• BS ISO 9924-3:2009

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Rubber and rubber products. Determination of the composition of vulcanizates and uncured compounds by thermogravimetry Hydrocarbon rubbers, halogenated rubbers and polysiloxane rubbers after extraction

    Available format(s):  Hardcopy, PDF

    Superseded date:  05-03-2024

    Language(s):  English

    Published date:  31-10-2009

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Principle
    4 Reagents
    5 Apparatus
    6 Preparation of samples
    7 Procedure
    8 Expression of results
    9 Test report
    10 Precision
    Annex A (informative) - Recommended procedures
    Annex B (informative) - Examples of thermogram
    Annex C (informative) - Precision
    Bibliography

    Abstract - (Show below) - (Hide below)

    Describes a thermogravimetric method for the determination of the main constituents of rubber compounds such as elastomer(s), carbon black and mineral filler.

    Scope - (Show below) - (Hide below)

    This part of ISO9924 specifies a thermogravimetric method for the determination of the main constituents of rubber compounds such as elastomer(s), carbon black and mineral filler.

    It establishes the “fingerprint” of the tested material. However, the result does not always correspond exactly to the theoretical formula of the rubber.

    This method applies to raw or compounded rubbers, vulcanized and unvulcanized, after preliminary extraction.

    This method applies to rubbers with hydrocarbon backbones (NR, BR, SBR, IIR, EPDM, ACM, AEM, etc.) used alone or as mixtures. For the mixtures, the polymer content corresponds to the total rubber, and it is not usually possible to identify individual polymers.

    This method applies to rubbers with halogenated hydrocarbon backbones (CR, CSM, FKM, CM, CO, ECO, etc.) or containing nitrogen (NBR, HNBR, NBR/PVC, etc.), as well as to their mixtures. However, these rubbers often form carbonaceous residues which interfere with the analysis. Application of an appropriate procedure minimizes these interferences.

    This method also applies to rubbers with a polysiloxane backbone (VMQ, etc.) and to rubbers not listed above.

    General Product Information - (Show below) - (Hide below)

    Committee PRI/22
    Development Note Supersedes 07/30161736 DC. (10/2009) Reviewed and confirmed by BSI, August 2014. (07/2014)
    Document Type Standard
    Publisher British Standards Institution
    Status Superseded
    Superseded By
    Supersedes

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 23529:2016 Rubber General procedures for preparing and conditioning test pieces for physical test methods
    ISO 1407:2011 Rubber — Determination of solvent extract
    ISO/TR 9272:2005 Rubber and rubber products Determination of precision for test method standards
    ISO 1629:2013 Rubber and latices — Nomenclature
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