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EN 15934:2012

Current

Current

The latest, up-to-date edition.

Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content

Published date

22-08-2012

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Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Sample preparation
6 Method A - Drying at 105 degrees C
7 Method B - Direct Karl-Fischer-titration
   (volumetric/coulometric detection)
8 Calculation of dry matter fraction
9 Precision
10 Test report
Annex A (informative) - Repeatability and reproducibility
Annex B (informative) - Azeotropic distillation with toluene
Annex C (informative) - Summary of general requirements
        and recommendations

This European Standard specifies methods for the calculation of the dry matter of sludge, treated biowaste, soil and waste for which the results of performed analysis are to be calculated to the dry matter basis. Depending on the nature and origin of the sample, the calculation is based on a determination of the dry residue (Method A) or a determination of the water content (Method B). It applies to samples containing more than 1 % (mass fraction) of dry residue or more than 1 % (mass fraction) of water.Method A applies to sludge, treated biowaste, soil and solid waste, Method B applies to liquid waste and to samples which are suspected or known to contain volatiles except for water.

Committee
CEN/TC 444
DevelopmentNote
Supersedes PREN 15934. (09/2012)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
DIN EN 15934:2012-11 Identical
NEN EN 15934 : 2012 Identical
I.S. EN 15934:2012 Identical
UNE-EN 15934:2012 Identical
PN EN 15934 : 2013 Identical
SN EN 15934:2012 Identical
NF EN 15934 : 2012 Identical
NBN EN 15934 : 2012 Identical
NS EN 15934 : 2012 Identical
BS EN 15934:2012 Identical
UNI EN 15934 : 2012 Identical
PNE-prEN 15934 Identical

