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I.S. EN 16691:2015

Current

Current

The latest, up-to-date edition.

WATER QUALITY - DETERMINATION OF SELECTED POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2015

For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.

Only cited Standards give presumption of conformance to New Approach Directives/Regulations.


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National Foreword
European foreword
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling
8 Procedure
9 Calibration
10 Measurement of samples
11 Identification of individual compounds by means
   of GC-MS (SIM)
12 Calculation
13 Expression of results
14 Test report
Annex A (informative) - Suitable gas chromatographic
        conditions and example chromatograms -
        GC-conditions
Annex B (informative) - Repeatability and reproducibility data
Annex C (informative) - Dilution Schedules for standards
Annex D (informative) - Silica clean-up
Annex E (informative) - Examples of suitable solid-phase
        extraction disks (SPE-disks)
Bibliography

Defines a method for the determination of 7 polycyclic aromatic hydrocarbons (PAH) in whole water samples.

DocumentType
Standard
Pages
36
PublisherName
National Standards Authority of Ireland
Status
Current

Standards Relationship
EN 16691:2015 Identical

ISO 7981-1:2005 Water quality — Determination of polycyclic aromatic hydrocarbons (PAH) — Part 1: Determination of six PAH by high-performance thin-layer chromatography with fluorescence detection after liquid-liquid extraction
EN ISO 17993:2003 Water quality - Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction (ISO 17993:2002)
NEN 7777 : 2011 + C1 2012 ENVIRONMENT AND FOOD - PERFORMANCE CHARACTERISTICS OF MEASUREMENT METHODS
ISO 1042:1998 Laboratory glassware — One-mark volumetric flasks
ISO/TS 13530:2009 Water quality — Guidance on analytical quality control for chemical and physicochemical water analysis
ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 7981-2:2005 Water quality — Determination of polycyclic aromatic hydrocarbons (PAH) — Part 2: Determination of six PAH by high-performance liquid chromatography with fluorescence detection after liquid-liquid extraction
ISO 17993:2002 Water quality — Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction
ISO 5667-3:2012 Water quality Sampling Part 3: Preservation and handling of water samples
EN ISO 1042:1999 Laboratory glassware - One-mark volumetric flasks (ISO 1042:1998)
ISO 5667-1:2006 Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
ISO 28540:2011 Water quality — Determination of 16 polycyclic aromatic hydrocarbons (PAH) in water — Method using gas chromatography with mass spectrometric detection (GC-MS)
ISO 6107-2:2006 Water quality Vocabulary Part 2:
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN ISO 5667-3:2012 Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN ISO 22892:2011 Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
EN 15527:2008 Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS)
ISO/TS 28581:2012 Water quality — Determination of selected non-polar substances — Method using gas chromatography with mass spectrometric detection (GC-MS)
EN ISO 5667-1 : 2006 COR 2007 WATER QUALITY - SAMPLING - PART 1: GUIDANCE ON THE DESIGN OF SAMPLING PROGRAMMES AND SAMPLING TECHNIQUES

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