BS ISO 16000-14:2009
Current
The latest, up-to-date edition.
Indoor air Determination of total (gas and particle-phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDDs/PCDFs). Extraction, clean-up and analysis by high-resolution gas chromatography and mass spectrometry
Hardcopy , PDF
English
31-05-2009
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Foreword
Introduction
1 Scope
2 Normative references
3 Terms, definitions and abbreviated terms
4 Principle
5 Apparatus and materials
6 Analysis
7 Minimum requirements for extraction and clean-up
8 Identification and quantification
9 Quality assurance criteria for the procedure blanks
10 Recovery
11 Calculation and presentation of results
12 Safety measures
13 Performance characteristics
14 Interferences
Annex A (informative) - Structure, toxicity and calculation
of toxic equivalents
Annex B (informative) - Example for the clean-up of
PCBs/PCDDs/PCDFs and the separation of PCBs
from PCDDs/PCDFs
Annex C (informative) - GC/MS analysis
Annex D (informative) - Masses of the ions for PCDDs/PCDFs
and PCBs
Annex E (informative) - Interferences
Annex F (normative) Calibration solutions for GC/MS calibration
Annex G (informative) - Standard deviations, detection limits
and indoor air concentrations for PCBs
Bibliography
Defines extraction, clean-up, and analysis procedures for the determination of polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs) collected from indoor air on particle filters backed by polyurethane foam (PUF).
| Committee |
EH/2/5
|
| DevelopmentNote |
Supersedes 07/30146333 DC. (06/2009)
|
| DocumentType |
Standard
|
| Pages |
64
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
| Supersedes |
| Standards | Relationship |
| ISO 16000-14:2009 | Identical |
| ISO 4793:1980 | Laboratory sintered (fritted) filters — Porosity grading, classification and designation |
| CEN/TS 1948-4:2007 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs |
| ISO 16000-13:2008 | Indoor air — Part 13: Determination of total (gas and particle-phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDDs/PCDFs) — Collection on sorbent-backed filters |
| EN 1948-2:2006 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs |
| VDI 3498 Blatt 2:2002-07 | Ambient air measurement - Indoor air measurement - Measurement of polychlorinated dibenzo-p-dioxins and dibenzofurans; Method using small filters |
| ISO 16017-1:2000 | Indoor, ambient and workplace air — Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography — Part 1: Pumped sampling |
| ISO 16017-2:2003 | Indoor, ambient and workplace air — Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography — Part 2: Diffusive sampling |
| EN 1948-3:2006 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs |
| ISO 16000-12:2008 | Indoor air Part 12: Sampling strategy for polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) and polycyclic aromatic hydrocarbons (PAHs) |
| ISO 12219-1:2012 | Interior air of road vehicles Part 1: Whole vehicle test chamber Specification and method for the determination of volatile organic compounds in cabin interiors |
| ISO 9169:2006 | Air quality Definition and determination of performance characteristics of an automatic measuring system |
| VDI 3498 Blatt 1:2002-07 | Ambient air measurement - Indoor air measurement - Measurement of polychlorinated dibenzo-p-dioxins and dibenzofurans; Method using large filters |
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