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DEFSTAN 03-2/4(2005) : 2005

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

CLEANING AND PREPARATION OF METAL SURFACES

Available format(s)

Hardcopy , PDF

Superseded date

20-11-2009

Language(s)

English

Published date

01-01-2005

€17.53
Excluding VAT

Foreword
Introduction
1 Scope
2 Warning
3 Normative References
4 Definitions
  4.2 Tensile Strength of Steels
       4.2.1 Tensile Strength
       4.2.2 Tensile strength/hardness relationship
  4.3 Process control schedule
5 Information to be Supplied to the Processor
6 Process Control
7 General Requirements
8 Standard Cleaning Methods
Annex A - Steels, Non-Corrosion Resisting, Cast Irons and
          Pure Irons
  A.1 Selection of Method of Cleaning
  A.2 Stress Relieving Heat Treatment
  A.3 General Degreasing and Cleaning
       A.3.1 Steels of specified maximum tensile strength
              up to 1100 MPa
       A.3.2 Steels of specified maximum tensile strength
              in the range 1100 to 1450 MPa
       A.3.3 Steels of specified maximum tensile strength
              over 1450 MPa
  A.4 Preparation for Electroplating
  A.5 Preparation for Electroless Nickel Plating
  A.6 Preparation Prior to Phosphating to Def Stan 03-11
  A.7 Preparation Prior to Sheradising to BS 4921
  A.8 Preparation Prior to Hot Dip Galvanising
       A.8.1 Steel (other than castings)
       A.8.2 Steel castings
  A.9 Preparation Prior to Metal Spraying
       A.9.1 Spraying for protection corrosion
       A.9.2 Spraying for reclamation purposes
  A.10 Preparation Prior to Direct Application of Paint to
       the Bare Metal
Annex B - Steels, Corrosion Resisting
  B.1 Stress Relieving Heat Treatment
  B.2 General Degreasing and Cleaning
  B.3 Preparation Prior to Electroplating
  B.4 Preparation Prior to Electroless Nickel Plating
  B.5 Preparation Prior to Metal Spraying
       B.5.1 Spraying to BS 2569
       B.5.2 Spraying for Reclamation Purposes
  B.6 Preparation Prior to the Direct Application of Paint
       to the Bare Metal
Annex C - Aluminium and Aluminium Alloys
  C.1 General Degreasing and Cleaning
  C.2 Removal of Corrosion Products
  C.3 Preparation Prior to Anodizing
  C.4 Preparation Prior to Process O or Filming Treatments
       to Def Stan 03-18
  C.5 Preparation Prior to Painting
  C.6 Preparation Prior to Adhesive Bonding of Unanodized Items
  C.7 Preparation Prior to Electroplating
  C.8 Preparation Prior to Metal Spraying (Def Stan 03-3)
Annex D - Copper and Copper Alloys
  D.1 General Degreasing and Cleaning
  D.2 Preparation Prior to Electroplating
  D.3 Preparation Prior to Electroless Nickel Plating
  D.4 Preparation Prior to Direct Application of Paint to Bare
       Metal
Annex E - Nickel Alloys
  E.1 General Degreasing and Cleaning
  E.2 Preparation Prior to Electroplating
