ENV 13800:2000
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), without separation of the lead matrix
26-08-2022
19-07-2000
Foreword
1 Scope
2 Normative references
3 Principle
3.1 Dissolution
3.2 Instrumental techniques
4 Apparatus
4.1 General
4.2 Volumetric glassware
4.3 Plastic ware
4.4 Instruments
5 Reagents
5.1 General
5.2 Nitric acid (HNO3)
5.3 Tartaric acid solution (C4H6O6) 300 g/l
5.4 Hydrochloric acid (HCI)
5.5 Fluoboric acid (HBF4)
5.6 Lead for matrix matching
5.7 Standard solutions
6 Sampling and sample preparation
7 Procedure
7.1 Preparation of the test solution
7.2 Preparation of the blank test solution
7.3 Dilution of the test solutions and of the blank
test solution
8 Determination of elements by FAAS
8.1 Preparation of calibration solutions
8.2 Calibration, measurements and results
9 Determination of elements by ICP-ES
9.1 Preparation of calibration solutions
9.2 Calibration, measurements and results
10 Test report
This European Prestandard specifies methods of analysis using flame atomic absorption spectrometry (FAAS) and inductively coupled plasma emission spectrometry (ICP-ES) for the determination of element contents in lead and lead alloys for the ranges given in Table 1.These methods are intended as the definitive methods in case of dispute for the determination of elements at low content in lead. They are also recommended for the analysis of Certified Reference Materials (CRM) and Reference Materials (RM) which are used in analysis according to ENV 12908.
| Committee |
CEN/TC 306
|
| DocumentType |
Standard Recommendation
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Withdrawn
|
| Standards | Relationship |
| NBN ENV 13800 : 2000 | Identical |
| UNI ENV 13800 : 2002 | Identical |
| NEN NVN ENV 13800 : 2000 | Identical |
| I.S. ENV 13800:2000 | Identical |
| DIN V ENV 13800:2000-11 | Identical |
| DD ENV 13800:2000 | Identical |
| DIN 17640-1:2004-02 | Lead alloys for general purposes |
| ENV 14029:2001 | Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation of the lead matrix |
| ENV 14138:2001 | Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation by co-precipitation |
| DD ENV 14138:2001 | Lead and lead alloys. Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emissions spectrometry (ICP-ES), after separation by co-precipitation |
| DD ENV 14029:2001 | Lead and lead alloys. Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation of the lead matrix |
| I.S. ENV 14138:2002 | LEAD AND LEAD ALLOYS - ANALYSIS BY FLAME ATOMIC ABSORPTION SPECTROMETRY (FAAS) OR INDUCTIVELY COUPLED PLASMA EMISSION SPECTROMETRY (ICP-ES), AFTER SEPARATION BY CO-PRECIPITATION |
| EN 12402:1999 | Lead and lead alloys - Methods of sampling for analysis |
| ISO 1042:1998 | Laboratory glassware — One-mark volumetric flasks |
| ISO 648:2008 | Laboratory glassware — Single-volume pipettes |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| ENV 12908:1997 | Lead and lead alloys - Analysis by Optical Emission Spectrometry (OES) with spark excitation |
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