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ASTM UOP303 : 2007

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Impurities in Catalysts by ICP-OES

Available format(s)

Hardcopy , PDF

Superseded date

07-01-2020

Superseded by

ASTM UOP303 : 2019

Language(s)

English

Published date

31-05-2007

€74.48
Excluding VAT

Defines trace metals in fresh, regenerated and spent alumina-, silica-, or aluminosilicate- (silica/alumina-) based catalysts by Inductively Coupled Plasma - Optical Emission Spectroscopy (ICP-OES).

DocumentType
Standard
Pages
12
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

This method is for determining trace metal elements in fresh, regenerated and spent alumina-, silica- or silica/alumina-based catalysts by Inductively Coupled Plasma-Atomic Emission Spectroscopy (ICP-AES). Fe, Ni, V, Ca, Mg, Mn, Cr, Sn, Cu, Zn, Ti, Pb, Na, Mo, Co and Si are determined quantitatively on catalysts. Si is not determined when it is a component of the catalyst base. Other elements can be added if required, however, Ba and Hg cannot be determined. In addition, As and P are determined on regenerated or spent alumina-based catalyst. The majority of the specified elements can be determined within the concentration range of 0.005 to 2.0 mass-%. Specific concentration ranges for the elements determined are listed in Table 1.

This method is not applicable to noble metals and modifiers on catalysts. Those elements can be determined by UOP Method 873.

This method cannot be used for determining impurities in alpha-alumina catalyst.

ASTM UOP 873 : 1986 Noble Metals and Modifiers in Catalysts by ICP-AES
ASTM UOP 926 : 1992 Aluminum and Silicon In Fresh Catalysts by Lithium Metaborate Fusion/ICP-AES
ASTM UOP 894 : 1991 Mercury in Catalysts by GF-AAS
ASTM D 4307 : 2017 : REDLINE Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM UOP 954 : 2011 Loss on Ignition (LOI) for Fresh, Regenerated, Used, and Spent Catalysts, Catalyst Supports, and Adsorbents
ASTM U 09 : 2013 Precision Statements in UOP Methods
ASTM UOP 879 : 1987 Aluminum in Catalysts by Atomic Absorption

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