  E.3 Preparation Prior to Direct Application of Paint to Bare
       Metal
Annex F - Titanium and Titanium Alloys
  F.1 General Degreasing and Cleaning
  F.2 Preparation Prior to Electroplating
  F.3 Preparation Prior to Electroless Nickel Plating
  F.4 Preparation Prior to Direct Application of Paint to Bare
       Metal
Annex G - Magnesium Alloys
  G.1 General Degreasing, Cleaning and Painting
Annex H - Zinc Based Alloys
  H.1 General Degreasing and Cleaning
  H.2 Cleaning of Corroded Items
  H.3 Preparation Prior to Painting
  H.4 Preparation Prior to Electroplating
Annex I - Tungsten Alloys
  I.1 Preparation Prior to Electroplating
  I.2 Preparation Prior to Adhesive Bonding and Painting
Annex J - Cleaning and Preparation Methods
  J.1 Introduction
  J.2 Process A - Organic Solvent Degreasing and Cleaning
  J.3 Process B - Alkaline Degreasing
  J.4 Process C - Acid Emulsion Cleaning
  J.5 Process D - Abrasive Cleaning
  J.6 Process E - Sodium Hydroxide De-Scaling
  J.7 Process F - Acid Pickling Without Electrolysis
  J.8 Process G - Acid Dipping
  J.9 Process H - Anodic Pickling
  J.10 Process J - Acid De-Rusting
  J.11 Process K - Alkaline De-Rusting
  J.12 Process L - Chemical Smoothing Process for Steel
  J.13 Process M - Removal of Surface Contamination from
       Corrosion Resisting Steel (Passivation)
  J.14 Process N - Acid Etching of Aluminium Alloys
  J.15 Process O - Oxide Removal Treatment for Aluminium and
       Aluminium Alloys - Bath Treatment
  J.16 Process P - Etching Treatment of Aluminium and
       Aluminium Alloys
  J.17 Process O - Cleaning Treatment for Copper and Copper
       Alloys
  J.18 Process R - Acid De-Scaling, Etching and Smoothing of
       Copper and Copper Alloys
  J.19 Process S - Pickling of Titanium and Titanium Alloys
  J.20 Process T - Pickling of Nickel Alloys
  J.21 Process U - Removal of Corrosion Products from Aluminium
       Alloys
  J.22 Process V - Preparation of Corrosion-Resisting Steels
       Prior to Electroplating
  J.23 Process W - Preparation of Aluminium Alloys Prior to
       Electroplating
  J.24 Process X - Preparation of Nickel Alloys Prior to
       Electroplating
  J.25 Process Y - Preparation of Titanium Alloys Prior to
       Electroplating
  J.26 Process Z - Preparation of Zinc and Zinc Alloys Prior
       to Electroplating
Appendix W - Maintenance of Organic Solvent and Vapour
             Degreasing Baths
  W.1 General
  W.2 Solvent Baths
  W.3 Vapour and Alkaline Degreasing
Appendix X - The Control of Acidity in Vapour Degreasing Plant
Appendix Y - Method for the Determination of the Rate of Attack
             on Mild Steel
Appendix Z - Pretreatment Solution for Aluminium
  Z.1 General
  Z.2 Description
  Z.3 Composition
  Z.4 Testing
  Z.5 Method for Determining Free Acidity
  Z.6 Method for Settling Test

