EN 12766-1:2000
Current
The latest, up-to-date edition.
Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)
22-03-2000
Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials
6 Apparatus
7 Sampling and sample preparation
8 Clean-up procedure
9 Gaschromatographic operating conditions
10 Check on instrumental performance
11 Calibration
12 Determination
13 Calculation
14 Expression of results
15 Precision
16 Test report
Annex A (normative) Identification PCB peaks
Annex B (normative) Alternative and additional clean-up
procedures
Annex C (informative) Systematic numbering of PCB compounds
Annex D (informative) Tradenames and manufacturers
Annex E (informative) Determination of TCBTs
This European Standard specifies a method to determine the concentration of up to 12 individual or defined unresolved small groups of polychlorinated biphenyl (PCB) congeners in petroleum products and related materials by means of a specified gaschromatographic separation procedure. The gas chromatographic separation is valid for the different quantification procedures described in Part 2 of this European Standard.
Committee |
CEN/TC 19
|
DocumentType |
Standard
|
PublisherName |
Comite Europeen de Normalisation
|
Status |
Current
|
Standards | Relationship |
NBN EN 12766-1 : 2000 | Identical |
UNI EN 12766-1 : 2001 | Identical |
I.S. EN 12766-1:2000 | Identical |
UNE-EN 12766-1:2000 | Identical |
SN EN 12766-1 : 2000 | Identical |
NF EN 12766-1 : 2000 | Identical |
NEN EN 12766-1 : 2000 | Identical |
NS EN 12766-1 : 1ED 2000 | Identical |
PN EN 12766-1 : 2010 | Identical |
IP 462-1 : 2001 | Identical |
SS-EN 12766-1 : 2000 | Identical |
DIN EN 12766-1:2000-11 | Identical |
BS 2000-462(2001) : 2001 | Identical |
BS EN 12766-1:2000 | Identical |
BS 2000-462.3(2004) : 2004 | PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD) |
BS EN 15308:2016 | Characterization of waste. Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection |
DIN EN 16167:2012-11 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
I.S. EN 12766-3:2005 | PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD) |
EN 1948-4:2010+A1:2013 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs |
EN 12766-2:2001 | Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content |
I.S. EN 1948-4:2010 | STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS |
UNI EN 16167 : 2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
BS EN 12766-3:2004 | Petroleum products and used oils. Determination of PCBs and related products Determination and quantification of polychlorinated terphenyls (PCT) and polychlorinated benzyl toluenes (PCBT) content by gas chromatography (GC) using an electron capture detector (ECD) |
EN 15308:2016 | Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection |
UNE-EN 15308:2017 | Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection |
05/30133366 DC : DRAFT MAY 2005 | EN 5XXXX BTTF 116-1 - STANDARD FOR THE INVENTORY, CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS |
BS EN 16167:2012 | Sludge, treated biowaste and soil. Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD) |
DIN EN 1948-4:2014-03 | STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS |
06/30159746 DC : 0 | BS EN 50503 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - STANDARD FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS |
12/30231385 DC | BS ISO 13876. Soil quality. Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD) |
01/124547 DC : DRAFT JAN 2002 | PREN 12766-3 - PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD) |
PREN 15308 : DRAFT 2015 | CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION |
17/30364002 DC : 0 | BS EN 16167 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
BS 2000-462.2(2001) : 2001 | METHODS OF TEST FOR PETROLEUM AND ITS PRODUCTS - PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT |
ISO 13876:2013 | Soil quality — Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD) |
I.S. EN 12766-2:2001 | PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 2: CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT |
05/30136951 DC : 0 | EN 15308 - CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE, SOIL AND SLUDGE BY USING CAPILLARY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION |
10/30147454 DC : 0 | BS EN 16167 - SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
UNE-EN 1948-4:2011 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs |
I.S. EN 16167:2012 | SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRONCAPTURE DETECTION (GC-ECD) |
PREN 16167 : DRAFT 2017 | SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD) |
I.S. EN 15308:2016 | CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION |
BS EN 1948-4 : 2010 | STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS |
15/30330799 DC : 0 | BS EN 15308 - CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION |
CLC/TR 50503:2010 | Guidelines for the inventory control, management, decontamination and/or disposal of electrical equipment and insulating liquids containing PCBs |
S.R. CLC/TR 50503:2010 | GUIDELINES FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS |
PREN 12766-3 : DRAFT 2001 | PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD) |
UNI EN 1948-4 : 2014 | STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS |
EN 16167:2012 | Sludge, treated biowaste and soil - Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD) |
DIN EN 12766-3:2005-02 | Petroleum products and used oils - Determination of PCBs and related products - Part 3: Determination and quantification of polychlorinated terphenyls (PCT) and polychlorinated benzyl toluenes (PCBT) content by gas chromatography (GC) using an electron capture detector (ECD) |
BS EN 12766-2:2001 | Methods of test for petroleum and its products. Petroleum products and used oils. Determination of PCBs and related products Calculation of polychlorinated biphenyl (PCB) content |
ISO 3171:1988 | Petroleum liquids — Automatic pipeline sampling |
ISO 3170:2004 | Petroleum liquids — Manual sampling |
ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
EN ISO 3170:2004 | Petroleum liquids - Manual sampling (ISO 3170:2004) |
EN ISO 3171:1999 | Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988) |
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