• EN ISO 16017-2:2003

    Current The latest, up-to-date edition.

    Indoor, ambient and workplace air - Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography - Part 2: Diffusive sampling (ISO 16017-2:2003)

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    Published date:  15-05-2003

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Principle
    4 Reagents and materials
    5 Apparatus
    6 Sample tube conditioning
    7 Sampling
    8 Procedure
       8.1 Safety precautions
       8.2 Desorption and analysis
       8.3 Calibration
       8.4 Determination of sample concentration
       8.5 Determination of desorption efficiency
       8.6 Calibration of uptake rate
    9 Calculations
       9.1 Mass concentration of analyte
       9.2 Volume concentration of analyte
       9.3 Uptake rates
    10 Interferences
    11 Performance characteristics
    12 Test report
    13 Quality control
    Annex A (informative) Operating principles of diffusive
            sampling
    Annex B (informative) Description of sorbent types
    Annex C (informative) Guidance on sorbent selection
    Annex D (informative) Guidance on sorbent use
    Annex E (informative) Summary of data on overall uncertainty,
            precision, bias and storage
    Bibliography

    Abstract - (Show below) - (Hide below)

    ISO 16017-2:2003 gives general guidance for the sampling and analysis of volatile organic compounds (VOCs) in air. It is applicable to indoor, ambient and workplace air.ISO 16017-2:2003 is applicable to a wide range of VOCs, including hydrocarbons, halogenated hydrocarbons, ester, glycol ethers, ketones and alcohols. A number of sorbents are recommended for the sampling of these VOCs, each sorbent having a different range of applicability. Very polar compounds generally require derivatisation; very low boiling compounds are only partially retained by the sorbents and can only be estimated qualitatively. Semi-volatile compounds are fully retained by the sorbents, but may only be partially recovered.ISO 16017-2:2003 is applicable to the measurement of airborne vapours of VOCs in a concentration range of approximately 0,002 mg/m3 to 100 mg/m3 individual organic for an exposure time of 8 h, or 0,3 g/m3 to 300 g/m3 individual organic for an exposure time of four weeks.The upper limit of the useful range is set by the sorptive capacity of the sorbent used and by the linear dynamic range of the gas chromatograph column and detector or by the sample splitting capability of the analytical instrumentation used. The lower limit of the useful range depends on the noise level of the detector and on blank levels of analyte and/or interfering artefacts on the sorbent tubes. Artefacts are typically sub-nanogram for well-conditioned Tenax GR and carbonaceous sorbents, carbonized molecular sieves and pure charcoals; at low nanogram levels for Tenax TA and at 5 ng to 50 ng levels for other porous polymers.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 264
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    06/30155808 DC : DRAFT SEP 2006 BS EN 13999-4 - ADHESIVES - SHORT-TERM METHOD FOR MEASURING THE EMISSION PROPERTIES OF LOW-SOLVENT OR SOLVENT-FREE ADHESIVES AFTER APPLICATION - PART 4: DETERMINATION OF VOLATILE DIISOCYANATES
    BS EN 13528-3:2003 Ambient air quality. Diffusive samplers for the determination of concentrations of gases and vapours. Requirements and test methods Guide to selection, use and maintenance
    BS EN 14662-4:2005 Ambient air quality. Standard method for measurement of benzene concentrations Diffusive sampling followed by thermal desorption and gas chromatography
    I.S. EN 13999-4:2007 ADHESIVES - SHORT TERM METHOD FOR MEASURING THE EMISSION PROPERTIES OF LOW-SOLVENT OR SOLVENT-FREE ADHESIVES AFTER APPLICATION - PART 4: DETERMINATION OF VOLATILE DIISOCYANATES
    I.S. EN 838:2010 WORKPLACE EXPOSURE - PROCEDURES FOR MEASURING GASES AND VAPOURS USING DIFFUSIVE SAMPLERS - REQUIREMENTS AND TEST METHODS
    EN 13528-3:2003 Ambient air quality - Diffusive samplers for the determination of concentrations of gases and vapours - Requirements and test methods - Part 3: Guide to selection, use and maintenance
    16/30332593 DC : 0 BS EN 15759-2 - CONSERVATION OF CULTURAL HERITAGE - INDOOR CLIMATE - PART 2: VENTILATION TO PROTECT HERITAGE BUILDINGS AND COLLECTIONS
    I.S. EN 15759-2:2018 CONSERVATION OF CULTURAL HERITAGE - INDOOR CLIMATE - PART 2: VENTILATION MANAGEMENT FOR THE PROTECTION OF CULTURAL HERITAGE BUILDINGS AND COLLECTIONS
    UNI EN 838 : 2010 WORKPLACE EXPOSURE - PROCEDURES FOR MEASURING GASES AND VAPOURS USING DIFFUSIVE SAMPLERS - REQUIREMENTS AND TEST METHODS
    VDI 4300 Blatt 9:2005-08 Measurement of indoor air pollution - Measurement strategy for carbon dioxide (CO)
    EN 15759-2:2018 Conservation of cultural heritage - Indoor climate - Part 2: Ventilation management for the protection of cultural heritage buildings and collections
    UNI EN 13999-4 : 2009 ADHESIVES - SHORT TERM METHOD FOR MEASURING THE EMISSION PROPERTIES OF LOW-SOLVENT OR SOLVENT-FREE ADHESIVES AFTER APPLICATION - PART 4: DETERMINATION OF VOLATILE DIISOCYANATES
    DIN EN 13999-4:2009-08 ADHESIVES - SHORT TERM METHOD FOR MEASURING THE EMISSION PROPERTIES OF LOW-SOLVENT OR SOLVENT-FREE ADHESIVES AFTER APPLICATION - PART 4: DETERMINATION OF VOLATILE DIISOCYANATES
    DIN EN 838:2010-05 Workplace exposure - Procedures for measuring gases and vapours using diffusive samplers - Requirements and test methods
    BS EN 13999-4 : 2007 ADHESIVES - SHORT TERM METHOD FOR MEASURING THE EMISSION PROPERTIES OF LOW-SOLVENT OR SOLVENT-FREE ADHESIVES AFTER APPLICATION - PART 4: DETERMINATION OF VOLATILE DIISOCYANATES
    BS EN 838:2010 Workplace exposure. Procedures for measuring gases and vapours using diffusive samplers. Requirements and test methods
    EN 14662-4:2005 Ambient air quality - Standard method for measurement of benzene concentrations - Part 4: Diffusive sampling followed by thermal desorption and gas chromatography
    EN 838:2010 Workplace exposure - Procedures for measuring gases and vapours using diffusive samplers - Requirements and test methods
    EN 13999-4:2007+A1:2009 Adhesives - Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application - Part 4: Determination of volatile diisocyanates
    DIN EN 14662-4:2005-08 AMBIENT AIR QUALITY - STANDARD METHOD FOR MEASUREMENT OF BENZENE CONCENTRATIONS - PART 4: DIFFUSIVE SAMPLING FOLLOWED BY THERMAL DESORPTION AND GAS CHROMATOGRAPHY
    DIN EN 13528-3:2004-04 Ambient air quality - Diffuse samplers for the determination of concentrations of gases and vapours - Part 3: Guide to selection, use and maintenance

