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CEN/TS 14997:2006

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

View Superseded by

Characterization of waste - Leaching behaviour tests - Influence of pH on leaching with continuous pH-control

Withdrawn date

23-10-2024

Superseded by

EN 14997:2015

Published date

29-11-2006

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Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
5 Principle
6 Reagents and laboratory devices
   6.1 Reagents
   6.2 Laboratory devices
7 Sampling
   7.1 Laboratory sample
   7.2 Test sample
   7.3 Determination of dry residue of the sample
   7.4 Test portion
8 Test procedure
   8.1 Contact time
   8.2 pH range
   8.3 Leaching test
   8.4 Natural pH
9 Eluate treatment, storage and analysis
10 Blank tests
11 Performance characteristics
12 Test report
Annex A (informative) Example of a data sheet
Annex B (informative) Operation and uses of the test: influence
                      of pH on the leaching behaviour
Annex C (informative) Preliminary determination of the acid/base
                      consumption
Annex D (informative) Examples of acid and base neutralisation
                      capacities for waste, soil, sediment and
                      construction materials
Bibliography

This document specifies a test method for the determination of the influence of pH on the leachability of inorganic constituents from a waste material. Equilibrium condition as defined in the document is established by continuous adjustment of the pH by addition of acid or base to reach desired pH values. This test method produces eluates, which are subsequently characterized physically and chemically. This document is a parameter specific test as specified in EN 12920. The application of this test method alone is not sufficient for the determination of the detailed leaching behaviour of a waste under specified conditions.NOTEThis generally requires the application of several test methods, behavioural modelling and model validation as specified in EN 12920.

Committee
CEN/TC 292
DocumentType
Technical Specification
PublisherName
Comite Europeen de Normalisation
Status
Withdrawn
SupersededBy

PD CEN/TR 16376:2012 Characterization of waste. Overall guidance document for characterization of waste from the extractive industries
UNI CEN ISO/TS 21268-4 : 2010 SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 4: INFLUENCE OF PH ON LEACHING WITH INITIAL ACID/BASE ADDITION
CEN/TS 15862:2012 Characterisation of waste - Compliance leaching test - One stage batch leaching test for monoliths at fixed liquid to surface area ratio (L/A) for test portions with fixed minimum dimensions
CEN/TR 16376:2012 Characterization of waste - Overall guidance document for characterization of waste from the extractive industries
CEN ISO/TS 21268-4:2009 Soil quality - Leaching procedures for subsequent chemical and ecotoxicological testing of soil and soil materials - Part 4: Influence of pH on leaching with initial acid/base addition (ISO/TS 21268-4:2007)
10/30233988 DC : 0 BS EN 16192 - CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
18/30368510 DC : 0 BS EN ISO 21268-4 - SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 4: INFLUENCE OF PH ON LEACHING WITH INITIAL ACID/BASE ADDITION
PREN 14429 : DRAFT 2013 CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST - INFLUENCE OF PH ON LEACHING WITH INITIAL ACID/BASE ADDITION
S.R. CEN/TR 16376:2012 CHARACTERIZATION OF WASTE - OVERALL GUIDANCE DOCUMENT FOR CHARACTERIZATION OF WASTE FROM THE EXTRACTIVE INDUSTRIES
S.R. CEN/TS 15863:2012 CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERISATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED TEST CONDITIONS
S.R. CEN/TS 15862:2012 CHARACTERISATION OF WASTE - COMPLIANCE LEACHING TEST - ONE STAGE BATCH LEACHING TEST FOR MONOLITHS AT FIXED LIQUID TO SURFACE AREA RATIO (L/A) FOR TEST PORTIONS WITH FIXED MINIMUM DIMENSIONS
BS EN 16192:2011 Characterization of waste. Analysis of eluates
BS EN 15875:2011 Characterisation of waste. Static test for determination of acid potential and neutralisation potential of sulfidic waste
DIN EN 16192:2012-02 Characterization of waste - Analysis of eluates
UNI CEN/TS 15862 : 2012 CHARACTERISATION OF WASTE - COMPLIANCE LEACHING TEST - ONE STAGE BATCH LEACHING TEST FOR MONOLITHS AT FIXED LIQUID TO SURFACE AREA RATIO (L/A) FOR TEST PORTIONS WITH FIXED MINIMUM DIMENSIONS
I.S. EN 15875:2011 CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
DIN EN 15875:2012-11 Characterization of waste - Static test for determination of acid potential and neutralisation potential of sulfidic waste (includes Corrigendum :2012)
12/30263896 DC : 0 BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
UNI EN 15875 : 2011 CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
PD CEN/TS 15862:2012 Characterisation of waste. Compliance leaching test. One stage batch leaching test for monoliths at fixed liquid to surface area ratio (L/A) for test portions with fixed minimum dimensions
PD CEN/TS 15863:2012 Characterisation of waste. Leaching behaviour test for basic characterisation. Dynamic monolithic leaching test with periodic leachant renewal, under fixed test conditions
ISO/TS 21268-4:2007 Soil quality Leaching procedures for subsequent chemical and ecotoxicological testing of soil and soil materials Part 4: Influence of pH on leaching with initial acid/base addition
S.R. CEN ISO TS 21268-4:2009 SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 4: INFLUENCE OF PH ON LEACHING WITH INITIAL ACID/BASE ADDITION
13/30286649 DC : 0 BS EN 14429 - CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST - INFLUENCE OF PH ON LEACHING WITH INITIAL ACID/BASE ADDITION
UNE-EN 15875:2012 Characterization of waste - Static test for determination of acid potential and neutralisation potential of sulfidic waste
08/30189276 DC : 0 BS EN 15875 - CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL OF SULFIDIC WASTE
UNE-EN 16192:2012 Characterization of waste - Analysis of eluates
I.S. EN 16192:2011 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
UNI EN 16192 : 2012 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
EN 16192:2011 Characterization of waste - Analysis of eluates
CEN/TS 15863:2012 Characterisation of waste - Leaching behaviour test for basic characterisation - Dynamic monolithic leaching test with periodic leachant renewal, under fixed test conditions

CEN/TS 14429:2005 Characterization of waste - Leaching behaviour tests - Influence of pH on leaching with initial acid/base addition
EN 14346:2006 Characterization of waste - Calculation of dry matter by determination of dry residue or water content
ISO 5667-3:2012 Water quality Sampling Part 3: Preservation and handling of water samples
EN 13370:2003 Characterization of waste - Analysis of eluates - Determination of Ammonium, AOX, conductivity, Hg, phenol index, TOC, easily liberatable CN-, F-
EN ISO 5667-3:2012 Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN 12920:2006+A1:2008 Characterization of waste - Methodology for the determination of the leaching behaviour of waste under specified conditions
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
EN 12506:2003 Characterization of waste - Analysis of eluates - Determination of pH, As, Ba, Cd, Cl-, Co, Cr, Cr Vl, Cu, Mo, Ni, NO2-, Pb, total S, SO42-, V and Zn
EN 14899:2005 Characterization of waste - Sampling of waste materials - Framework for the preparation and application of a Sampling Plan

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