ASTM E 3047 : 2016

Superseded

Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Analysis of Nickel Alloys by Spark Atomic Emission Spectrometry

Available format(s): Hardcopy, PDF

Superseded date: 10-12-2022

Language(s): English

Published date: 12-05-2016

Publisher: American Society for Testing and Materials

Abstract - (Show below) - (Hide below)

CONTAINED IN VOL. 03.05, 2016 Specifies the spark atomic emission spectrometric (Spark-AES) analysis of nickel alloys, such as those specified by committee B 02, having chemical compositions.

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1.1This method describes the spark atomic emission spectrometric (Spark-AES) analysis of nickel alloys, such as those specified by committee B02, having chemical compositions within the following limits:

Element	Application Range (Mass Fraction, %)
Aluminum	0.005-6.00
Boron	0.001-0.10
Carbon	0.005-0.15
Chromium	0.01-33.00
Copper	0.01-35.00
Cobalt	0.01-25.00
Iron	0.05-55.00
Magnesium	0.001-0.020
Manganese	0.01-1.00
Molybdenum	0.01-35.00
Niobium	0.01-6.0
Nickel	25.00-100.0
Phosphorous	0.001-0.025
Silicon	0.01-1.50
Sulfur	0.0001-0.01
Titanium	0.0001-6.0
Tantalum	0.01-0.15
Tin	0.001-0.020
Tungsten	0.01-5.0
Vanadium	0.0005-1.0
Zirconium	0.01-0.10

1.2The following elements may be determined using this method.

Element	Quantification Range (Mass Fraction, %)
Aluminum	0.010-1.50
Boron	0.004-0.025
Carbon	0.014-0.15
Chromium	0.09-20.0
Cobalt	0.05-14.00
Copper	0.03-0.6
Iron	0.17-20
Magnesium	0.001-0.03
Manganese	0.04-0.6
Molybdenum	0.07-5.0
Niobium	0.02-5.5
Phosphorous	0.005-0.020
Silicon	0.07-0.6
Sulfur	0.002-0.005
Tantalum	0.025-0.15
Tin	0.001-0.02
Titanium	0.025-3.2
Tungsten	0.02-0.10
Vanadium	0.005-0.25
Zirconium	0.01-0.05

1.3This method has been interlaboratory tested for the elements and quantification ranges specified in section 1.2. The ranges in section 1.2 indicate intervals within which results have been demonstrated to be quantitative. It may be possible to extend this method to other elements or different composition ranges provided that a method validation study as described in Guide E2857 is performed and that the results of this study show that the method extension is meeting laboratory data quality objectives. Supplemental data on other elements not included in the scope are found in the supplemental data tables of the Precision and Bias section.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.

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Committee	E 01
Document Type	Test Method
ISBN
Pages
Published
Publisher	American Society for Testing and Materials
Status	Superseded
Superseded By	ASTM E 3047 : 2022

Standards Referenced By This Book - (Show below) - (Hide below)

SAE AMS 7000 : 2018	LASER-POWDER BED FUSION (L-PBF) PRODUCED PARTS, NICKEL ALLOY, CORROSION AND HEAT-RESISTANT, 62NI - 21.5CR - 9.0MO - 3.65NB STRESS RELIEVED, HOT ISOSTATIC PRESSED AND SOLUTION ANNEALED
SAE AMS 7001 : 2018	NICKEL ALLOY, CORROSION AND HEAT-RESISTANT, POWDER FOR ADDITIVE MANUFACTURING, 62NI - 21.5CR - 9.0MO - 3.65NB

Standards Referencing This Book - (Show below) - (Hide below)

ASTM E 177 : 1990 : REV A : R1996	Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM E 177 : 2014 : REDLINE	Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM E 29 : 2013 : R2019	Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 1257 : 2016	Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis
ASTM E 2857 : 2021	Standard Guide for Validating Analytical Methods
ASTM E 29 : 2002	Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 135 : 2021 : REV A	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1257 : 1993 : R1998 : EDT 1	Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis
ASTM E 1329 : 2000 : R2005	Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
ASTM E 691 : 2020	Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2019 : EDT 1	Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 135 : 2003 : REV B	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1601 : 2019	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1601 : 1998	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 2972 : 2015	Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
ASTM E 1601 : 2010	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1329 : 2010	Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019)
ASTM E 2857 : 2022	Standard Guide for Validating Analytical Methods
ASTM E 691 : 2022	Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 1329 : 2000	Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
ASTM E 1601 : 2012 : REDLINE	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 305 : 2013	Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves
ASTM E 691 : 2009	Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 135 : 2002 : REV A	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 305 : 2013 : REDLINE	Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves
ASTM E 1601 : 2012	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 2857 : 2011 : R2021 : EDT 1	Standard Guide for Validating Analytical Methods
ASTM E 1257 : 1993 : R2003	Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis
ASTM E 691 : 2021	Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 2857 : 2011 : R2016	Standard Guide for Validating Analytical Methods
ASTM E2972 : 2015(2019)	Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
ASTM E 135 : 2021	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2003	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2003 : REV C	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 305 : 2021	Standard Practice for Establishing and Controlling Spark Atomic Emission Spectrochemical Analytical Curves
ASTM E 2857 : 2011	Standard Guide for Validating Analytical Methods
ASTM E 1257 : 1993 : R2008	Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis
ASTM E 135 : 2020 : REV B	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ISO/IEC Guide 98-3:2008	Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)
ASTM E 29 : 2022	Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 1257 : 2016 : REDLINE	Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis

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