CEN/TS 16183:2012
Current
The latest, up-to-date edition.
Sludge, treated biowaste and soil - Determination of selected phthalates using capillary gas chromatography with mass spectrometric detection (GC-MS)
22-02-2012
Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling and sample storage
8 Procedure
9 Calibration
10 Calculation
11 Expression of results
12 Precision
13 Test report
Annex A (informative) - Repeatability and reproducibility
data
Annex B (informative) - Example of a reference solution for
multipoint calibration
Annex C (informative) - Examples for gas chromatographic
conditions
Annex D (informative) - Flow scheme of the determination
of phthalates
Bibliography
This Technical Specification specifies a method for the determination of selected phthalates in sludge, treated biowaste and soil, after extraction and gas chromatographic analysis with mass spectrometric detection.The method is applicable for the determination of phthalates (see Table 2) at the lowest mass content of 0,1 mg/kg to 0,5 mg/kg (expressed as dry matter), depending on the individual substance. The applicability of the method to other phthalates not specified in Table 2 is not excluded except the isomeric mixtures e.g. DiNP (Di-isononylphthalate), but shall be verified in each case.
| Committee |
CEN/TC 444
|
| DocumentType |
Technical Specification
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Current
|
| Standards | Relationship |
| DIN CEN/TS 16183;DIN SPEC 91265:2012-05 | Identical |
| UNI CEN/TS 16183 : 2012 | Identical |
| S.R. CEN/TS 16183:2012 | Identical |
| XP CEN/TS 16183 : 2012 XP | Identical |
| 16/30340580 DC : 0 | BS EN 17009 - FLOORING OF LIGNIFIED MATERIALS OTHER THAN WOOD - CHARACTERISTICS, EVALUATION OF CONFORMITY AND MARKING |
| ISO 5667-13:2011 | Water quality Sampling Part 13: Guidance on sampling of sludges |
| PREN 15934 : DRAFT 2009 | SOIL, SLUDGE, WASTE, AND TREATED BIOWASTE - DETERMINATION OF DRY MATTER - GRAVIMETRIC METHOD |
| ISO 22892:2006 | Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| ISO 383:1976 | Laboratory glassware — Interchangeable conical ground joints |
| PREN 16179 : DRAFT 2010 | SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT |
| ISO 10381-2:2002 | Soil quality Sampling Part 2: Guidance on sampling techniques |
| ISO 5667-15:2009 | Water quality — Sampling — Part 15: Guidance on the preservation and handling of sludge and sediment samples |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| EN ISO 5667-13:2011 | Water quality - Sampling - Part 13: Guidance on sampling of sludges (ISO 5667-13:2011) |
| ISO 8466-1:1990 | Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function |
| EN ISO 22892:2011 | Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006) |
| EN ISO 5667-15:2009 | Water quality - Sampling - Part 15: Guidance on the preservation and handling of sludge and sediment samples (ISO 5667-15:2009) |
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