BS EN 62321-3-2:2014
Current
The latest, up-to-date edition.
Determination of certain substances in electrotechnical products Screening. Total bromine in polymers and electronics by Combustion. Ion Chromatography
Hardcopy , PDF
English
31-05-2014
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INTRODUCTION
1 Scope
2 Normative references
3 Terms, definitions and abbreviations
4 Principle
5 Reagents and materials
6 Apparatus
7 Sampling
8 Procedure
9 Calculation
10 Precision
11 Quality assurance and control
12 Test report
Annex A (informative) - Oxygen bomb
combustion-ion chromatography
Annex B (informative) - Oxygen flask
combustion-ion chromatography
Annex C (informative) - Example of a
combustion device and IC system
Annex D (informative) - Results of international
interlaboratory study #4A (IIS 4A)
Annex E (informative) - Additional results of
TG 3-2 test
Annex F (informative) - Additional validation data
Annex G (informative) - Additional IC data
Bibliography
Annex ZA (normative) - Normative references to international
Publications with their corresponding
European publications
Defines the screening analysis of the total bromine (Br) in homogeneous materials found in polymers and electronics by using the analytical technique of combustion ion chromatography (C-IC).
| Committee |
GEL/111
|
| DevelopmentNote |
Supersedes BS EN 62321, which remains current. Supersedes 10/30229134 DC. (05/2014)
|
| DocumentType |
Standard
|
| Pages |
36
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
| Supersedes |
Part 3-2 of IEC 62321 specifies the screening analysis of the total bromine (Br) in homogeneous materials found in polymers and electronics by using the analytical technique of combustion ion chromatography (C-IC). This test method has been evaluated for ABS (acrylonitrile butadiene styrene), EMC (epoxy molding compound), and PE (polyethylene) within the concentration ranges as specified in Table 1. The use of this method for other types of materials or concentration ranges outside those specified below has not been evaluated. Table 1 – Tested concentration ranges for bromine by C-IC in various materials Substance/element Bromine Parameter Unit of measure
mg/kg Medium/material tested ABS EMC PE Concentration or concentration range tested 124 to 890 195 to 976 96 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
| Standards | Relationship |
| EN 62321-3-2:2014 | Identical |
| IEC 62321-3-2:2013 | Identical |
| ISO 5725-1:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions |
| EN 62321-1:2013 | Determination of certain substances in electrotechnical products - Part 1: Introduction and overview |
| ASTM D 808 : 2016 : REDLINE | Standard Test Method for Chlorine in New and Used Petroleum Products (High Pressure Decomposition Device Method) |
| IEC 60754-1:2011 | Test on gases evolved during combustion of materials from cables - Part 1: Determination of the halogen acid gas content |
| EN 14582:2016 | Characterization of waste - Halogen and sulfur content - Oxygen combustion in closed systems and determination methods |
| EN 14346:2006 | Characterization of waste - Calculation of dry matter by determination of dry residue or water content |
| EN 62321-3-1:2014 | Determination of certain substances in electrotechnical products - Part 3-1: Screening - Lead, mercury, cadmium, total chromium and total bromine by X-ray fluorescence spectrometry |
| ISO 10304-1:2007 | Water quality Determination of dissolved anions by liquid chromatography of ions Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate |
| ISO 5667-1:2006 | Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques |
| EN 60754-1:2014 | Test on gases evolved during combustion of materials from cables - Part 1: Determination of the halogen acid gas content |
| IEC 60754-2:2011 | Test on gases evolved during combustion of materials from cables - Part 2: Determination of acidity (by pH measurement) and conductivity |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| ISO 8466-1:1990 | Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function |
| EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
| EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| ISO 6206:1979 | Chemical products for industrial use — Sampling — Vocabulary |
| EN 62321-2:2014 | Determination of certain substances in electrotechnical products - Part 2: Disassembly, disjointment and mechanical sample preparation |
| EN ISO 10304-1:2009 | Water quality - Determination of dissolved anions by liquid chromatography of ions - Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate (ISO 10304-1:2007) |
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