• S.R. CEN/TS 16181:2013

    Withdrawn A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

    SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)

    Available format(s):  Hardcopy, PDF

    Withdrawn date:  09-01-2019

    Language(s):  English

    Published date:  01-01-2013

    Publisher:  National Standards Authority of Ireland

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Interferences
    6 Safety remarks
    7 Reagents
    8 Apparatus
    9 Sample storage and preservation
    10 Procedure
    11 Performance characteristics
    12 Precision
    13 Test report
    Annex A (informative) - Repeatability and
            reproducibility data
    Annex B (informative) - Examples of instrumental
            conditions and chromatograms
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines the quantitative determination of 16 polycyclic aromatic hydrocarbons (PAH) in sludge, soil and treated biowaste using GC-MS and HPLC-UV-DAD/FLD covering a wide range of PAH contamination levels.

    General Product Information - (Show below) - (Hide below)

    Document Type Standard
    Publisher National Standards Authority of Ireland
    Status Withdrawn
    Superseded By

    Standards Referencing This Book - (Show below) - (Hide below)

    EN ISO 17993 : 2003 WATER QUALITY - DETERMINATION OF 15 POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WATER BY HPLC WITH FLUORESCENCE DETECTION AFTER LIQUID-LIQUID EXTRACTION
    DIN 38414-23:2002-02 GERMAN STANDARD METHODS FOR THE EXAMINATION OF WATER, WASTE WATER AND SLUDGE - SLUDGE AND SEDIMENTS (GROUP S) - PART 23: DETERMINATION OF 15 POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) AND FLUORESCENCE DETECTION (S 23)
    ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
    ISO 18287:2006 Soil quality Determination of polycyclic aromatic hydrocarbons (PAH) Gas chromatographic method with mass spectrometric detection (GC-MS)
    EN 15308:2016 Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
    ISO 5667-15:2009 Water quality — Sampling — Part 15: Guidance on the preservation and handling of sludge and sediment samples
    ISO 17993:2002 Water quality — Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction
    ISO 16720:2005 Soil quality Pretreatment of samples by freeze-drying for subsequent analysis
    ISO 28540:2011 Water quality — Determination of 16 polycyclic aromatic hydrocarbons (PAH) in water — Method using gas chromatography with mass spectrometric detection (GC-MS)
    EN ISO 16720:2007 Soil quality - Pretreatment of samples by freeze-drying for subsequent analysis (ISO 16720:2005)
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
    EN ISO 22892:2011 Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
    EN 15527:2008 Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS)
    EN ISO 5667-15:2009 Water quality - Sampling - Part 15: Guidance on the preservation and handling of sludge and sediment samples (ISO 5667-15:2009)
    EN 15934:2012 Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content
    EN 16179:2012 Sludge, treated biowaste and soil - Guidance for sample pretreatment
    ISO 18512:2007 Soil quality Guidance on long and short term storage of soil samples
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