• BS ISO 16592:2012

    Current The latest, up-to-date edition.

    Microbeam analysis. Electron probe microanalysis. Guidelines for determining the carbon content of steels using a calibration curve method

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  31-08-2012

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Procedure
    3 Evaluation of uncertainty
    4 Test report
    Annex A (informative) - Method of estimating the
            uncertainty of the calculated value using
            a calibration curve
    Annex B (informative) - A practical example of the
            determination of the mass fraction of carbon
            and the evaluation of uncertainty in a steel
    Bibliography

    Abstract - (Show below) - (Hide below)

    Provides guidance on a method for the determination of the carbon content in steels containing other alloying elements (less than 1% to 2% by mass) using the calibration curve method.

    Scope - (Show below) - (Hide below)

    This International Standard gives guidance on a method for the determination of the carbon content in steels containing other alloying elements (less than 1%to 2%by mass) using the calibration curve method. It specifies the sample preparation, X-ray detection, establishment of the calibration curve and the procedure for the determination of the uncertainty of the measured carbon content. It is applicable to steels containing a mass fraction of carbon of less than 1,0%. The method is not applicable to steels with higher carbon contents, which could significantly affect the accuracy of the analysis results.

    This International Standard applies to analyses performed using normal beam incidence and wavelength-dispersive X-ray spectrometry; it is not designed to be used for energy-dispersive X-ray spectrometry.

    General Product Information - (Show below) - (Hide below)

    Committee CII/9
    Development Note Supersedes 05/30118734 DC (10/2006)
    Document Type Standard
    Publisher British Standards Institution
    Status Current
    Supersedes

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
    ISO 5725-6:1994 Accuracy (trueness and precision) of measurement methods and results — Part 6: Use in practice of accuracy values
    ISO 23833:2013 Microbeam analysis — Electron probe microanalysis (EPMA) — Vocabulary
    ISO 14594:2014 Microbeam analysis Electron probe microanalysis Guidelines for the determination of experimental parameters for wavelength dispersive spectroscopy
    ISO 14595:2014 Microbeam analysis — Electron probe microanalysis — Guidelines for the specification of certified reference materials (CRMs)
    ISO 17470:2014 Microbeam analysis — Electron probe microanalysis — Guidelines for qualitative point analysis by wavelength dispersive X-ray spectrometry
    ISO 22309:2011 Microbeam analysis — Quantitative analysis using energy-dispersive spectrometry (EDS) for elements with an atomic number of 11 (Na) or above
    ISO/IEC Guide 98-3:2008 Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)
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