• ASTM F 519 : 2018

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Test Method for Mechanical Hydrogen Embrittlement Evaluation of Plating/Coating Processes and Service Environments

    Available format(s):  Hardcopy, PDF

    Superseded date:  27-02-2024

    Language(s):  English

    Published date:  28-11-2018

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    This test method describes mechanical test methods and defines acceptance criteria for coating and plating processes that can cause hydrogen embrittlement in steels.

    Scope - (Show below) - (Hide below)

    1.1This test method describes mechanical test methods and defines acceptance criteria for coating and plating processes that can cause hydrogen embrittlement in steels. Subsequent exposure to chemicals encountered in service environments, such as fluids, cleaning treatments or maintenance chemicals that come in contact with the plated/coated or bare surface of the steel, can also be evaluated.

    1.2This test method is not intended to measure the relative susceptibility of different steels. The relative susceptibility of different materials to hydrogen embrittlement may be determined in accordance with Test Method F1459 and Test Method F1624.

    1.3This test method specifies the use of air melted SAE 4340 steel (Grade A, see 7.1.1) per SAE AMS 6415 (formerly SAE AMS-S-5000 and formerly MIL-S-5000) or an alternative VAR (Vacuum Arc Remelt) SAE 4340 steel (Grade B, see 7.1.1) per SAE AMS 6414, and both are heat treated to 260 to 280 ksi (pounds per square inch ×1000) as the baseline. This combination of alloy and heat treat level has been used for many years and a large database has been accumulated in the aerospace industry on its specific response to exposure to a wide variety of maintenance chemicals, or electroplated coatings, or both. Components with ultimate strengths higher than 260 to 280 ksi may not be represented by the baseline. In such cases, the cognizant engineering authority shall determine the need for manufacturing specimens from the specific material and heat treat condition of the component. Deviations from the baseline shall be reported as required by 12.1.2. The sensitivity to hydrogen embrittlement shall be demonstrated for each lot of specimens as specified in 9.5.

    Note 1:Extensive testing has shown that VAR 4340 steel may be used as an alternative to the air melted steel with no loss in sensitivity.2

    Note 2:VAR 4340 also meets the requirements in AMS 6415 and could be used as an alternative to air melt steel by the steel suppliers because AMS 6415 does not specify a melting practice.

    1.4Test procedures and acceptance requirements are specified for seven specimens of different sizes, geometries, and loading configurations.

    1.5Pass/Fail Requirements—For plating/coating processes, specimens must meet or exceed 200 h using a sustained load test (SLT) at the levels shown in Table 3.

    1.5.1The loading conditions and pass/fail requirements for service environments are specified in Annex A5.

    1.5.2If approved by the cognizant engineering authority, a quantitative, accelerated ( 24 h) incremental step-load (ISL) test as defined in Annex A3 may be used as an alternative to SLT.

    1.6This test method is divided into two parts. The first part gives general information concerning requirements for hydrogen embrittlement testing. The second is composed of annexes that give specific requirements for the various loading and specimen configurations covered by this test method (see section 9.1 for a list of types) and the details for testing service environments.

    1.7The values stated in the foot-pound-second (fps) system in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.