    Standards Referencing This Book - (Show below) - (Hide below)

    VDI 2119 Blatt 4:1997-08 Measurement of Particulate Precipitations - Microscopic differentiation and size fractionated determination of particle deposition on adhesive collection plates - Sigma-2 sampler
    EN 838:2010 Workplace exposure - Procedures for measuring gases and vapours using diffusive samplers - Requirements and test methods
    EN 482:2012+A1:2015 Workplace exposure - General requirements for the performance of procedures for the measurement of chemical agents
    EN 13528-1:2002 Ambient air quality - Diffusive samplers for the determination of concentrations of gases and vapours - Requirements and test methods - Part 1: General requirements
    EN 13528-2:2002 Ambient air quality - Diffusive samplers for the determination of concentrations of gases and vapours - Requirements and test methods - Part 2: Specific requirements and test methods
    ISO 6145-5:2009 Gas analysis Preparation of calibration gas mixtures using dynamic volumetric methods Part 5: Capillary calibration devices
    ISO 16000-1:2004 Indoor air — Part 1: General aspects of sampling strategy
    ISO 6145-4:2004 Gas analysis Preparation of calibration gas mixtures using dynamic volumetric methods Part 4: Continuous syringe injection method
    ISO 6145-3:1986 Gas analysis Preparation of calibration gas mixtures Dynamic volumetric methods Part 3: Periodic injections into a flowing gas stream
    ISO 6145-1:2003 Gas analysis Preparation of calibration gas mixtures using dynamic volumetric methods Part 1: Methods of calibration
    ISO 6141:2015 Gas analysis Contents of certificates for calibration gas mixtures
    ISO 6145-6:2017 Gas analysis — Preparation of calibration gas mixtures using dynamic methods — Part 6: Critical flow orifices
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