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ASTM E 3061 : 2017

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Analysis of Aluminum and Aluminum Alloys by Inductively Coupled Plasma Atomic Emission Spectrometry (Performance Based Method)

Available format(s)

Hardcopy , PDF

Superseded date

20-06-2024

Superseded by

ASTM E 3061 : 2024

Language(s)

English

Published date

15-01-2017

€74.48
Excluding VAT

CONTAINED IN VOL. 03.05, 2017 Specifies the inductively coupled plasma atomic emission spectrometric analysis of aluminum and aluminum alloys.

Committee
E 01
DevelopmentNote
Supersedes ASTM E 34. (09/2017)
DocumentType
Test Method
Pages
11
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

1.1This test method describes the inductively coupled plasma atomic emission spectrometric analysis of aluminum and aluminum alloys for the following elements:

Elements

Application Range, %

Minimum

Maximum

Si

0.02

16.8

Fe

0.02

3.06

Cu

0.005

7.0

Mn

0.003

1.41

Mg

0.006

8.2

Cr

0.004

0.52

Ni

0.004

2.71

Zn

0.02

9.65

Ti

0.009

0.20

Ag

0.003

0.4

As

0.005

0.012

B

0.009

0.027

Ba

0.002

0.03

Be

0.002

0.11

Bi

0.01

0.59

Ca

0.003

0.048

Cd

0.002

0.055

Co

0.002

0.034

Ga

0.01

0.019

Li

0.001

2.48

Mo

0.02

0.15

Na

0.008

0.026

P

0.01

0.025

Pb

0.009

0.51

Sb

0.01

0.28

Sc

0.01

0.065

Sn

0.008

6.28

Sr

0.0008

0.028

Ti

0.005

0.20

Tl

0.009

0.13

V

0.01

0.12

Zr

0.004

0.25

1.2This test method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this test method to other elements or different composition ranges if method validation, which includes evaluation of method sensitivity and precision and bias (as described in Section 14), is performed. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials and/or spike recoveries. The user should carefully evaluate the validation data against the laboratory’s data quality objectives. Method validation of scope extensions is also a requirement of ISO/IEC 17025.

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Safety hazard statements are given in Section 10 and specific warning statements are given in Sections 15, 17, 18, 19, 20 and 21.

ASTM B 479 : 2019 Standard Specification for Annealed Aluminum and Aluminum-Alloy Foil for Flexible Barrier, Food Contact, and Other Applications
MIL-DTL-512 Revision C:2001 Aluminum Powder, Flaked, Grained, and Atomized
ASTM B 234M : 2017 Standard Specification for Aluminum and Aluminum-Alloy Drawn Seamless Tubes for Surface Condensers, Evaporators, and Heat Exchangers (Metric)
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SAE AMS4406A Aluminum Alloy, Centrifugal Castings 5.6Zn - 2.5Mg - 1.6Cu - 0.23Cr (709.0-T61) Hot Isostatically Pressed, Solution and Precipitation Heat Treated
SAE AMS4225E Aluminum Alloy, Heat-Resistant, Castings 5.0Cu - 1.5Ni - 0.25Mn - 0.25Sb - 0.25Co - 0.20Ti - 0.20Zr (203.0-T6) Solution Heat Treated and Precipitation Heat Treated
ASTM B 234 : 2017 : REDLINE Standard Specification for Aluminum and Aluminum-Alloy Drawn Seamless Tubes for Surface Condensers, Evaporators, and Heat Exchangers
ASTM B 632/B632M : 2024 Standard Specification for Aluminum-Alloy Rolled Tread Plate
ASTM B 210/B210M : 2019 : REV A Standard Specification for Aluminum and Aluminum-Alloy Drawn Seamless Tubes
ASTM B 247 : 2020 Standard Specification for Aluminum and Aluminum-Alloy Die Forgings, Hand Forgings, and Rolled Ring Forgings
ASTM B 483/B483M : 2021 Standard Specification for Aluminum and Aluminum-Alloy Drawn Tube and Drawn Pipe for General Purpose Applications
ASTM B 373 : 2019 Standard Specification for Aluminum Foil for Capacitors
ASTM B 316/B316M : 2020 Standard Specification for Aluminum and Aluminum-Alloy Rivet and Cold-Heading Wire and Rods
ASTM B 221 : 2021 Standard Specification for Aluminum and Aluminum-Alloy Extruded Bars, Rods, Wire, Profiles, and Tubes
ASTM B 317/B317M : 2023 Standard Specification for Aluminum-Alloy Extruded Bar, Rod, Tube, Pipe, Structural Profiles, and Profiles for Electrical Purposes (Bus Conductor)
ASTM B 236/B236M : 2023 Standard Specification for Aluminum Bars for Electrical Purposes (Bus Bars)
ASTM B 241/B241M : 2022 Standard Specification for Aluminum and Aluminum-Alloy Seamless Pipe and Seamless Extruded Tube
ASTM B 308/B308M : 2020 Standard Specification for Aluminum-Alloy 6061-T6 Standard Structural Profiles
ASTM B 211/B211M : 2023 Standard Specification for Aluminum and Aluminum-Alloy Rolled or Cold Finished Bar, Rod, and Wire
ASTM B 429/B429M : 2020 Standard Specification for Aluminum-Alloy Extruded Structural Pipe and Tube
ASTM B 247M : 2020 Standard Specification for Aluminum and Aluminum-Alloy Die Forgings, Hand Forgings, and Rolled Ring Forgings (Metric)
ASTM B 221M : 2021 Standard Specification for Aluminum and Aluminum-Alloy Extruded Bars, Rods, Wire, Profiles, and Tubes (Metric)

ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM E 1479 : 2016 Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM E 177 : 2014 : REDLINE Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM E 1479 : 1999 : R2005 Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
ASTM E 2857 : 2021 Standard Guide for Validating Analytical Methods
ASTM E 135 : 2023 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 716 : 2016 : R2021 : EDT 2 Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM E 50 : 2017 : REDLINE Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 135 : 2021 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 716 : 2016 : R2021 Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry
ASTM E 1329 : 2000 : R2005 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 1479 : 2016 : REDLINE Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 716 : 2016 Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry
ASTM E 135 : 2003 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM E 135 : 2023 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1452 : 1992 : R1996 Standard Practice for Preparation of Calibration Solutions for Spectrophotometric and for Spectroscopic Atomic Analysis (Withdrawn 2005)
ASTM E 1329 : 2010 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019)
ASTM E 1479 : 1999 : R2011 Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
ASTM E 2857 : 2022 Standard Guide for Validating Analytical Methods
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 1329 : 2000 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 716 : 2016 : REDLINE Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM E 135 : 2002 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2022 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 2857 : 2011 : R2021 : EDT 1 Standard Guide for Validating Analytical Methods
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 2857 : 2011 : R2016 Standard Guide for Validating Analytical Methods
ASTM E 135 : 2022 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2021 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2003 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2003 : REV C Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 716 : 2016 : R2021 : EDT 1 Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM E 2857 : 2011 Standard Guide for Validating Analytical Methods
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM E 135 : 2022 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 50 : 1982 : R1986 Standard Practices for Apparatus, Reagents, and Safety Precautions for Chemical Analysis of Metals
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM E 135 : 2020 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM E 1479 : 2024 Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM E 1479 : 1999 Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
ISO/IEC Guide 98-3:2008 Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)

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