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CR 10320:2004

Current

Current

The latest, up-to-date edition.

Optical emission analysis of low alloy steels (routine method) - Method for determination of C, Si, S, P, Mn, Cr, Ni and Cu

Published date

29-09-2004

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Foreword
1 Scope
2 Test sample preparation
3 Calibration of the instrument
   3.1 Determination of calibration curve
   3.2 Linear correlation
   3.3 Quadratic correlation
   3.4 Confidence limit (Syc) and standard error (Syx) in
       a linear correlation
   3.5 Confidence limit (Syc) and standard error (Syx) in
       a quadratic correlation
   3.6 Correlation accuracy
4 Calculation of interferences
   4.1 Spectral interferences
   4.2 Matrix interferences
   4.3 Calculation of an interfered element due to
       either matrix effect or spectral interference
5 Determination of performance criteria
   5.1 Determination of background equivalent concentration
       BEC
   5.2 Determination of detection limit DL
   5.3 Determination of repeatability as relative
       standard deviation RSD
   5.4 Determination of accuracy SEA
6 Performing analysis
7 Ordinary maintenance
8 Quality control
   8.1 Control chart
   8.2 Calibration curve control
9 Examples
   9.1 Determination of calibration curve
   9.2 Calculation of interferences
   9.3 Determination of background equivalent concentration
   9.4 Determination of detection limit
   9.5 Determination of repeatability
   9.6 Determination of accuracy
   9.7 Ordinary maintenance
   9.8 Control CHART
   9.9 Calibration curve control
10 Statistical results
Annex A Optical emission spectrometry
Bibliography

This document specifies an optical emission spectrometry spark source routine standard method for multi-element analysis of unalloyed steel and iron.

Committee
CEN/TC 459/SC 2
DocumentType
Report
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
NEN NPR CR 10320 : 2004 Identical
I.S. CR 10320:2004 Identical

PD CEN/TR 10261:2013 Iron and steel. European standards for the determination of chemical composition
UNI CEN/TR 10261 : 2008 IRON AND STEEL - REVIEW OF AVAILABLE METHODS OF CHEMICAL ANALYSIS
17/30347067 DC : 0 BS EN 10340-1 - STEEL CASTINGS FOR STRUCTURAL USES - PART 1: GENERAL
CEN/TR 10261:2013 Iron and steel - European standards for the determination of chemical composition

ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
CR 10316:2001 Optical emission analysis of low alloy steels (routine method) - Guidelines for the preparation of standard routine method for optical emission spectrometry

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