ASTM UOP303 : 2007
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
Impurities in Catalysts by ICP-OES
Hardcopy , PDF
07-01-2020
English
31-05-2007
Defines trace metals in fresh, regenerated and spent alumina-, silica-, or aluminosilicate- (silica/alumina-) based catalysts by Inductively Coupled Plasma - Optical Emission Spectroscopy (ICP-OES).
DocumentType |
Standard
|
Pages |
12
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy |
This method is for determining trace metal elements in fresh, regenerated and spent alumina-, silica- or silica/alumina-based catalysts by Inductively Coupled Plasma-Atomic Emission Spectroscopy (ICP-AES). Fe, Ni, V, Ca, Mg, Mn, Cr, Sn, Cu, Zn, Ti, Pb, Na, Mo, Co and Si are determined quantitatively on catalysts. Si is not determined when it is a component of the catalyst base. Other elements can be added if required, however, Ba and Hg cannot be determined. In addition, As and P are determined on regenerated or spent alumina-based catalyst. The majority of the specified elements can be determined within the concentration range of 0.005 to 2.0 mass-%. Specific concentration ranges for the elements determined are listed in Table 1.
This method is not applicable to noble metals and modifiers on catalysts. Those elements can be determined by UOP Method 873.
This method cannot be used for determining impurities in alpha-alumina catalyst.
ASTM UOP 873 : 1986 | Noble Metals and Modifiers in Catalysts by ICP-AES |
ASTM UOP 926 : 1992 | Aluminum and Silicon In Fresh Catalysts by Lithium Metaborate Fusion/ICP-AES |
ASTM UOP 894 : 1991 | Mercury in Catalysts by GF-AAS |
ASTM D 4307 : 2017 : REDLINE | Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards |
ASTM UOP 954 : 2011 | Loss on Ignition (LOI) for Fresh, Regenerated, Used, and Spent Catalysts, Catalyst Supports, and Adsorbents |
ASTM U 09 : 2013 | Precision Statements in UOP Methods |
ASTM UOP 879 : 1987 | Aluminum in Catalysts by Atomic Absorption |
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