution Heat Treated and Centerless Ground or Peeled and Polished |
| SAE AMS4917J | Titanium Alloy Sheet, Strip, and Plate 13.5V - 11Cr - 3.0Al Solution Heat Treated |
| SAE AMS6931D | Titanium Alloy Bars, Forgings and Forging Stock 6.0Al - 4.0V Annealed |
| SAE AMS2249H | Chemical Check Analysis Limits Titanium and Titanium Alloys |
| SAE AMS4942G | Titanium Tubing, Seamless Annealed, 40.0 ksi (275 MPa) Yield Strength |
| SAE AMS4993F | Titanium Alloy, Blended Powder Compacts, Sintered 6Al - 4V |
| SAE AMS4979J | Titanium Alloy, Bars, Wire, Forgings, and Rings 6Al - 6V - 2Sn Solution and Precipitation Heat Treated |
| SAE AMS4970K | Titanium Alloy Bars, Wire, and Forgings 7Al - 4Mo Solution and Precipitation Heat Treated |
| SAE AMS6950 | Titanium Alloy Bars, Forgings, and Forging Stock 4Al - 2.5V - 1.5 Fe Single Hearth Melted, Annealed |
| SAE AMS6951 | Titanium Alloy, Sheet 5Al - 4V - 0.75Mo - 0.5Fe Annealed |
| SAE AMS4915M | Titanium Alloy Sheet, Strip, and Plate 8Al - 1V - 1Mo Single Annealed |
| SAE AMS4933F | Titanium Alloy Extrusions and Flash Welded Rings 8Al - 1Mo - 1V Solution Heat Treated and Stabilized |
| SAE AMS4941G | Titanium Tubing, Welded 40 ksi (276 MPa) Yield Strength |
| SAE AMS4954K | Titanium Alloy, Welding Wire 6Al - 4V |
| SAE AMS4967L | Titanium Alloy, Bars, Wire, Forgings, and Rings 6.0Al - 4.0V Annealed, Heat Treatable |
| SAE AMS4971L | Titanium Alloy, Bars, Wire, Forgings, and Rings 6Al - 6V - 2Sn Annealed, Heat Treatable |
| SAE AMS4991E | Titanium Alloy Castings, Investment 6Al - 4V Hot Isostatic Pressed, Anneal Optional |
| SAE AMS2368D | Sampling and Testing of Wrought Titanium Raw Material Except Forgings and Forging Stock |
| SAE AMS4945F | Titanium Alloy Tubing, Seamless, Hydraulic 3Al - 2.5V, Controlled Contractile Strain Ratio Cold Worked, Stress Relieved |
| ASTM B 348/B348M : 2021 | Standard Specification for Titanium and Titanium Alloy Bars and Billets |
| ASTM F 620 : 2020 | Standard Specification for Titanium Alloy Forgings for Surgical Implants in the Alpha Plus Beta Condition |
| ASTM B 863 : 2019 | Standard Specification for Titanium and Titanium Alloy Wire |
| ASTM F 1472 : 2020 : REV A | Standard Specification for Wrought Titanium-6Aluminum-4Vanadium Alloy for Surgical Implant Applications (UNS R56400) |
| ASTM F 2989 : 2021 | Standard Specification for Metal Injection Molded Unalloyed Titanium Components for Surgical Implant Applications |
| ASTM B 861 : 2019 | Standard Specification for Titanium and Titanium Alloy Seamless Pipe |
| ASTM B 862 : 2019 | Standard Specification for Titanium and Titanium Alloy Welded Pipe |
| ASTM B 1009 : 2020 | Standard Specification for Titanium Alloy Bars for Near Surface Mounts in Civil Structures |
| ASTM F 1108 : 2021 | Standard Specification for Titanium-6Aluminum-4Vanadium Alloy Castings for Surgical Implants (UNS R56406) |
| ASTM B 381 : 2021 | Standard Specification for Titanium and Titanium Alloy Forgings |
| ASTM F 3046 : 2021 | Standard Specification for Wrought Titanium-3Aluminum-2.5Vanadium Alloy for Surgical Implant Applications (UNS R56320) |
| ASTM E 177 : 1990 : REV A : R1996 | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
| ASTM E 177 : 2014 : REDLINE | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
| ASTM E 135 : 2021 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 1329 : 2000 : R2005 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis |
| ASTM E 691 : 2020 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 1507 : 1998 : R2003 | Standard Guide for Describing and Specifying the Spectrometer of an Optical Emission Direct-Reading Instrument (Withdrawn 2003) |
| ASTM E 691 : 2019 : EDT 1 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 135 : 2003 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 1601 : 2019 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 1601 : 1998 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 2972 : 2015 | Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials |
| ASTM E 1601 : 2010 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 1329 : 2010 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019) |
| ASTM E 1329 : 2000 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis |
| ASTM E 1601 : 2012 : REDLINE | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 305 : 2013 | Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves |
| ASTM E 691 : 2009 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 135 : 2002 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 305 : 2013 : REDLINE | Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves |
| ASTM E 1601 : 2012 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 2857 : 2011 : R2021 : EDT 1 | Standard Guide for Validating Analytical Methods |
| ASTM E 691 : 2021 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 2857 : 2011 : R2016 | Standard Guide for Validating Analytical Methods |
| ASTM E2972 : 2015(2019) | Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials |
| ASTM E 135 : 2021 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 135 : 2003 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 135 : 2003 : REV C | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 305 : 2021 | Standard Practice for Establishing and Controlling Spark Atomic Emission Spectrochemical Analytical Curves |
| ASTM E 2857 : 2011 | Standard Guide for Validating Analytical Methods |
| ASTM E 1507 : 1998 | Standard Guide for Describing and Specifying the Spectrometer of an Optical Emission Direct-Reading Instrument |
| ASTM E 135 : 2020 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ISO/IEC Guide 98-3:2008 | Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995) |
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