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Fat and oil derivatives - Fatty acid methyl ester (FAME) - Determination of Ca, K, Mg and Na content by optical emission spectral analysis with inductively coupled plasma (ICP OES)
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Published date: 06-06-2006
Publisher: Comite Europeen de Normalisation
Foreword1 Scope2 Normative references 3 Principle4 Chemicals5 Apparatus6 Sampling7 Preparation of the calibration solutions and the blank solution 7.1 General 7.2 Blank solution 7.3 Calibration solution with a nominal element content of 0,5 mg/kg 7.4 Calibration solution with a nominal element content of 1 mg/kg 7.5 Calibration solution with a nominal element content of 5 mg/kg 7.6 Calibration solution with a nominal element content of 10 mg/kg8 Calibration 8.1 General 8.2 Calibration 8.3 Check of calibration 9 Sample analysis 9.1 Sample preparation 9.2 Measurement10 Calculation11 Results12 Precision 12.1 Repeatability 12.2 Reproducibility13 Test report
This document specifies a procedure for the direct determination of the soap building elements Calcium (Ca), Magnesium (Mg), Sodium (Na) and Potassium (K) in fatty acid methyl esters (FAME) by ICP OES at levels of about 1 mg/kg to 10 mg/kg.
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