    1.8This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

    1.9This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee F 07
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM F 3043 : 2015 Standard Specification for “Twist Off” Type Tension Control Structural Bolt/Nut/Washer Assemblies, Alloy Steel, Heat Treated, 200 ksi Minimum Tensile Strength
    ASTM B 733 : 2022 Standard Specification for Autocatalytic (Electroless) Nickel-Phosphorus Coatings on Metal
    ASTM A 1093/A1093M : 2015 : R2020 : EDT 1 Standard Specification for Electrolytic Plasma Treatment Processing of Conductive Materials
    ASTM F 3111 : 2016 Standard Specification for Heavy Hex Structural Bolt/Nut/Washer Assemblies, Alloy Steel, Heat Treated, 200 ksi Minimum Tensile Strength
    ASTM F 326 : 2023 Standard Test Method for Electronic Measurement for Hydrogen Embrittlement From Cadmium-Electroplating Processes
    ASTM B 700 : 2020 Standard Specification for Electrodeposited Coatings of Silver for Engineering Use
    ASTM F 1940 : 2007 : REV A : R2019 Standard Test Method for Process Control Verification to Prevent Hydrogen Embrittlement in Plated or Coated Fasteners
    SAE AMS2411K:2024 Plating, Silver for High Temperature Applications
    ASTM B 699 : 1986 : R2021 : EDT 1 Standard Specification for Coatings of Cadmium Vacuum-Deposited on Iron and Steel
    ASTM B 994/B994M : 2022 Standard Specification for Nickel-Cobalt Alloy Coating
    ASTM B 689 : 1997 : R2023 Standard Specification for Electroplated Engineering Nickel Coatings
    ASTM B 999 : 2015 : R2022 Standard Specification for Titanium and Titanium Alloys Plating, Electrodeposited Coatings of Titanium and Titanium Alloys on Conductive and Non-Conductive Substrate
    ASTM B 177/B177M : 2011 : R2021 Standard Guide for Engineering Chromium Electroplating
    ASTM B 734 : 1997 : R2023 Standard Specification for Electrodeposited Copper for Engineering Uses
    ASTM F 1113 : 1987 : R2017 Standard Test Method for Electrochemical Measurement of Diffusible Hydrogen in Steels (Barnacle Electrode)
    ASTM B 607 : 2021 Standard Specification for Autocatalytic Nickel Boron Coatings for Engineering Use
    ASTM D 6361/D6361M : 1998 : R2020 Standard Guide for Selecting Cleaning Agents and Processes
    ASTM F 1941/F1941M : 2016 Standard Specification for Electrodeposited Coatings on Mechanical Fasteners, Inch and Metric
    ASTM F 2660 : 2020 Standard Test Method for Qualifying Coatings for Use on F3125 Grade A490 Structural Bolts Relative to Environmental Hydrogen Embrittlement
    ASTM B 766 : 2023 Standard Specification for Electrodeposited Coatings of Cadmium

