ASTM E 3047 : 2016
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Analysis of Nickel Alloys by Spark Atomic Emission Spectrometry
Hardcopy , PDF
10-12-2022
English
12-05-2016
CONTAINED IN VOL. 03.05, 2016 Specifies the spark atomic emission spectrometric (Spark-AES) analysis of nickel alloys, such as those specified by committee B 02, having chemical compositions.
Committee |
E 01
|
DocumentType |
Test Method
|
Pages |
15
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy |
1.1This method describes the spark atomic emission spectrometric (Spark-AES) analysis of nickel alloys, such as those specified by committee B02, having chemical compositions within the following limits:
Element | Application Range (Mass Fraction, %) |
Aluminum | 0.005-6.00 |
Boron | 0.001-0.10 |
Carbon | 0.005-0.15 |
Chromium | 0.01-33.00 |
Copper | 0.01-35.00 |
Cobalt | 0.01-25.00 |
Iron | 0.05-55.00 |
Magnesium | 0.001-0.020 |
Manganese | 0.01-1.00 |
Molybdenum | 0.01-35.00 |
Niobium | 0.01-6.0 |
Nickel | 25.00-100.0 |
Phosphorous | 0.001-0.025 |
Silicon | 0.01-1.50 |
Sulfur | 0.0001-0.01 |
Titanium | 0.0001-6.0 |
Tantalum | 0.01-0.15 |
Tin | 0.001-0.020 |
Tungsten | 0.01-5.0 |
Vanadium | 0.0005-1.0 |
Zirconium | 0.01-0.10 |
1.2The following elements may be determined using this method.
Element | Quantification Range (Mass Fraction, %) |
Aluminum | 0.010-1.50 |
Boron | 0.004-0.025 |
Carbon | 0.014-0.15 |
Chromium | 0.09-20.0 |
Cobalt | 0.05-14.00 |
Copper | 0.03-0.6 |
Iron | 0.17-20 |
Magnesium | 0.001-0.03 |
Manganese | 0.04-0.6 |
Molybdenum | 0.07-5.0 |
Niobium | 0.02-5.5 |
Phosphorous | 0.005-0.020 |
Silicon | 0.07-0.6 |
Sulfur | 0.002-0.005 |
Tantalum | 0.025-0.15 |
Tin | 0.001-0.02 |
Titanium | 0.025-3.2 |
Tungsten | 0.02-0.10 |
Vanadium | 0.005-0.25 |
Zirconium | 0.01-0.05 |
1.3This method has been interlaboratory tested for the elements and quantification ranges specified in section 1.2. The ranges in section 1.2 indicate intervals within which results have been demonstrated to be quantitative. It may be possible to extend this method to other elements or different composition ranges provided that a method validation study as described in Guide E2857 is performed and that the results of this study show that the method extension is meeting laboratory data quality objectives. Supplemental data on other elements not included in the scope are found in the supplemental data tables of the Precision and Bias section.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.
SAE AMS 7000 : 2018 | LASER-POWDER BED FUSION (L-PBF) PRODUCED PARTS, NICKEL ALLOY, CORROSION AND HEAT-RESISTANT, 62NI - 21.5CR - 9.0MO - 3.65NB STRESS RELIEVED, HOT ISOSTATIC PRESSED AND SOLUTION ANNEALED |
SAE AMS 7001 : 2018 | NICKEL ALLOY, CORROSION AND HEAT-RESISTANT, POWDER FOR ADDITIVE MANUFACTURING, 62NI - 21.5CR - 9.0MO - 3.65NB |
ASTM E 177 : 1990 : REV A : R1996 | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
ASTM E 177 : 2014 : REDLINE | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
ASTM E 29 : 2013 : R2019 | Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications |
ASTM E 1257 : 2016 | Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis |
ASTM E 2857 : 2021 | Standard Guide for Validating Analytical Methods |
ASTM E 29 : 2002 | Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications |
ASTM E 135 : 2021 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
ASTM E 1257 : 1993 : R1998 : EDT 1 | Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis |
ASTM E 1329 : 2000 : R2005 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis |
ASTM E 691 : 2020 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 691 : 2019 : EDT 1 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 135 : 2003 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
ASTM E 1601 : 2019 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
ASTM E 1601 : 1998 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
ASTM E 2972 : 2015 | Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials |
ASTM E 1601 : 2010 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
ASTM E 1329 : 2010 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019) |
ASTM E 2857 : 2022 | Standard Guide for Validating Analytical Methods |
ASTM E 691 : 2022 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 1329 : 2000 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis |
ASTM E 1601 : 2012 : REDLINE | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
ASTM E 305 : 2013 | Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves |
ASTM E 691 : 2009 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 135 : 2002 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
ASTM E 305 : 2013 : REDLINE | Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves |
ASTM E 1601 : 2012 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
ASTM E 2857 : 2011 : R2021 : EDT 1 | Standard Guide for Validating Analytical Methods |
ASTM E 1257 : 1993 : R2003 | Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis |
ASTM E 691 : 2021 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 2857 : 2011 : R2016 | Standard Guide for Validating Analytical Methods |
ASTM E2972 : 2015(2019) | Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials |
ASTM E 135 : 2021 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
ASTM E 135 : 2003 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
ASTM E 135 : 2003 : REV C | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
ASTM E 305 : 2021 | Standard Practice for Establishing and Controlling Spark Atomic Emission Spectrochemical Analytical Curves |
ASTM E 2857 : 2011 | Standard Guide for Validating Analytical Methods |
ASTM E 1257 : 1993 : R2008 | Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis |
ASTM E 135 : 2020 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
ISO/IEC Guide 98-3:2008 | Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995) |
ASTM E 29 : 2022 | Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications |
ASTM E 1257 : 2016 : REDLINE | Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis |
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