Covers processes for the cleaning of metal surfaces to remove any extraneous or undesirable material or deposits at any stage of manufacture, storage or service and for the preparation of these surfaces for further treatment.

DevelopmentNote
Supersedes DEFSTAN 03-2/3(1995) (10/2005)
DocumentType
Standard
Pages
62
PublisherName
UK Ministry of Defence Standards
Status
Superseded
SupersededBy
Supersedes

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DEFSTAN 03-4/5(2006) : 2006 THE PRE-TREATMENT AND PROTECTION OF STEEL ITEMS OF MAXIMUM TENSILE STRENGTH EXCEEDING 1450 MPA
DEFSTAN 80-16/4(2006) : 2006 PAINT REMOVER, DICHLOROMETHANE, WATER RINSABLE TYPE - TYPE 1: HIGH VISCOSITY (BRUSHING) TYPE 2: LOW VISCOSITY (SPRAYING)
DEFSTAN 03-29/4(2008) : 2008 PROTECTION OF METALLIC SPRINGS AGAINST CORROSION
DEFSTAN 03-3/4(2008) : 2008 PROTECTION OF ALUMINIUM ALLOYS BY SPRAYED METAL COATINGS
DEFSTAN 00-970(PT0)/7(2011) : 2011 DESIGN AND AIRWORTHINESS REQUIREMENTS FOR SERVICE AIRCRAFT - PART 0: PROCEDURES FOR USE, CONTENT AND DEFINITIONS
DEFSTAN 03-28(PT3)/4(2008) : 2008 PHYSICAL VAPOUR DEPOSITION OF METALS - PART 3: PHYSICAL VAPOUR DEPOSITION OF TITANIUM NITRIDE FOR SURFACE PROTECTION
DEFSTAN 03-28(PT2)/4(2008) : 2008 PHYSICAL VAPOUR DEPOSITION OF METALS - PART 2: PHYSICAL VAPOUR DEPOSITION OF CADMIUM FOR PROTECTION AGAINST CORROSION
DEFSTAN 03-11/5(2008) : 2008 PHOSPHATE TREATMENT OF IRON AND STEEL
DEFSTAN 00-970(PT7)SEC4/2(2007) : 2007 DESIGN AND AIRWORTHINESS REQUIREMENTS FOR SERVICE AIRCRAFT - PART 7: ROTORCRAFT - SECTION 4: DETAIL DESIGN AND STRENGTH OF MATERIALS
DEFSTAN 00-970(PT1)SEC4/5(2007) : 2007 DESIGN AND AIRWORTHINESS REQUIREMENTS FOR SERVICE AIRCRAFT - PART 1: COMBAT AIRCRAFT - SECTION 4: DESIGN AND CONSTRUCTION
DEFSTAN 81-41(PT2)/6(2005) : 2005 PACKAGING OF DEFENCE MATERIEL - PART 2: DESIGN
DEFSTAN 00-970(PT7)SEC4/1(2006) : 2006 DESIGN AND AIRWORTHINESS REQUIREMENTS FOR SERVICE AIRCRAFT - PART 7: ROTORCRAFT - SECTION 4: DETAIL DESIGN AND STRENGTH OF MATERIALS
DEFSTAN 00-970(PT1)SEC4/4(2006) : 2006 DESIGN AND AIRWORTHINESS REQUIREMENTS FOR SERVICE AIRCRAFT - PART 1: COMBAT A/C - SECTION 4: DESIGN AND CONSTRUCTION
DEFSTAN 03-25/5(2008) : 2008 SULFURIC ACID ANODIZING OF ALUMINIUM AND ALUMINIUM ALLOYS
DEFSTAN 80-222/1(2007) : 2007 SURFACE DEGREASING CLEANER FOR AEROSPACE PURPOSES
DEFSTAN 03-27/3(2005) : 2005 ELECTRO-DEPOSITION OF NICKEL FOR ENGINEERING PURPOSES
DEFSTAN 03-28(PT1)/4(2008) : 2008 PHYSICAL VAPOUR DEPOSITION OF METALS - PART 1: PHYSICAL VAPOUR DEPOSITION OF ALUMINIUM FOR PROTECTION AGAINST CORROSION
DEFSTAN 00-970(PT0)/5(2007) : 2007 DESIGN AND AIRWORTHINESS REQUIREMENTS FOR SERVICE AIRCRAFT - PART 0: PROCEDURES FOR USE, CONTENT AND DEFINITIONS
DEFSTAN 03-39/1(2008) : 2008 ELECTRODEPOSITION OF ZINC-COBALT ALLOYS
DEFSTAN 03-21/4(2008) : 2008 MECHANICAL METHODS FOR THE INDUCEMENT OF RESIDUAL SURFACE COMPRESSIVE STRESSES
SBAC TS 24 : 6 MANUFACTURING SPECIFICATION FOR BOLTS, 1275 MPA (185,000 LBF/IN[2]) - TENSILE AT ROOM TEMPERATURE, 1000 MPA (145,000 LBF/IN[2]) TENSILE AT 650 DEGREE C
DEFSTAN 03-17/3(2007) : 2007 ELECTRO-DEPOSITION OF GOLD
DEFSTAN 81-136/2(2009) : 2009 PACKAGING OF METAL PIPES AND PIPE ASSEMBLIES
DEFSTAN 03-43/1(2008) : 2008 THERMAL SPRAYED COATINGS FOR WEAR RESISTANCE
DEFSTAN 03-40/1(2008) : 2008 ELECTRODEPOSITION OF ZINC-NICKEL ALLOYS
DEFSTAN 03-41/1(2008) : 2008 TRIVALENT CHROMIUM PASSIVATION TREATMENTS FOR ELECTRODEPOSITED ZINC-BASE COATINGS
DEFSTAN 03-18/4(2008) : 2008 CHROMATE CONVERSION COATINGS (CHROMATE FILMING TREATMENTS) GRADES: STANDARD AND BRUSHING FOR ALUMINIUM AND ALUMINIUM ALLOYS
DEFSTAN 03-24/5(2008) : 2008 CHROMIC ACID ANODIZING OF ALUMINIUM AND ALUMINIUM ALLOYS

