EN 15779:2009+A1:2013
Current
The latest, up-to-date edition.
Petroleum products and fat and oil derivates - Fatty acid methyl esters (FAME) for diesel engines - Determination of polyunsaturated (≥4 double bonds) fatty acid methyl esters (PUFA) by gas chromatography
25-09-2013
Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Apparatus
5 Reagents and materials
6 Sampling
7 Procedure
8 Calculation
9 Expression of results
10 Precision
11 Test report
Bibliography
This European Standard specifies a method for the determination of the polyunsaturated (≥ 4 double bonds) fatty acid (PUFA) methyl esters content of fatty acid methyl ester (FAME) as a whole between 0,6 % (m/m) and 1,5 % (m/m).The method covers the predominant four polyunsaturated fatty acid methyl esters of eicosatetraenoic acid (C 20:4 (n-6)), eicosapentaenoic acid (C 20:5 (n-3)), docosapentaenoic acid (C 22:5 (n 3), and docosahexaenoic acid (C 22:6 (n 3)). Studies have indicated that based on the linearity of results from this European Standard, PUFA methyl esters can be determined in FAME in the range between 0,3 % (m/m) to 3,0 % (m/m). However, the precision was not established in that range, as no samples within the upper ranges where included in the final interlaboratory test (see 10.1).Although the method is applicable to all uses, it is predominantly for FAME for use in diesel engines.NOTE 1For the purposes of this document, the term “% (m/m)” is used to represent the mass fraction of a material.NOTE 2This European Standard is based on A.O.C.S Official Method Ce 1b-89 [1].
Committee |
CEN/TC 19
|
DevelopmentNote |
2009 Edition Re-Issued in September 2013 & incorporates AMD 1 2013. (10/2013)
|
DocumentType |
Standard
|
PublisherName |
Comite Europeen de Normalisation
|
Status |
Current
|
Standards | Relationship |
PN EN 15779 : 2011 + A1 2013 | Identical |
UNE-EN 15779:2010 | Identical |
NF EN 15779 : 2010 + A1 2014 | Identical |
BS 2000-578(2009) : 2009 | Identical |
BS EN 15779 : 2009 | Identical |
UNI EN 15779 : 2013 | Identical |
NS EN 15779 : 2009 + A1 2013 | Identical |
I.S. EN 15779:2009 | Identical |
IP 578 : 2015 | Identical |
DIN EN 15779:2013-12 | Identical |
SN EN 15779+A1:2013 | Identical |
NEN EN 15779 : 2009 + A1 2013 | Identical |
NBN EN 15779 : 2010 + A1 2013 | Identical |
UNE-EN 15779:2010+A1:2013 | Identical |
BS EN 15779:2009+A1:2013 | Identical |
09/30205523 DC : 0 | BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS |
BS EN 14214:2012 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
DIN EN 14214:2014-06 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
PD ISO/TS 17307:2016 | Petroleum products. Biodiesel. Determination of total esters content by gas chromatography |
I.S. EN 14214:2012 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
ISO/TS 17307:2016 | Petroleum products — Biodiesel — Determination of total esters content by gas chromatography |
UNI EN 14214 : 2014 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
PREN 14214 : DRAFT 2009 | AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS |
18/30369065 DC : DRAFT FEB 2018 | BS EN 14214 AMD 2 - LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
UNE-EN 14214:2013 | Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods |
DIN EN 14214:2003-11 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
ISO 3171:1988 | Petroleum liquids — Automatic pipeline sampling |
ISO 3170:2004 | Petroleum liquids — Manual sampling |
ISO 4259:2006 | Petroleum products Determination and application of precision data in relation to methods of test |
EN ISO 5509:2000 | Animal and vegetable fats and oils - Preparation of methyl esters of fatty acids (ISO 5509:2000) |
ISO 5509:2000 | Animal and vegetable fats and oils Preparation of methyl esters of fatty acids |
EN ISO 3170:2004 | Petroleum liquids - Manual sampling (ISO 3170:2004) |
EN ISO 3171:1999 | Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988) |
EN ISO 4259:2006 | Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006) |
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