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM B 851 : 1994 Standard Specification for Automated Controlled Shot Peening of Metallic Articles Prior to Nickel, Autocatalytic Nickel, or Chromium Plating, or as Final Finish (Withdrawn 2004)
    ASTM E 8/E8M : 2016 : REV A : EDT 1 Standard Test Methods for Tension Testing of Metallic Materials
    ASTM E 29 : 2013 : R2019 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
    ASTM F 2078 : 2022 Standard Terminology Relating to Hydrogen Embrittlement Testing
    ASTM E 1823 : 2012 : REV : EDT 0 Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 1823 : 2007 : REV A Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM F 1459 : 2006 : R2017 Standard Test Method for Determination of the Susceptibility of Metallic Materials to Hydrogen Gas Embrittlement (HGE)
    ASTM E 1417 : 2005 Standard Practice for Liquid Penetrant Testing
    ASTM F 1624 : 2012 : R2018 Standard Test Method for Measurement of Hydrogen Embrittlement Threshold in Steel by the Incremental Step Loading Technique
    ASTM E 8/E8M : 2021 Standard Test Methods for Tension Testing of Metallic Materials
    ASTM G 38 : 2001 : R2013 Standard Practice for Making and Using C-Ring Stress-Corrosion Test Specimens
    ASTM E 18 : 2022 Standard Test Methods for Rockwell Hardness of Metallic Materials
    ASTM E 709 : 2015 Standard Guide for Magnetic Particle Testing
    ASTM F 2078 : 2015 Standard Terminology Relating to Hydrogen Embrittlement Testing
    ASTM E 1823 : 2009 : REV A Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 29 : 2002 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
    ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
    ASTM F 1624 : 2012 Standard Test Method for Measurement of Hydrogen Embrittlement Threshold in Steel by the Incremental Step Loading Technique
    ASTM E 18 : 2020 Standard Test Methods for Rockwell Hardness of Metallic Materials
    ASTM E 709 : 2021 Standard Guide for Magnetic Particle Testing
    ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM G 5 : 1994 Standard Reference Test Method for Making Potentiostatic and Potentiodynamic Anodic Polarization Measurements
    ASTM E 1417 : 2005 : EDT 1 Standard Practice for Liquid Penetrant Testing
    ASTM F 1459 : 2006 Standard Test Method for Determination of the Susceptibility of Metallic Materials to Hydrogen Gas Embrittlement (HGE)
    ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
    ASTM E 1823 : 2005 : REV A : EDT 1 Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 1823 : 2010 : REV A Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 1823 : 2021 Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 8/E8M : 2022 Standard Test Methods for Tension Testing of Metallic Materials
    ASTM E 1417 : 1999 Standard Practice for Liquid Penetrant Examination
    ASTM E 1823 : 2009 : REV B Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 1823 : 2012 : REV D Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 1823 : 2012 : REV B Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM B 374 : 2006 : R2019 Standard Terminology Relating to Electroplating
    ASTM F 2078 : 2001 Standard Terminology Relating to Hydrogen Embrittlement Testing
    ASTM F 1624 : 2000 Standard Test Method for Measurement of Hydrogen Embrittlement Threshold in Steel by the Incremental Step Loading Technique
    ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 1193 : 1991 Standard Specification for Reagent Water
    ASTM G 5 : 1994 : R1999 Standard Reference Test Method for Making Potentiostatic and Potentiodynamic Anodic Polarization Measurements
    ASTM G 5 : 2014 : EDT 1 Standard Reference Test Method for Making Potentiodynamic Anodic Polarization Measurements
    ASTM E 1444 : 2005 Standard Practice for Magnetic Particle Testing
    ASTM E 1444 : 2001 Standard Practice for Magnetic Particle Examination
    ASTM E 4 : 2021 Standard Practices for Force Calibration and Verification of Testing Machines
    ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM F 1624 : 2006 Standard Test Method for Measurement of Hydrogen Embrittlement Threshold in Steel by the Incremental Step Loading Technique
    ASTM E 1823 : 1996 : R2002 Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 1823 : 1996 : EDT 1 Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 18 : 2019 Standard Test Methods for Rockwell Hardness of Metallic Materials
    ASTM E 1444 : 1994 : REV A Standard Practice for Magnetic Particle Examination
    ASTM E 1823 : 2012 : REV A Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 1823 : 2007 Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM G 38 : 2001 : R2021 Standard Practice for Making and Using C-Ring Stress-Corrosion Test Specimens
    ASTM F 2078 : 2008 : REV A Standard Terminology Relating to Hydrogen Embrittlement Testing
    ASTM F 2078 : 2007 Standard Terminology Relating to Hydrogen Embrittlement Testing
    ASTM G 5 : 2014 : R2021 Standard Reference Test Method for Making Potentiodynamic Anodic Polarization Measurements
    ASTM B 374 : 2021 Standard Terminology Relating to Electroplating
    ASTM D 1193 : 1970 Standard Specification For Reagent Water
    ASTM D 1193 : 2006 Standard Specification for Reagent Water
    ASTM D 1193 : 1999 Standard Specification for Reagent Water
    ASTM E 1823 : 2023 Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM F 1459 : 2006 : R2012 Standard Test Method for Determination of the Susceptibility of Metallic Materials to Hydrogen Gas Embrittlement (HGE)
    ASTM F 1459 : 1993 : R1998 : EDT 1 Standard Test Method for Determination of the Susceptibility of Metallic Materials to Gaseous Hydrogen Embrittlement
    ASTM E 1823 : 2013 Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
    ASTM E 1823 : 2012 : REV C Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 1823 : 2020 : REV B Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 1823 : 2005 : REV A Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM F 1624 : 2009 Standard Test Method for Measurement of Hydrogen Embrittlement Threshold in Steel by the Incremental Step Loading Technique
    ASTM E 1823 : 2011 Standard Terminology Relating to Fatigue and Fracture Testing
    ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
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