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    I.S. EN 15308:2016

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    Withdrawn A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
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    CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION

    Available format(s):  Hardcopy, PDF

    Withdrawn date:  31-01-2021

    Language(s):  English

    Published date:  01-01-2016

    Publisher:  National Standards Authority of Ireland

    For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.
    Only cited Standards give presumption of conformance to New Approach Directives/Regulations.

    Dates of withdrawal of national standards are available from NSAI.

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    Table of Contents - (Show below) - (Hide below)

    National Foreword
    European foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Reagents
    6 Apparatus
    7 Safety precautions
    8 Interferences
    9 Sample storage
    10 Pretreatment
    11 Procedure
    12 Calculation
    13 Test report
    Annex A (informative) - Performance characteristics
    Annex B (informative) - Examples of GC-MS
            chromatograms of a calibration standard
            solution and a contaminated soil sample
    Annex C (informative) - Examples of GC-ECD
            chromatograms of a calibration standard
            solution and a cable shredder sample
    Annex D (normative) - Calculation method for
            the estimation of total PCB content
    Annex E (informative) - Summary of general
            requirements and recommendations
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines a method for quantitative determination of seven polychlorinated biphenyl congeners (PCB-28, PCB-52, PCB-101, PCB-118, PCB-138, PCB-153 and PCB-180) in solid waste using high-resolution gas chromatography with electron capture or mass spectrometric detection.

    General Product Information - (Show below) - (Hide below)

    Document Type Standard
    Publisher National Standards Authority of Ireland
    Status Withdrawn
    Superseded By
    Supersedes

    Standards Referencing This Book - (Show below) - (Hide below)

    EN ISO 6468 : 1996 WATER QUALITY - DETERMINATION OF CERTAIN ORGANOCHLORINE INSECTICIDES, POLYCHLORINATED BIPHENYLS AND CHLOROBENZENES - GAS CHROMATOGRAPHIC METHOD AFTER LIQUID-LIQUID EXTRACTION
    EN 12766-1:2000 Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)
    ISO 11464:2006 Soil quality Pretreatment of samples for physico-chemical analysis
    ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
    EN 61619:1997 Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography
    EN 14346:2006 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT
    ISO 14507:2003 Soil quality Pretreatment of samples for determination of organic contaminants
    EN 12766-2:2001 Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content
    EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
    EN ISO 22892:2011 Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
    ISO 6468:1996 Water quality Determination of certain organochlorine insecticides, polychlorinated biphenyls and chlorobenzenes Gas chromatographic method after liquid-liquid extraction
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