EN 14538:2006
Current
The latest, up-to-date edition.
Fat and oil derivatives - Fatty acid methyl ester (FAME) - Determination of Ca, K, Mg and Na content by optical emission spectral analysis with inductively coupled plasma (ICP OES)
07-06-2006
Foreword
1 Scope
2 Normative references
3 Principle
4 Chemicals
5 Apparatus
6 Sampling
7 Preparation of the calibration solutions and the
blank solution
7.1 General
7.2 Blank solution
7.3 Calibration solution with a nominal element
content of 0,5 mg/kg
7.4 Calibration solution with a nominal element
content of 1 mg/kg
7.5 Calibration solution with a nominal element
content of 5 mg/kg
7.6 Calibration solution with a nominal element
content of 10 mg/kg
8 Calibration
8.1 General
8.2 Calibration
8.3 Check of calibration
9 Sample analysis
9.1 Sample preparation
9.2 Measurement
10 Calculation
11 Results
12 Precision
12.1 Repeatability
12.2 Reproducibility
13 Test report
This document specifies a procedure for the direct determination of the soap building elements Calcium (Ca), Magnesium (Mg), Sodium (Na) and Potassium (K) in fatty acid methyl esters (FAME) by ICP OES at levels of about 1 mg/kg to 10 mg/kg.
| Committee |
CEN/TC 19
|
| DevelopmentNote |
Supersedes PREN 14538. (12/2007)
|
| DocumentType |
Standard
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Current
|
| Supersedes |
| Standards | Relationship |
| NS EN 14538 : 1ED 2006 | Identical |
| SS-EN 14538:2006 | Identical |
| BS 2000-547(2006) : 2006 | Identical |
| NF EN 14538 : 2007 | Identical |
| SN EN 14538 : 2006 | Identical |
| NBN EN 14538 : 2006 | Identical |
| UNI EN 14538 : 2006 | Identical |
| GOST R EN 14538 : 2009 | Identical |
| PN EN 14538 : 2008 | Identical |
| UNE-EN 14538:2006 | Identical |
| BS EN 14538:2006 | Identical |
| IP 547 : 2007 | Identical |
| NEN EN 14538 : 2006 | Identical |
| I.S. EN 14538:2006 | Identical |
| DIN EN 14538:2006-09 | Identical |
| 09/30205523 DC : 0 | BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS |
| 15/30303049 DC : 0 | BS ISO 21033 - ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF TRACE ELEMENTS BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES) |
| BS ISO 21033:2016 | Animal and vegetable fats and oils. Determination of trace elements by inductively coupled plasma optical emission spectroscopy (ICP-OES) |
| BS EN 14214:2012 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| UNE-EN 14214:2013 | Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods |
| CEN/TR 17144:2017 | Resistance of metallic materials to liquid biogenic and alternative fuels and their blends |
| BS PD ISO/TS 21033 : 2011 | ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF TRACE ELEMENTS BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES) |
| DIN EN 14214:2014-06 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| S.R. CEN/TR 17144:2017 | RESISTANCE OF METALLIC MATERIALS TO LIQUID BIOGENIC AND ALTERNATIVE FUELS AND THEIR BLENDS |
| I.S. EN 14214:2012 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| DD ISO/TS 21033 : 2011 | ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF TRACE ELEMENTS BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES) |
| ISO 21033:2016 | Animal and vegetable fats and oils Determination of trace elements by inductively coupled plasma optical emission spectroscopy (ICP-OES) |
| UNI EN 14214 : 2014 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| ISO/TS 21033:2011 | Animal and vegetable fats and oils Determination of trace elements by inductively coupled plasma optical emission spectroscopy (ICP-OES) |
| PREN 14214 : DRAFT 2009 | AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS |
| PD CEN/TR 17144:2017 | Resistance of metallic materials to liquid biogenic and alternative fuels and their blends |
| DIN EN 14214:2003-11 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| ISO 3171:1988 | Petroleum liquids — Automatic pipeline sampling |
| ISO 3170:2004 | Petroleum liquids — Manual sampling |
| EN ISO 3170:2004 | Petroleum liquids - Manual sampling (ISO 3170:2004) |
| EN ISO 3171:1999 | Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988) |
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