DEFSTAN 08-39/2(2003) : 2003 CUTTING, WELDING AND CORROSION PROTECTION OF ALUMINIUM ALLOY MILITARY EQUIPMENT
BS 4921:1988 Specification for sherardized coatings on iron or steel
BS EN ISO 3696:1995 Water for analytical laboratory use. Specification and test methods
DEFSTAN 03-11/4(2003) : 2003 PHOSPHATE TREATMENT OF IRON AND STEEL
BS EN ISO 6507-1:2005 Metallic materials. Vickers hardness test Test method
DEFSTAN 03-18/3(2003) : 2003 CHROMATE CONVERSION COATINGS (CHROMATE FILMING TREATMENTS) GRADES: STANDARD AND BRUSHING FOR ALUMINIUM AND ALUMINIUM ALLOYS
BS EN ISO 4788:2005 Laboratory glassware. Graduated measuring cylinders
DEFSTAN 03-4/4(1998) : 1998 THE PRE-TREATMENT AND PROTECTION OF STEEL ITEMS OF SPECIFIED MAXIMUM TENSILE STRENGTH EXCEEDING 1450 MPA
BS EN ISO 11124-2:1997 Preparation of steel substrates before application of paints and related products. Specifications for metallic blast-cleaning abrasives Chilled-iron grit
DEFSTAN 68-189/2(2004) : 2004 SOLVENT FOR GREASE, EMULSIFIABLE
BS 5599:1993 Specification for hard anodic oxidation coatings on aluminium and its alloys for engineering purposes
DEFSTAN 68-188/2(2001) : 2001 EMULSIFIER FOR SOLVENT CLEANER
BS EN ISO 4527:2003 Metallic coatings. Autocatalytic (electroless) nickel-phosphorus alloy coatings. Specification and test methods
DEFSTAN 03-27/2(1998) : 1998 ELECTRODEPOSITION OF NICKEL FOR ENGINEERING PURPOSES
DEFSTAN 03-25/4(2003) : 2003 SULFURIC ACID ANODISING OF ALUMINIUM AND ALUMINIUM ALLOYS
BS 4130:1984 Specification for sodium hydroxide (technical grades)
DEFSTAN 03-3/3(2002) : 2002 PROTECTION OF ALUMINIUM ALLOYS BY SPRAYED METAL COATINGS
DEFSTAN 68-160/2(2004) : INTERIM DEGREASING COMPOUND, TYPES A AND C
BS 245:1976 Specification for mineral solvents (white spirit and related hydrocarbon solvents) for paints and other purposes
BS 2X 32:1998 Specification for pre-treatment etch primer for aerospace purposes
BS 6338:1982 Specification for chromate conversion coatings on electroplated zinc and cadmium coatings
DTD 911C : MAR 69 PROTECTION OF MAGNESIUM-RICH ALLOYS AGAINST CORROSION
DEFSTAN 80-15/2(1990) : 1990 PAINT, PRE-TREATMENT PRIMER (ETCHING PRIMER) - TYPES: BRUSHING (BASE AND ACID COMPONENT), SPRAYING (BASE AND ACID COMPONENT)
DEFSTAN 03-24/4(2003) : 2003 CHROMIC ACID ANODIZING OF ALUMINIUM AND ALUMINIUM ALLOYS
BS 2869:1998 Specification for fuel oils for agricultural, domestic and industrial engines and boilers

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