S.R. CEN/TS 16171:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
ISO 18187:2016 Soil quality — Contact test for solid samples using the dehydrogenase activity of Arthrobacter globiformis
BS ISO 16729:2013 Soil quality. Digestion of nitric acid soluble fractions of elements
S.R. CEN/TS 16170:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
PD CEN/TR 16193:2013 Sludge, treated biowaste and soil. Detection and enumeration of Escherichia coli
S.R. CEN/TR 16193:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETECTION AND ENUMERATION OF ESCHERICHIA COLI
I.S. EN 15936:2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF TOTAL ORGANIC CARBON (TOC) BY DRY COMBUSTION
EN ISO 18187:2018 Soil quality - Contact test for solid samples using the dehydrogenase activity of Arthrobacter globiformis (ISO 18187:2016)
DIN EN 16167:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
17/30363999 DC : 0 BS EN 16190 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
17/30364005 DC : 0 BS EN 16181 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
CEN/TS 16171:2012 Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS)
CEN/TS 16172:2013 Sludge, treated biowaste and soil - Determination of elements using graphite furnace atomic absorption spectrometry (GF-AAS)
EN 16175-2:2016 Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS)
DIN EN 15935:2012-11 Sludge, treated biowaste, soil and waste - Determination of loss on ignition; German version EN 15935:2012
CEN/TS 16175-1:2013 Sludge, treated biowaste and soil - Determination of mercury - Part 1: Cold-vapour atomic absorption spectrometry (CV-AAS)
DIN EN 15936:2012-11 Sludge, treated biowaste, soil and waste - Determination of total organic carbon (TOC) by dry combustion
BS EN 16179:2012 Sludge, treated biowaste and soil. Guidance for sample pretreatment
UNI CEN/TS 16170 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
UNI EN 16169 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN
I.S. EN 16173:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS
I.S. EN ISO 18187:2018 SOIL QUALITY - CONTACT TEST FOR SOLID SAMPLES USING THE DEHYDROGENASE ACTIVITY OF ARTHROBACTER GLOBIFORMIS (ISO 18187:2016)
PREN 16190 : DRAFT 2017 SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
S.R. CEN/TS 16181:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
VDI 3957 Blatt 2:2016-03 Biological measuring techniques for the determination and assessment of effects of air pollutants on plants (biomonitoring) - Method of the standardised grass exposure
ISO 13913:2014 Soil quality Determination of selected phthalates using capillary gas chromatography with mass spectrometric detection (GC/MS)
BS EN 16175-2:2016 Sludge, treated biowaste and soil. Determination of mercury Cold-vapour atomic fluorescence spectrometry (CV-AFS)
BS EN 16166:2012 Sludge, treated biowaste and soil. Determination of adsorbable organically bound halogens (AOX)
BS EN 15935:2012 Sludge, treated biowaste, soil and waste. Determination of loss on ignition
UNI EN 15936 : 2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF TOTAL ORGANIC CARBON (TOC) BY DRY COMBUSTION
UNI CEN/TS 16172 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
BS ISO 18187 : 2016 SOIL QUALITY - CONTACT TEST FOR SOLID SAMPLES USING THE DEHYDROGENASE ACTIVITY OF ARTHROBACTER GLOBIFORMIS
UNI EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
UNI CEN/TS 16189 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF LINEAR ALKYLBENZENE SULFONATES (LAS) BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) WITH FLUORESCENCE DETECTION (FLD) OR MASS SELECTIVE DETECTION (MS)
DIN EN 16173:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS
I.S. EN 16167:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRONCAPTURE DETECTION (GC-ECD)
I.S. EN 16166:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ADSORBABLE ORGANICALLY BOUND HALOGENS (AOX)
I.S. EN 15935:2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF LOSS ON IGNITION
EN 15935:2012 Sludge, treated biowaste, soil and waste - Determination of loss on ignition
I.S. EN 16168:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF TOTAL NITROGEN USING DRY COMBUSTION METHOD
17/30364002 DC : 0 BS EN 16167 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
I.S. EN 16175-1:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
UNE-EN 16179:2013 Sludge, treated biowaste and soil - Guidance for sample pretreatment
UNI EN 16179 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT
UNI CEN/TS 16171 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
UNI EN 16168 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF TOTAL NITROGEN USING DRY COMBUSTION METHOD
UNI CEN/TS 16181 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
BS EN ISO 18187:2018 Soil quality. Contact test for solid samples using the dehydrogenase activity of Arthrobacter globiformis
17/30362321 DC : 0 BS EN ISO 23161 - SOIL QUALITY - DETERMINATION OF SELECTED ORGANOTIN COMPOUNDS - GAS-CHROMATOGRAPHIC METHOD
BS EN 15936:2012 Sludge, treated biowaste, soil and waste. Determination of total organic carbon (TOC) by dry combustion
DIN EN 16169:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN
S.R. CEN/TS 16172:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
S.R. CEN/TS 16175-2:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
DIN EN 16168:2012-11 Sludge, treated biowaste and soil - Determination of total nitrogen using dry combustion method; German version EN 16168:2012
UNI CEN/TS 16182 : 2012 SLUDGE TREATED BIOWASTE AND SOIL - DETERMINATION OF NONYLPHENOLS (NP) AND NONYLPHENOL-MONO- AND DIETHOXYLATES USING GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GCMS)
I.S. EN 16169:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN
I.S. EN 16171:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
PREN 16167 : DRAFT 2017 SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
EN 16169:2012 Sludge, treated biowaste and soil - Determination of Kjeldahl nitrogen
EN 16179:2012 Sludge, treated biowaste and soil - Guidance for sample pretreatment
EN 16168:2012 Sludge, treated biowaste and soil - Determination of total nitrogen using dry combustion method
EN 16173:2012 Sludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements
EN 15936:2012 Sludge, treated biowaste, soil and waste - Determination of total organic carbon (TOC) by dry combustion
BS EN 16168:2012 Sludge, treated biowaste and soil. Determination of total nitrogen using dry combustion method
UNI CEN/TS 16183 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF SELECTED PHTHALATES USING CAPILLARY GAS CHROMATOGRAPHY WITH MASS SPECTROMETRIC DETECTION (GC-MS)
BS EN 16169:2012 Sludge, treated biowaste and soil. Determination of Kjeldahl nitrogen
UNI EN 16173 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS
DIN EN 16179:2012-11 Sludge, treated biowaste and soil - Guidance for sample pretreatment
BS EN 16173:2012 Sludge, treated biowaste and soil. Digestion of nitric acid soluble fractions of elements
DIN EN 16166:2012-11 Sludge, treated biowaste and soil - Determination of adsorbable organically bound halogens (AOX)
BS ISO 13913:2014 Soil quality. Determination of selected phthalates using capillary gas chromatography with mass spectrometric detection (GC/MS)
UNI EN 15935 : 2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF LOSS ON IGNITION
I.S. EN 16179:2012 SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT
I.S. EN 16170:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
I.S. EN 16175-2:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
S.R. CEN/TS 16175-1:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
EN 16167:2012 Sludge, treated biowaste and soil - Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
CEN/TR 16193:2013 Sludge, treated biowaste and soil - Detection and enumeration of Escherichia coli
ISO 16729:2013 Soil quality — Digestion of nitric acid soluble fractions of elements
CEN/TS 16181:2013 Sludge, treated biowaste and soil - Determination of polycyclic aromatic hydrocarbons (PAH) by gas chromatography (GC) and high performance liquid chromatography (HPLC)
CEN/TS 16175-2:2013 Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS)
UNI EN 16166 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ADSORBABLE ORGANICALLY BOUND HALOGENS (AOX)
CEN/TS 16170:2012 Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma optical emission spectrometry (ICP-OES)
EN 16166:2012 Sludge, treated biowaste and soil - Determination of adsorbable organically bound halogens (AOX)

EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
EN 16179:2012 Sludge, treated biowaste and soil - Guidance for sample pretreatment

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