• EN 14331:2004

    Current The latest, up-to-date edition.

    Liquid petroleum products - Separation and characterisation of fatty acid methyl esters (FAME) from middle distillates - Liquid chromatography (LC)/gas chromatography (GC) method

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    Published date:  24-03-2004

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Principle
    4 Reagents and materials
    5 Apparatus
    6 Sampling
    7 Procedure
    8 Determination of the composition of a mixture of methyl esters
    9 Expression of results
    10 Precision
    11 Interpretation of results
    12 Test report
    Annex A (normative) Summary of the conditions for analysis of
            fatty acid methyl esters by gas chromatography
    Annex B (informative) Example of a FAME chromatogram
    Annex C (informative) Typical compositional data for fatty
            acids in vegetable oils
    Bibliography

    Abstract - (Show below) - (Hide below)

    This European Standard specifies a method for the separation of fatty acid methyl esters (FAME) from middle distillate fuel by liquid chromatography (LC) and for quantitative determination of the individual esters by gas chromatography (GC). This method is applicable to FAME of vegetable or animal origin that contain methyl esters between C14 to C24. These FAME are mainly composed of C16 - C18 fatty acids. This method is applicable whatever the origin of the middle distillate fuel.This test method has been evaluated for the separation and characterisation of FAME present at up to 5 % (V/V) in middle distillate fuel.NOTEFor the purposes of this European Standard, the terms "% (m/m)" and "% (V/V)" are used to represent respectively the mass fraction and the volume fraction.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 19
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    09/30205523 DC : 0 BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
    11/30249539 DC : 0 BS EN 590 - AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
    BS EN 590 : 2013 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
    I.S. EN 16300:2012 AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE IN FATTY ACID METHYL ESTERS (FAME) - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
    EN 16734:2016 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
    EN 15940:2016 Automotive fuels - Paraffinic diesel fuel from synthesis or hydrotreatment - Requirements and test methods
    BS EN 16734 : 2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
    I.S. EN 14213:2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
    DIN EN 16300:2012-11 Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data
    UNE-EN 16300:2013 Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data
    BS EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    DIN EN 14214:2014-06 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    I.S. EN 16734:2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
    DIN EN 14214 E : 2003 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    14/30298209 DC : 0 BS EN 16734 - AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
    BS 2000-607(2012) : 2012 AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE IN FATTY ACID METHYL ESTERS (FAME) - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
    PREN 590 : DRAFT 2011 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
    UNE-EN 16734:2017 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
    I.S. EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    UNI EN 14214 : 2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    EN 14214:2012+A1:2014/AC:2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    DIN EN 15940 E : 2016 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
    PREN 14214 : DRAFT 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
    BS EN 16300:2012 Automotive fuels. Determination of iodine value in fatty acid methyl esters (FAME). Calculation method from gas chromatographic data
    11/30245755 DC : 0 BS EN 16300 - AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
    UNI EN 16300 : 2013 AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE IN FATTY ACID METHYL ESTERS (FAME) - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
    DIN EN 15940:2016-09 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
    EN 590:2013 Automotive fuels - Diesel - Requirements and test methods
    BS EN 14213:2003 Heating fuels. Fatty acid methyl esters (FAME). Requirements and test methods
    EN 14213:2003/AC:2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
    EN 16300:2012 Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data
    DIN EN 590:2017-10 Automotive fuels - Diesel - Requirements and test methods (includes Amendment :2017)
    I.S. EN 590:2013+A1:2017&LC:2017 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
    UNE-EN 14214:2013 Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods
    UNE-EN 15940:2016 Automotive fuels - Paraffinic diesel fuel from synthesis or hydrotreatment - Requirements and test methods
    DIN EN 14213 E : 2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
    UNE-EN 590:2014 Automotive fuels - Diesel - Requirements and test methods
    DIN EN 14214:2003-11 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    DIN EN 14213:2003-11 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
    EN 14103:2011 Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of ester and linolenic acid methyl ester contents
    ISO 5508:1990 Animal and vegetable fats and oils Analysis by gas chromatography of methyl esters of fatty acids
    EN ISO 5508 : 1995 ANIMAL AND VEGETABLE FATS AND OILS - ANALYSIS BY GAS CHROMATOGRAPHY OF METHYL ESTERS OF FATTY ACIDS
    EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
    EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)
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